Abstract: A process for producing low alcoholic wine includes the following steps: evaporating alcohol-containing wine in a vacuum evaporator so that a first mixture comprising water, alcohol and flavoring substance is separated from a second mixture having a low-alcoholic content, separating water from said first mixture in a multistage flavor substance apparatus and drawing off a third mixture comprising alcohol and flavoring substance, distilling alcohol from the third mixture, adding the water from the multistage flavor substance apparatus to a mixing vessel in an amount, which together with the low-alcohol second mixture and the flavoring substances produces a quantity of low-alcoholic wine having an alcoholic content below legally determined values for low-alcoholic wine, the process allowing only outputs of low-alcoholic wine, distilled alcohol and flavoring substances and inputs of essentially only the alcohol-containing wine.
Abstract: A portion of the best of vaporization, required to separate and recover methanol from wash water used to remove methanol from a C.sub.4 raffinate resulting from the reaction of isobutene containing C.sub.4 hydrocarbons and methanol to produce MTBE is recovered by conducting the distillation of the methanol/water mixture at a pressure of 40 to 60 psig, thereby increasing the temerature of the methanol overhead to 104.degree. to 114.degree. C. and using the reaction effluent from the MTBE reactor to cool and condense the methanol overhead, said reactor effluent being correspondingly heated prior to entry into a debutanizer tower where unreacted C.sub.4 's and methanol are removed as a raffinate and MTBE product recovered. It is this raffinate that is washed with water to recover the unreacted methanol, with the methanol/water mixture being distilled as set forth above.
Type:
Grant
Filed:
October 28, 1988
Date of Patent:
April 17, 1990
Assignee:
Chemical Research & Licensing Company
Inventors:
Lawrence A. Smith, Jr., Edward M. Jones, Jr., Dennis Hearn
Abstract: An ethanol-producing plant and a method is provided for producing ethanol from sugars, starches, or cellulose. Some ethanol-producing plants consume more thermal energy than they produce. The present invention solves the efficiency problem by utilizing an internal combustion engine with high-efficiency mechanical drives for providing the mechanical power requirements of the ethanol-producing plant and by utilizing the thermal energy of engine coolant and exhaust to provide some, or all, of the thermal energy requirements of the ethanol-producing plant. The method includes electrically loading the internal combustion engine to increase the thermal losses of the engine to equal the thermal energy requirements of the steps of the ethanol-producing process.
Type:
Grant
Filed:
February 2, 1983
Date of Patent:
May 24, 1988
Assignees:
Douglas W. Wills, Linda Wills Maher, Nancy Wills Coffin
Abstract: In a combination solvent extraction-steam distillation process for the recovery of aromatic hydrocarbons, the improvement comprising(a) introducing high pressure steam into a steam ejector;(b) passing the steam from step (a) to a first heat exchanger where it exchanges heat with cooler lean solvent coming from the bottom of the distillation column and is condensed;(c) returning the lean solvent from step (b) to the bottom of the distillation column;(d) passing part of the condensate from step (b) to a second heat exchanger where it exchanges heat with the warmer lean solvent coming from the bottom of the distillation column, cooling the lean solvent and vaporizing the condensate; and(e) passing the vapor from step (d) to the steam ejector in step (a).
Abstract: This invention relates to a solar still wherein the evaporation takes place in partially evacuated tubings which are heated by sunlight. The water to be distilled is supplied from a reservoir vessel which is sealed off after batch loading. The reservoir vessel is elevated above the solar collector. The water is fed into the heater tubings routed through the solar collector by gravity, through an orifice and a heat exchanger-condenser. The steam tubing branches off from the heater tubing in the solar collector vertically, and is routed through the heat exchanger-condenser. At this end, it is connected to a vertical tubing of a sizable length that empties into the distilled water reservoir. The exit end of the heater tubing routed through the solar collector is connected to another vertical tubing of a sizable length that empties into an overflow tank.
