Abstract: A spray drying process and apparatus for drying a spray dryable liquid composition to a spray dried powder is described, in which the spray dryable liquid composition contains no carrier. The spray dryable liquid composition is processed at a solids concentration not exceeding 80% by weight, based on total weight of the spray dryable liquid composition, being atomized to generate an atomized spray of liquid particles of the spray dryable liquid composition into a spray drying chamber, in which the atomized spray is contacted with a stream of drying fluid flowed at temperature not exceeding 100° C. into the spray drying chamber, to form the spray dried powder.

Abstract: A spray drying process and apparatus for drying a spray dryable liquid composition to a spray dried powder is described, in which the spray dryable liquid composition contains no carrier. The spray dryable liquid composition is processed at a solids concentration not exceeding 80% by weight, based on total weight of the spray dryable liquid composition, being atomized to generate an atomized spray of liquid particles of the spray dryable liquid composition into a spray drying chamber, in which the atomized spray is contacted with a stream of drying fluid flowed at temperature not exceeding 100° C. into the spray drying chamber, to form the spray dried powder.

Abstract: A method for making a lithium-ion cell includes depositing an electrode material as a coating on a substrate of the lithium-ion cell, irradiating the deposited electrode material with microwave radiation of varying frequency, wetting the irradiated electrode material with a non-aqueous electrolyte solution, and sealing the wetted electrode material in an air-tight enclosure.

Abstract: A fuel injection valve includes: a needle valve with a seat surface at a distal end; a nozzle body with a seat section on which the seat surface rests and with an injection opening disposed downstream of the seat section; and a swirl flow generating section with a spiral groove for causing fuel injected via the injection opening to swirl. The seat surface includes a first contact point. The first contact point contacts a second contact point included in the seat section during valve closing. A line segment that is drawn by connecting the first contact point and the second contact point during valve opening intersects a virtual straight line passing a bottom of a first groove section that appears the most downstream side of a cross section of the swirl flow generating portion in a plane including a central axis of the needle valve and a bottom of a second groove section that appears one step upstream side of the first groove portion.

Abstract: The invention relates to a spinneret for spinning threads from a spinning mass—in the form of a melt or solution of natural or synthetic origin—comprising a rotationally symmetrical spinneret. The rotationally symmetrical spinneret inner part is surrounded at least partially by a rotationally symmetrical outer part, wherein in the longitudinal direction between the spinneret inner part and outer part an insulating chamber is formed, in which a gas, preferably air, is received in order to form an insulating gas layer. The invention further relates to a spinning device for spinning threads from a spinning mass, comprising a spinneret part and a gas nozzle part arranged at a distance from the spinneret part. A plurality of spinnerets according to the invention are inserted in the spinneret part and project from the spinneret part, facing the gas nozzle part, and the gas nozzle part comprises a plurality of gas nozzles associated with the spinnerets.

Abstract: An apparatus is disclosed for forming a non-woven web.

Abstract: The present invention relates to a method for purifying a liquid comprising liquid particles and residual particles. It is hereby possible to generate substantially pure water from, for instance seawater.

Abstract: The invention relates to the field of preparing nanoparticles. In particular, the invention provides a method for preparing organic or inorganic nanoparticles by instantaneous evaporation or flash evaporation, e.g. for the manufacture of nanoparticles of fertilizers, pharmaceutical or phytopharmaceutical active ingredients, or insensitive energy materials.

Abstract: An anti-gravity liquid evaporator comprises a tank body (1). The top surface of the tank body (1) is provided with an upper opening (2), the bottom surface of the tank body is provided with a lower opening (7), the inside of the tank is provided with a liquid spray nozzle (3), and plate-shaped dispersion flaps (8) are mounted in the tank body (1), wherein the dispersion flaps (8) are a plurality of horizontal flow boards (9) extending in a horizontal or inclined direction, and the horizontal flow boards (9) are connected by a vertical flow board (10) or an inclined flow board (16) that is inclined.

