Particular Or Specific Manner Of Positioning, Arranging, Or Conveying Of Plural Articles Or Plural Preforms (e.g., Stacking, Utilizing Spacer, Etc.) During Sintering, Vitrifying, Or Drying Patents (Class 264/605)
  • Patent number: 11174360
    Abstract: The present application relates to a block copolymer and a use thereof. The present application can provide a laminate which is capable of forming a highly aligned block copolymer on a substrate and thus can be effectively applied to production of various patterned substrates, and a method for producing a patterned substrate using the same.
    Type: Grant
    Filed: November 29, 2017
    Date of Patent: November 16, 2021
    Inventors: Mi Sook Lee, Se Jin Ku, No Jin Park, Jung Keun Kim, Je Gwon Lee, Hyung Ju Ryu, Eun Young Choi
  • Patent number: 10422581
    Abstract: Setter plates are fabricated from Li-stuffed garnet materials having the same, or substantially similar, compositions as a garnet Li-stuffed solid electrolyte. The Li-stuffed garnet setter plates, set forth herein, reduce the evaporation of Li during a sintering treatment step and/or reduce the loss of Li caused by diffusion out of the sintering electrolyte. Li-stuffed garnet setter plates, set forth herein, maintain compositional control over the solid electrolyte during sintering when, upon heating, lithium is prone to diffuse out of the solid electrolyte.
    Type: Grant
    Filed: October 26, 2017
    Date of Patent: September 24, 2019
    Assignee: QuantumScape Corporation
    Inventors: Sriram Iyer, Tim Holme, Niall Donnelly
  • Patent number: 10365042
    Abstract: A tray is provided for conveying a workpiece placed on the tray inside a heat treatment furnace. The tray includes plural kinds of positional displacement regulating parts for respectively regulating horizontal positional displacements of plural kinds of workpieces with different sizes, wherein the plural kinds of positional displacement regulating parts are arranged concentrically in a plane shape.
    Type: Grant
    Filed: February 14, 2017
    Date of Patent: July 30, 2019
    Assignee: MITSUI HIGH-TEC, INC.
    Inventors: Takeaki Kozono, Yusuke Hasuo
  • Patent number: 9970711
    Abstract: Setter plates are fabricated from Li-stuffed garnet materials having the same, or substantially similar, compositions as a garnet Li-stuffed solid electrolyte. The Li-stuffed garnet setter plates, set forth herein, reduce the evaporation of Li during a sintering treatment step and/or reduce the loss of Li caused by diffusion out of the sintering electrolyte. Li-stuffed garnet setter plates, set forth herein, maintain compositional control over the solid electrolyte during sintering when, upon heating, lithium is prone, to diffuse out of the solid electrolyte.
    Type: Grant
    Filed: October 5, 2016
    Date of Patent: May 15, 2018
    Assignee: QuantumScape Corporation
    Inventors: Sriram Iyer, Tim Holme, Niall Donnelly
  • Patent number: 9624136
    Abstract: A transparent, tape casted, spinel article, as defined herein. Also disclosed is a method of method of making the tape casted, transparent spinel, and laminates of the tape casted. transparent spinel, as defined herein.
    Type: Grant
    Filed: June 11, 2015
    Date of Patent: April 18, 2017
    Assignee: Corning Incorporated
    Inventors: Michael Edward Badding, Weiguo Miao, Nathan Michael Zink
  • Patent number: 9393590
    Abstract: Small structures are formed by applying to a substrate a structural material and a layer of a sacrificial material having a lower surface energy than the structural material, to form an intermediate product. The substrate is then heated to a temperature at which the sacrificial material evaporates or sublimes and the structural material is mobilized. The sacrificial material is permitted to evaporate or sublime, an area of the substrate covered by the sacrificial material to diminish, and the structural material to agglomerate on the remaining sacrificial material to form a structure.
    Type: Grant
    Filed: April 15, 2013
    Date of Patent: July 19, 2016
    Assignee: TEMPLE UNIVERSITY—OF THE COMMONWEALTH SYSTEM OF HIGHER EDUCATION
    Inventors: Svetlana Neretina, Robert Alan Hughes, Pouyan Farzinpour
  • Patent number: 8974721
    Abstract: A method of making ceramic bodies includes systematically orienting the bodies during firing relative to a temperature gradient in a kiln. The systematic orientation of the bodies relative to the temperature gradient can allow for an average deviation of a measured shape of the ceramic bodies from a predetermined target contour shape to be less than what they would be if the bodies were oriented randomly relative to the temperature gradient.
    Type: Grant
    Filed: August 1, 2012
    Date of Patent: March 10, 2015
    Assignee: Corning Incorporated
    Inventors: Daniel Edward McCauley, Anthony Nicholas Rodbourn, David Robertson Treacy, Jr., Casey Allen Volino
  • Patent number: 8932502
    Abstract: Methods and apparatuses disclosed herein relate to a recyclable thermoplastic unit that includes a casing body composed of a first thermoplastic having a first melting point. The casing body also includes a first locking mechanism that is configured to mate with a second locking mechanism of a sacrifice layer. The sacrifice layer is composed of a second thermoplastic and includes the second locking mechanism. The sacrifice layer has a melting point that is greater than the melting point of the casing body.