Abstract: The present invention provides a process for distillation of styrenes which can be stably operated without loss of energy saving effect, by leading a part or all of low boiling point component vapor from the top to a compressor to use as a heat source for a reboiler and returning the low boiling point components condensed in the reboiler or a mixture of the condensate and a part of the uncondensed vapor to a recycling line of a distillation column.
Abstract: A liquid distillation apparatus provides recirculating flow of unevaporated liquid and recovery of energy from the liquid circulation. Liquid columns in communication with each other are provided differing liquid levels to enhance circulation of the liquid, and to provide efficient operation of the apparatus. Aeration is used to raise the level of the liquid in one of the liquid columns as well as to improve vapor generation for use in a condenser. The two liquid columns are separated from one another except for a connection at the tops and bottoms thereof to permit recirculation of the liquid. The aeration system may be operated by energy recovered from the circulating liquid.
Abstract: An apparatus for generating at least two vapor zones, one above the other, by vaporizing a fluid mixture having at least two compounds therein having different vaporizing temperatures. The apparatus includes a chamber with vaporizing means, and vapor condensing means. Condensate recovery means is provided for recovering the condensed vapor and the condensate recovery means is in flow communication with a separation device for receiving the condensate from the condensate recovery means. The flow communication between the condensate recovery means and the separation device is external of the chamber. The separation means revaporizes the liquid with the lower vaporizing temperature for return to the vapor zone in the upper portion of the chamber and separates as a liquid the fluid having a higher vaporizing temperature.
Abstract: A method of utilizing the energy of a high pressure condensate stream including passing steam at an elevated pressure in indirect heat exchange with a material to be heated, collecting a condensate product condensed from the steam of the heat exchange step at an elevated pressure, passing the condensate directly to a steam stripping step at essentially the same pressure at which the condensate was collected and reducing the pressure of the condensate while simultaneously contacting the condensate with a material to be stripped in the stripping step.
Abstract: A method is disclosed for fractionating a hydrocarbon conversion zone effluent stream comprising at least three components which are to be isolated into separate streams. A two-column system for fractionating the effluent of a benzene alkylation zone is employed. The overhead vapor of a downstream second column is condensed in a side reboiler of a preceding recycle column. This side reboiler is located between the feed point to the recycle column and a separate reboiler located at the bottom of the recycle column. The utilities cost of performing the fractionation is reduced.
Abstract: In a combination alkylation-methyltertiary butyl ether (MTBE) operation, isobutane vapor side-draw and bottoms product yield from the alkylation fractionation, respectively, are used to indirectly heat the mid-section and reboil section of the methyltertiary butyl ether fractionator for heat conservation, beneficiating both the alkylation operation and the MTBE operation.
Abstract: A new process for the production of very pure 4,4'-diisocyanatodiphenylmethane is disclosed, in which diisocyanatodiphenylmethane isomers which are obtained by distillation from the phosgenation products of aniline/formaldehyde condensates are initially freed from 2,2'- and 2,4'-isomers under certain distillation conditions and are then further worked-up by distillation, in that in a first final stage, from 50 to 90%, by weight of the diisocyanate freed from 2,2'- and 2,4'-isomers is isolated as the head product in the form of pure 4,4'-diisocyanatodiphenylmethane and in a second final stage, another quantity of pure 4,4'-diisocyanatodiphenylmethane is separated as the head product from the distillation of the sump of the first final stage.