Abstract: The present invention generally relates to microfluidics, and to spray drying and other drying techniques. By at least partially drying fluids within a microfluidic channel, instead of or in addition to conventional spray drying techniques, better control of the drying process can be achieved in certain aspects of the invention. In addition, various embodiments of the invention are generally directed to systems and methods for drying fluids contained within a channel such as a microfluidic channel. For example, a fluid may be partially or completely dried within a microfluidic channel, prior to being sprayed into a collection region. In some embodiments, gases such as air may be directed into a channel containing a fluid, which may facilitate drying of the fluid. In some cases, the fluid may be accelerated due to the introduction of gases into the channel, and in certain embodiments, droplets of fluid may be disrupted to form smaller droplets as a result.

Abstract: A production saltwater disposal facility comprising a separator configured to receive production saltwater from a pipeline or a vehicle and separate hydrocarbons from the production saltwater, wherein the production saltwater received from the pipeline or vehicle is substantially the same composition as when the production saltwater was located in a subterranean formation, a hydrocarbon storage tank configured to receive hydrocarbons from the separator, a settling pit configured to receive the production saltwater from the separator and separate metals and/or other solids from the saltwater, an evaporator in fluid communication with the settling pit and comprising a nozzle configured to emit a stream of the saltwater along a path in air such that water in the saltwater evaporates, and a collection pit positioned under the path and configured to collect the salt from the saltwater after the water has evaporated.

Abstract: This invention relates to apparatus for a methods of crystallization of salt from brine on top of any soil surface, including repeating spraying of a ground surface, evaporation in air, controlling a moisture depth, capillary action and enhanced renewable energy to grow a layer of salt which can be collected. The brine is pumped from an underground source, sprayed in ambient air over a solid surface at a rate to either produce salt upon the ground and, if water is not completely evaporated, allowed to seep through the surface to saturate the capillary zone. In the use of a structural truss extension, a plastic or PVC pipe is isolated from the truss extension as the truss extension carries it about a hub with flow rate and speed to produce salt on the ground.

Abstract: A process for separation of solid and liquid components in a distillation whole stillage utilizing airless spray drying is disclosed, which is more efficient and economical than conventional processes. In the process, distillation whole stillage resulting from distillation of fermented biomass is first subjected to an evaporation step for separating the whole stillage into a condensate and a concentrate including water, dissolved solids and suspended solids. The concentrate is then subjected to airless steam spray drying for converting the concentrate into dried solids, steam and vapors. All steam and vapors resulting from the airless steam spray drying step are then redirected as energy source to a processing step upstream of the airless spray drying step. At least some of the steam generated in the airless spray drying step is airless steam.

Abstract: A production saltwater disposal facility comprising a separator configured to receive production saltwater from a pipeline or a vehicle and separate hydrocarbons from the production saltwater, wherein the production saltwater received from the pipeline or vehicle is substantially the same composition as when the production saltwater was located in a subterranean formation, a hydrocarbon storage tank configured to receive hydrocarbons from the separator, a settling pit configured to receive the production saltwater from the separator and separate metals and/or other solids from the saltwater, an evaporator in fluid communication with the settling pit and comprising a nozzle configured to emit a stream of the saltwater along a path in air such that water in the saltwater evaporates, and a collection pit positioned under the path and configured to collect the salt from the saltwater after the water has evaporated.

Abstract: Water evaporation devices, systems and methods are used to evaporate large quantities of water from water impoundment ponds or other waste water sources. Water evaporation devices include a water evaporation barrel having an air acceleration chamber that creates venturi suction so as to draw water from a water source into a venturi chamber. Fast moving air and water create fine water droplets within a water atomization chamber, which droplets are then emitted from the water evaporation barrel through a discharge nozzle and into the air as a spray or cloud of fine water droplets. Water evaporation devices and associated systems and methods can be used to efficiently evaporate waster water produced by a wide variety of industrial processes.