    Type: Grant
    Filed: February 16, 2011
    Date of Patent: January 13, 2015
    Assignee: Empire Technology Development LLC
    Inventor: Aya Seike
  • Publication number: 20140361470
    Abstract: When a multilayer ceramic substrate with a cavity is reduced in thickness, a bottom wall portion defining the bottom of the cavity is reduced in thickness, thereby leading to the problem that the bottom wall portion is likely to be broken. A bottom wall portion defining a cavity of a multilayer ceramic substrate has a stack structure formed with a high thermal expansion coefficient layer sandwiched between first and second low thermal expansion coefficient layers. This configuration generates compression stress in the low thermal expansion coefficient layers during a cooling process after firing, thereby allowing the mechanical strength at the bottom wall portion to be improved.
    Type: Application
    Filed: August 22, 2014
    Publication date: December 11, 2014
    Inventor: Yuichi IIDA
  • Publication number: 20140328747
    Abstract: Provided is a zinc oxide sputtering target, which can effectively suppress the occurrence of break or crack in the target during sputtering to enable production of a zinc oxide transparent conductive film with high productivity. The zinc oxide sputtering target is composed of a zinc oxide sintered body comprising zinc oxide crystal grains, wherein the zinc oxide sputtering target has a sputter surface having a (100) crystal orientation degree of 50% or more.
    Type: Application
    Filed: June 16, 2014
    Publication date: November 6, 2014
    Inventors: Jun YOSHIKAWA, Katsuhiro IMAI, Koichi KONDO
  • Patent number: 8821661
    Abstract: A method of manufacturing a honeycomb structure including a honeycomb unit includes forming a honeycomb molded body having a plurality of cells extending from a first end face to a second end face of the honeycomb molded body along a longitudinal direction of the honeycomb molded body and separated by a plurality of cell walls, placing the honeycomb molded body in a degreasing apparatus so that the first end face faces downward and the second end face faces upward, feeding introduced gas into the degreasing apparatus, degreasing the honeycomb molded body at a temperature of approximately 200° C. to approximately 400° C., and firing the degreased honeycomb molded body at a temperature of approximately 500° C. to approximately 900° C. to obtain the honeycomb unit.
    Type: Grant
    Filed: October 21, 2011
    Date of Patent: September 2, 2014
    Assignee: Ibiden Co., Ltd.
    Inventors: Yuji Haga, Yusuke Fujii, Tadafumi Ohashi
  • Publication number: 20140131926
    Abstract: Methods of firing ware in a furnace. At least one stack of ware is positioned in a ware space of a furnace. The stack of ware comprises a plurality of ware articles arranged such that at least laterally adjacent ware articles are spaced apart. The at least one stack of ware is heated in the ware space of the furnace. At least one gas is introduced into the ware space on a first side of the at least one stack of ware as the stack is heated. A flow condition of the at least one gas is adjusted to create a pressure differential within the furnace across at least a portion of the ware space such that at least some of the at least one gas flows through the at least one stack of ware.
    Type: Application
    Filed: November 13, 2012
    Publication date: May 15, 2014
    Applicant: CORNING INCORPORATED
    Inventors: Bernd Geismar, Thomas Madison Tebo, III, Christopher Steven Witte
  • Patent number: 8652378
    Abstract: The present invention relates to rapid dissolve thin film drug delivery compositions for the oral administration of active components. The active components are provided as taste-masked or controlled-release coated particles uniformly distributed throughout the film composition. The compositions may be formed by wet casting methods, where the film is cast and controllably dried, or alternatively by an extrusion method.
    Type: Grant
    Filed: March 29, 2013
    Date of Patent: February 18, 2014
    Assignee: MonoSol Rx LLC
    Inventors: Robert K. Yang, Richard C. Fuisz, Garry L. Myers, Joseph M. Fuisz
  • Publication number: 20130288875
    Abstract: A method and apparatus for sintering flat ceramics using a mesh or lattice is described herein.
    Type: Application
    Filed: March 15, 2013
    Publication date: October 31, 2013
    Inventors: Hiroaki Miyagawa, Guang Pan, Hironaka Fujii, Bin Zhang, Amane Mochizuki, Toshitaka Nakamura
  • Patent number: 8407915
    Abstract: Tray assemblies and methods for manufacturing ceramic articles are provided. In one embodiment, a tray assembly includes a tray body having a supporting surface operable to support a ceramic article for passage through a microwave drying apparatus during a microwave drying process and a microwave coupling cover associated with the tray body. The microwave coupling cover envelopes at least a portion of the ceramic article during the microwave drying process. The microwave coupling cover has a dielectric property such that a greater percentage of microwave energy is coupled into the ceramic article with the microwave coupling cover present during the microwave drying process than with the microwave coupling cover not present. Methods may include rotating the ceramic article when the ceramic article is about 40%-60 dry.