Type:
Grant
Filed:
October 25, 1982
Date of Patent:
November 8, 1983
Assignee:
Bayer Aktiengesellschaft
Inventors:
Gunther Ellendt, Gunter Gleitsmann, Max Scheidel
Abstract: A liquid purification system, method and apparatus includes a plurality of operationally interconnected chambers. A supply or inlet chamber is held at about atmospheric temperature while other chambers of the system are held at a partial vacuum. The liquid to be purified is metered through a pressure differential between the supply or first chamber and a second chamber to induce spontaneous vaporization of the liquid. The temperatures of the chambers are reduced sufficiently so that, in the case of water, temperature-pressure conditions in the second chamber are below the triple point so as to condense ice and precipitate impurities into another chamber from the spontaneous vaporization. Condensation of the vapor in still another chamber recovers pure liquid. A temperature differential mechanism operatively connected to the chambers insures that condensation of the vapor will occur.
Abstract: A method and apparatus for dehydrating mixtures of organic liquids and water comprising consecutive distillation and membrane permeation, wherein at least a portion of the material retained by the separator is passed into indirect heat exchange relationship within the distillation column and recycled to the separator to provide the heat input required for the permeation process.
Abstract: The invention provides a process and apparatus for reducing the amount of energy which must be supplied to thermally activated separation processes such as fractional distillation, distillation, dehydration, or acid gas scrubbing. The reduction is accomplished by incorporating an absorption heat pump into the process such that the absorption heat pump accepts reject heat from (i.e. provides cooling to) the process and supplies higher temperature heat back to the process. The absorption heat pump causes the necessary temperature increase through the motive power of an external heat source applied to it, in contrast to the mechanical power source required by conventional heat pumps.1.
Abstract: A process and apparatus for the separation of components from a mixture which forms an azeotrope is disclosed by subjecting the mixture to extractive distillation to remove one of the components and regeneration to separate another component from the extracting agent added to the extractive distillation column. According to the invention, a first side stream is withdrawn from the extractive distillation column, passed in heat exchange with the bottoms from the extractive distillation column en route to the regeneration column and returned to the extractive distillation column at a point below the point at which it is withdrawn. A second side stream from the extractive distillation column is withdrawn, passed in heat exchange with the bottoms of the regeneration zone and returned to the extractive distillation column. For this purpose, separate heat exchangers are used for the respective side streams.
Abstract: Apparatus usable to heat fluid comprises:(a) a steam vessel having an inlet for water and an outlet for steam,(b) heating means associated with the vessel to heat water received therein and produce steam, and(c) a condenser connected with the vessel outlet to receive steam, the condenser adapted to extend in heat transfer relation with the fluid to heat that fluid in response to condensation of steam in said condenser, the condenser having a condensate outlet, and(d) other means to remove solid particles from the vessel.
Abstract: Reconcentration of moist glycol, which has been used to dry natural gas, by heating the moist glycol with flue gas from a reboiler and by thereafter stripping water from the moist glycol with the dried flue gas or with a hydrocarbon gas by-product of the natural gas being dried.
Abstract: Reconcentration of moist glycol, which has been used to dry natural gas, by heating the moist glycol with flue gas from a reboiler and by thereafter stripping water from the moist glycol with the dried flue gas or with a hydrocarbon gas by-product of the natural gas being dried.
Abstract: Method and apparatus for desalinizing water. Salt water in an evaporation zone is provided with heat of vaporization by a heat pump which transfers heat to the water from a thermal sink. The evaporation zone is maintained at subatmospheric pressure so that the salt water boils at a temperature at least about 10 degrees above the ambient dew point. The pressure in the evaporation zone is maintained at a low level by a vacuum pump and by condensing the vapor in a condensation zone from which fresh water is collected. The heat of condensation is dissipated into a "cold" sink if available or by a heat dissipating means such as an evaporative cooling apparatus. Energy efficiency results from the ability of the heat pump or pumps in the system to operate at a high coefficient of performance.
Abstract: A water purification system for use in combination with a domestic hot water heating tank. The system includes a water container for containing water separate from the water in the tank. A conduit carries hot water from the tank to the container, passing in close proximity to the heating unit of the hot water tank. A duct leading from the container conveys water vapor formed in the container to a receptacle. The water in the receptacle having been evaporated and condensed is thus purified for domestic use.