Abstract: Pressurized water evaporation systems and methods are used to evaporate large quantities of water from water impoundment ponds or other waste water sources. Water evaporation systems include one or more water evaporation barrels having an air acceleration chamber, water atomization chamber, and pressurizable air and water lines in fluid communication with the barrel. Fast moving air and water create fine water droplets within the water atomization chamber of each barrel. A fine spray or mist of tiny water droplets is emitted from a discharge nozzle of each barrel. Water evaporation systems and methods can be used to efficiently evaporate waster water produced by a wide variety of industrial processes, including waste water produced at oil or gas wells.

Abstract: Described herein are devices and techniques for spray drying a fluid to produce a dried powder. Assemblies include a spray drying head attachable to a gas supplier and a liquid sample, such as a standard unit of blood product. The spray drying head can be adapted to provide an aerosolized flow of liquid sample exposed to a drying gas. The assembly also includes a drying chamber adapted to separate the aerosolized flow of liquid sample into a dried powder and humid air. The assembly can be disposable, provided in a sterilized kit and having simplified attachments allowing quick connect and disconnect from the gas and liquid sample. Separation of the powder from the humid air exiting the drying chamber occurs within a filtered collection bag. In some embodiments, one or more of the drying chamber and collection bag are formed form a thin-walled, collapsible material.

Abstract: An apparatus for generating high temperature steam according to the present invention comprises a high pressure container including a hollow body having a certain volume and sealed shape and a vapor outlet formed at an upper or lower portion of the body for discharging vapor generated therein; a heat supply unit for supplying high temperature heat to the high pressure container; a water supply pump positioned at an outside of the high pressure container and supplying the high pressure container with water from an outside; a spray nozzle for spraying the water supplied from the water supply pump to the high pressure container; and a vapor discharge line connected to the outlet of the high pressure container to guide the vapor generated in the body.

Abstract: A method and an apparatus for monitoring an evaporator (2), whereby a liquid is applied onto a heating unit (3) and evaporated and the temperature drop caused by the evaporation heat in the heating unit (3) is detected. In the absence of a predetermined temperature drop, a signal is generated. In this way, the evaporation process can be controlled in a simple manner.

Abstract: A system for treating feedwater includes a fluidized bed heat exchanger unit connected to receive feedwater and a flash concentrator column connected to receive feedwater discharged from the fluidized bed heat exchanger unit. A spray dryer is provided to receive a solids/liquid slurry discharged from the flash concentrator column. Feedwater can be treated by converting dissolved solids in the feedwater to suspended solids, vaporizing a portion of the feedwater to produce a solids/liquid slurry, and separating solids from the solids/liquid slurry.

Abstract: The present invention relates to a fractionation process for producing at least two concentration fractions of a fluid including a solute, suspended or dissolved content using at least two fluidly connected evaporator units. The process includes the steps of: feeding a feed fluid including a solute, suspended or dissolved content into at least a first evaporator unit; evaporating a first amount of fluid from the feed fluid in at least the first evaporator unit to produce a first concentrated fluid; feeding at least a portion of the first concentrated fluid into at least a second evaporator unit; and evaporating a second amount of fluid from the first concentrated fluid in at least the second evaporator unit to produce a second concentrated fluid.

Abstract: A method of preparing a pharmaceutical composition is described, comprising 1) atomizing a liquid formulation of a therapeutic agent to produce an atomized formulation; 2) freezing said atomized formulation to form solid particles; and 3) drying said solid particles at about atmospheric pressure to produce a powder, wherein said drying is performed in the presence of vibration, internals, mechanical stirring, or a combination thereof. Another method is described, comprising 1) atomizing a liquid formulation of a therapeutic agent to produce an atomized formulation; 2) freezing said atomized formulation to form solid particles; and 3) drying said solid particles to produce a powder; wherein the atomized formulation comprises droplets having an average mean diameter of between about 35? and about 300?, and/or the powder comprises dried particles having an average mean diameter of between about 35? and about 300?. Compositions made by the above methods, and methods of using the compositions, are also described.

Abstract: A devolatilizer apparatus and method for devolatilization of viscous polymer liquids yields polymer products with very low levels of residual volatile components. A stream of liquid polymer is dropped through a first vacuum chamber, thereby removing a portion of the volatile components. The stream is collected at the bottom of the first chamber, and is re-circulated to a manifold and liquid distributor assembly in a second chamber in the same vessel. The stream flows by gravity through the second chamber, which is maintained at a higher level of vacuum than the first chamber. Improved devolatilization is accomplished by exposing the polymer liquid to multiple stages of vacuum in a single vessel. The first chamber may be located generally above the second chamber, but in the same vessel, with the stream falling through the second chamber a first time before re-circulation to the manifold.

Abstract: A floating water evaporation system for use in disposing of excess water from oil and gas drilling operations is provided. One or more nozzle arrays float on the surface of a wastewater pond a distance away from the pond shoreline. Each nozzle array includes a series of upright risers that extend above a water reservoir tank. Spray nozzles are mounted on each riser. The water reservoir tank is mounted between floating pontoons that elevate the nozzles a distance above the surface of the pond. Water from the pond is pumped through the nozzles to create a patterned spray of small evaporable droplets.

Abstract: A fluid evaporation system includes a housing bounding a fluid reservoir and an air flow path that is disposed over top of the fluid reservoir. The housing has an inlet opening and a spaced apart outlet opening that both provide communication between the outside environment and the air flow path. A fan is positioned to draw the air out of the air flow path through the outlet opening. A baffle projects into the air flow path at a location between inlet opening and the outlet opening so as to constrict the area of the air flow path thereat. A plurality of spray nozzles are positioned within air flow path between the baffle and the first end of the housing. A pump is configured to draw fluid from the reservoir and deliver it to the plurality of spray nozzles.

Abstract: A heating system for a spray dryer has a heating element, a heating unit having an open-pore metal foam, and a fluid input and a fluid output. The metal foam is arranged between the fluid input and the fluid output so that fluid which flows in through the fluid input and out through the fluid output is laminarized. A method for simultaneously heating and laminarizing a fluid with the aid of an open-pore metal foam is also disclosed, as is an electrostatic precipitator having a sleeve-shaped electrode connected to a base part of the precipitator. Also disclosed is a device for detaching particles from an inner surface of a sleeve-shaped electrode, a method for detaching particles, and a spray dryer with a heating system as above and/or with an electrostatic precipitator.

Abstract: Improved oil reconditioning systems and methods are disclosed. One preferred system provides an oil purifier for an internal combustion engine for separating contaminants in an oil stream from the oil. The system may include a housing, an oil distributor, and a heating element. The housing may enclose a platen having an evaporation surface. The oil distributor may also be located in the housing and may be configured to receive an incoming oil stream. The oil distributor may have a discharge manifold for transforming the oil stream into a mist. The mist may be directed toward, and distributed over, at least a portion of the evaporation surface. The heating element may be in thermal communication with the platen. The evaporation surface may be heated to a temperature sufficient to volatilize the contaminants, resulting in a purified liquid oil which may be collected and reused with the engine.

Abstract: The invention provides a hydrofluoric acid wastewater treatment method that achieves efficient recovery of hydrofluoric acid from hydrofluoric acid wastewater and also achieves sufficient reduction in the hydrofluoric acid concentration of the dehydrofluorinated water after treatment.

Abstract: A process for the separation of volatile material from particulate polymer which has been substantially freed from unreacted monomer in an earlier separation step, comprising (a) feeding the particulate polymer to a purge vessel, optionally causing it to move through the vessel in substantially plug-flow mode, (b) heating the particulate polymer in the purge vessel to a temperature greater than 30° C. but insufficiently high to cause the particles to become agglomerated, and/or maintaining the polymer at a temperature in this range in the purge vessel, (c) feeding air to the purge vessel counter-current to the movement of the particulate polymer to remove volatile material therefrom, (d) removing the particulate polymer from the purge vessel. Preferably the particulate polymer fed to the purge vessel is caused to move through the vessel in substantially plug-flow mode. The process is particularly suitable for polyethylene.

Abstract: A distillation unit (10) employs a rotary heat exchanger (32) forming a multiplicity of evaporation chambers (56) into which a liquid to be purified is sprayed for evaporation. Spray arms (58) spray at a steady rate into all of the evaporation chambers (56) simultaneously but not at a rate that is adequate to maintain the wetting required for efficient transfer of heat to the liquid. A scanning sprayer (140) supplements this steady spray with spray from nozzles (142 and 144) into only a few of the evaporation chambers at a time, visiting all of them cyclically. The overall rate of spray from the two sources thus combined to spray the chamber cyclically maintains proper wetting even though on average it is lower than the rate that would be required of a constant-rate spray into all of the evaporation chambers.

Abstract: A gas to liquid converter to convert liquids (1) to gas (2) that can include a liquid pressurization element (3), a liquid preheating element (5), and a nozzle (10) to disperse liquids into energy (7) generated by an energy source (8). The gas to liquid converter can be located inside an enclosure (17) and substances dissolved in the liquid can accumulate as solids (13) on deposition surface (12) of the enclosure as the liquid (1) converts to gas (2). Condesation of a portion of the gas (2) generated can be combined with the solids (13) for continuous removal of such solids (13) from the enclosure (17). A gas expansion compensator can generate a pressure gradient (24) to move the volume of gas generated from the liquid from the enclosure (17).

Abstract: An apparatus for removing fluorinated and chlorinated compounds contained in waste gas streams from semiconductor etch and deposition processes. The apparatus has a treatment chamber in which a plurality of liquid films are formed to absorb the fluorinated and chlorinated compounds contained in the waste gas streams that pass through the liquid films. The apparatus includes a tank for receiving the mixture of the absorbed fluorinated and chlorinated compounds and the liquid, and a dehumidifying device for stabilizing and dehumidifying the humidified waste gas streams.

Abstract: A distillation unit (10) employs a rotary heat exchanger (32) forming a multiplicity of evaporation chambers (56) into which a liquid to be purified is sprayed for evaporation. Spray arms (58) spray at a steady rate into all of the evaporation chambers (56) simultaneously but not at a rate that is adequate to maintain the wetting required for efficient transfer of heat to the liquid. A scanning sprayer (140) supplements this steady spray with spray from nozzles (142 and 144) into only a few of the evaporation chambers at a time, visiting all of them cyclically. The overall rate of spray from the two sources thus combined to spray the chamber cyclically maintains proper wetting even though on average it is lower than the rate that would be required of a constant-rate spray into all of the evaporation chambers.

Abstract: Process and apparatus for regenerating spent acid liquor includes a primary roasting furnace for evaporating a substantial portion of the liquid from the spent acid to produce acid vapors and partially roasted metal salts. The partially roasted metal salts are transferred to a secondary roasting chamber where the acids adhering to the surface of the metal salts is vaporized and the metal salts are oxidized. The acid vapors from the primary roasting furnace are then transferred to an absorption column to regenerate the acid. The primary roasting furnace is operated at a different temperature from the secondary roasting chamber and has different retention times for the metal salts. The secondary roasting chamber includes a raking device to mix and convey the metal salts during the secondary roasting step to produce a uniformly roasted metal oxide.

Abstract: A liquid distributor includes a principal container with a perforated bottom, as well as transport members to transmit, by gravity, the liquid from at least one opening in the perforated bottom, to a supply point not in vertical alignment with this opening.

Abstract: A process for extracting salt from brine contained in at least one open evaporation basin. At least part of the brine is heated in a heating unit located outside the evaporation basis and returned to the evaporation basin. The heating unit is driven by waste heat from a recooling industrial plant. According to this process, climatic values and the degree of recooling are measured and evaluated in a control unit. At least part of the heated brine and some non-heated brine are sprayed by a spraying device of the evaporation basin. The amount of sprayed brine is regulated by the control unit depending on the measured data.

Abstract: Spray drying system for drying a liquid feed which is made up of a solution or suspension of particles in a fluid medium. The system enables the spray drying of wet material and converting the material into powder by evaporation of a liquid medium at reduced pressure or at a vacuum. The system includes a heating chamber and an evacuation device, communicating with the interior of the heating chamber. This provision enables creation of reduced pressure within the chamber, accompanied by evaporation of the fluid medium at temperatures lower than needed for evaporation at normal pressure, and evacuation of the moisture vapor generated during evaporation.

Abstract: Process for generating a vacuum and separating the condensable components of the vapors of melt-phase polycondensation in the production of polycarbonate, where at least one or two vapor jets with a downstream spray condenser are connected to the intake side of the polycondensation reactor to be evacuated, and the motive vapor is diphenyl carbonate vapor, and the spray liquid is liquid diphenyl carbonate.

Abstract: A distillation apparatus by flashing and boiling of solution and condensing the resulting steam having a central rotating partitioned brine conduit with coupling to a two-disk centrifugal distributor and a wiping blade system in a chamber having at least one conically shaped wall heated by a condensing steam in a spirally formed conduit, and a surrounding annular spiral condenser. The vertical stacking of such conically shaped evaporators and annular spiral condensers with brine inflow and outflow through a central rotating partitioned tubular conduit make up the desalination tower. The solution flowing through the central tubular conduit to the centrifugal distributor is pressurized by the centrifugal force before flashing through spray nozzles. The flowing liquid film formed on the heated conical surface boils with further enhancement from thinning action due to a rotating wiping pivoting blade system.

Abstract: In the preparation and production of plastic materials by a continuously operating double shaft screw-type extruder, the efficiency of production often depends on good delivery of material to the extruder. In accordance with the invention for processing various types of plastic materials, a primary stage is mounted in a pressure-tight sealed manner on the housing of the extruder, the primary stage being formed by a vertical double conical container in which a pair of screw-type helices are rotatably supported and driven from above. The helices are connected to two replaceable feed elements at their lower ends so that delivery of material to the extruder is achieved without any intermediate dead spaces.

Abstract: The process is used to remove the solvent from an elastomeric polymer solution containing at least 8% by weight of elastomeric polymer. The elastomeric polymer solution undergoes a preprocessing step in order to remove a large part of the solvent. Thereafter, the elastomeric polymer solution is fed into a main extruder in order to remove the remaining solvent. The preprocessing step includes: (a) introducing a heating fluid and the elastomeric polymer solution into a static mixer in order to mix the heating fluid and the elastomeric polymer solution and heat rapidly the elastomeric polymer solution to a temperature of 60.degree.-250.degree. C.

Abstract: A vacuum drying method and wherein a feed liquid is sprayed into a solvent vapor before being introduced into a vacuum chamber for vacuum evaporation, whereby a powder having spherical particles is produced. Moreover, the amount of solvent remaining in the powder obtained is small.

Abstract: An apparatus including an evaporator, a pre-crystallizer, a spray dryer and a fluid bed for drying whey and a rotating disc having a cone-shaped upper surface is provided for receiving partially dried whey from the spray dryer and delivering the whey to the fluid bed while permitting crystallization of the whey as it rests on the surface of the disc.

Abstract: The spray drying process and the apparatus therefor, of the present invention use a spray drying chamber formed by a heat-resistant porous membrane. Said porous membrane enables rapid separation of a discharge gas and a produced powder and accordingly total recovery of the produced powder from the spray drying chamber. Therefore, there occurs no nonuniformity in product composition; cleaning and blowing-off of adhered fine powder can be conducted rapidly and easily even in frequent product change inevitable with a less grade larger quantity production system; as a result, a fine powder of higher quality and higher purity can be produced.

Abstract: An atmospheric evaporator for reducing the water content of various chemical solutions, more particularly useful in the electroplating industry, wherein the evaporator includes a solution-secure molded tank in which a removable blower sleeve is mounted having a blower inlet duct and support strut members formed at the opposite end thereof to support a multiplicity of finned evaporator members over which the solution is sprayed. When a large-volume, low RPM blower is mounted to the inlet duct, a straight-line downdraft of both air and solution is created, allowing the air and evaporated water to exhaust through an up-facing outlet duct, thus defining a substantially "U" shaped duct arrangement from the inlet side to the exhaust side of the tank with the heavy chemical particles returning to the process tank from the bottom of the evaporator tank.

Abstract: A method and apparatus for removing residual water from heavy crude oil comprising a casing, an inlet for admitting liquid crude oil into the casing so as to establish a liquid surface in the casing, an outlet passage for discharging dehydrated liquid crude oil from the casing, a heater in the casing for maintaining the liquid oil at a distillation temperature for evaporating water and light hydrocarbons, a vapor outlet for discharging a mixture of water vapor and light hydrocarbons evaporated from the crude oil, a spray device above the surface of the liquid in the casing for spraying incoming crude oil onto and in heat exchange contact with the surface of the heated oil in the casing, whereby water and light hydrocarbon vapors are distilled from incoming crude oil upon contact with the surface of the heated liquid crude oil.

Abstract: Photographic waste solution is treated by a method which comprises contacting the waste solution with air, in an especially designed treatment vessel, at a solution temperature of from about 120.degree. F. to about 140.degree. F. The air thus becomes supersaturated with the liquid in the waste, and the waste solution is thus concentrated to form a waste slurry which is transferred out into a waste storage vessel. The supersaturated air which is virtually free from waste is discharged to the atmosphere. The method is carried out in an especially constructed apparatus comprising a uniquely designed treatment vessel.

Abstract: The present invention provides a process for the separation of materials obtained by means of high pressure extraction from an extraction agent, wherein extraction agent loaded with extracted material is passed from below into a separator comprising a head (2), a bottom (3), a runback pipe (4) and a heat exchanger (1) in the form of one or more pipes and extract recycled in a forced circulation via the head (2) and the runback pipe (4) to the bottom (3) and there either discharged and/or returned to the heat exchanger (1), the extraction agent evaporated in the heat exchanger being removed via a filter (11) on the head (2).

Abstract: A method and apparatus for converting a long tube vertical evaporator to a falling film evaporator in a manner which permits salvaging most of the long tube vertical evaporator structure. The bottom chamber of the existing evaporator is extended to define a flash chamber intermediate the existing heat exchanger chamber and the bottom chamber. A vapor riser conduit is provided for directing vapor from the flash chamber to the vapor separation chamber positioned above the heat exchanger chamber. A recirculation conduit is provided for directing liquid from the bottom chamber therethrough into a distribution chamber which is provided above and in communication with the upper ends of the heat exchange tubes positioned in the heat exchanger chamber. The distribution chamber is preferably provided with a plurality of spray nozzles which communicate with the recirculation conduit to evenly distribute a film of liquid downwardly through the heat exchange tubes.

Abstract: A method and apparatus for removing residual water from heavy crude oil comprising a casing, an inlet for admitting liquid crude oil into the casing so as to establish a liquid surface in the casing, an outlet passage for discharging dehydrated liquid crude oil from the casing, a heater in the casing for maintaining the liquid oil at a distillation temperature for evaporating water and light hydrocarbons, a vapor outlet for discharging a mixture of water vapor and light hydrocarbons evaporated from the crude oil, a spray device above the surface of the liquid in the casing for spraying incoming crude oil onto and in heat exchange contact with the surface of the heated oil in the casing, whereby water and light hydrocarbon vapors are distilled from incoming crude oil upon contact with the surface of the heated liquid crude oil.