    Type: Grant
    Filed: February 22, 2011
    Date of Patent: April 2, 2013
    Assignee: Corning Incorporated
    Inventors: Jacob George, James Anthony Feldman, Nadezhda P Paramonova, Michael Dean Seymour
  • Publication number: 20120121880
    Abstract: Provided is a long and large-area graphite film having improved thermal diffusivity and flex resistance, and accompanied by ameliorated ruffling. According to a method for producing a graphite film, in which graphitization of a heat-treated film consisting of a carbonized polymer film is carried out in a state being wrapped around an internal core, the method being characterized in that a heat treatment is executed by controlling distance(s) between the internal core and the film, and/or between the layers of the film, a graphite film accompanied by significantly ameliorated ruffling can be obtained.
    Type: Application
    Filed: June 22, 2009
    Publication date: May 17, 2012
    Inventors: Yusuke Ohta, Makoto Mishiro, Takashi Inada, Yasushi Nishikawa
  • Publication number: 20120113562
    Abstract: A dielectric composition having a high dielectric constant, multi layered ceramic condensers comprising the same, and a method of preparing for multi layered ceramic condensers. The dielectric composition includes: a compound represented by general formula (Ba1-XCax)m(Ti1-yZry)O3 (0.995?m?1.010, 0.001?x?0.10, 0.001, 0.001?y?0.20) as a main component; an Al oxide as a first sub-component; at least one metal selected from a group consisting of Mg, Sr, Ba, Ca, and Zr and the salt thereof, as a second sub-component; at least one metal selected from a group consisting of Sc, Y, La, Ac, Ce, Pr, Nd, Pm, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, and Lu and the salt thereof, as a third sub-component; at least one metal selected from a group consisting of Cr, Mo, W, Mn, Fe, Co, and Ni and the salt thereof, as a fourth sub-component; and a fifth sub-component selected from Si containing glass forming compounds.
    Type: Application
    Filed: November 1, 2011
    Publication date: May 10, 2012
    Inventors: Sung Hyung KANG, Min Sung Song, Du Won Choi, Sang Hoon Kwon, Chang Hoon Kim, Kang Heon Hur
  • Publication number: 20120068389
    Abstract: Provided is a method of fabricating polycrystalline ceramic for thermoelectric devices. The method includes preparing calcined ceramic powders, forming a ceramic sheet by uni-axially pressing the calcined ceramic powders, stacking a plurality of the ceramic sheets in a uni-axial direction, and cofiring the stacked the plurality of the ceramic sheets.
    Type: Application
    Filed: March 11, 2011
    Publication date: March 22, 2012
    Inventors: Chan Park, Wook Jo, Jin-Sang Kim, O-Jong Kwon
  • Publication number: 20120056359
    Abstract: Method and apparatus for preparing of at least one ceramic shaped part. A cavity is provided between at least one external shape and at least one internal shape. A Si-containing powder composition is then provided in the cavity. The composition is then heated in a reactive gas atmosphere to obtain a reaction bounded ceramic shaped part. Use of the apparatus is also described.
    Type: Application
    Filed: April 23, 2010
    Publication date: March 8, 2012
    Inventors: Håvard Sørheim, Arve Solheim
  • Patent number: 8105557
    Abstract: A microreactor assembly [100] is provided comprising a fluidic interconnect backbone [10] and plurality of fluidic microstructures. Interconnect input/output ports [12] of the fluidic interconnect backbone [10] are interfaced with microchannel input/output ports [14] of the fluidic microstructures at a plurality of non-polymeric interconnect seals [50]. Interconnect microchannels [15] are defined entirely by the fluidic interconnect backbone [10] and extend between the non-polymeric interconnect seals [50] without interruption by additional sealed interfaces. At least one of the fluidic microstructures [20, 30, 40] may comprise a mixing microstructure formed by a molding process. Another of the fluidic microstructures [20, 30, 40] may comprise an extruded reactor body. Still another fluidic microstructure [20, 30, 40] may comprise a quench-flow or hydrolysis microreactor formed by a hot-pressing method.
    Type: Grant
    Filed: January 28, 2009
    Date of Patent: January 31, 2012
    Assignee: Corning Incorporated
    Inventors: Jean-Pierre Henri Rene Lereboullet, Olivier Lobet, Yann P M Nedelec, Ronan Tanguy
  • Publication number: 20110177266
    Abstract: A firing aid, in particular for supporting material to be fired in a furnace during filing, is obtainable by a method including the following steps: a) providing a mixture of at least 60% by weight mullite powder which comprises 74.0 to 78.0% by weight Al2O3, 22.0 to 26% by weight SiO2 and a maximum of 0.5% contaminants, with the sum of the Al2O3 content and of the SiO2 content amounting to at least 99.5% by weight; 1 to 20% by weight binder; 0 to 20% by weight plasticizer; and remainder to 100% by weight of one or more additives; b) pressing the mixture provided in step a) to a green body; and c) sintering the green body.
    Type: Application
    Filed: November 10, 2010
    Publication date: July 21, 2011
    Applicant: Dekema Dental-Keramikofen GmbH
    Inventor: Stephan Miller
  • Patent number: 7947214
    Abstract: This process is a fused glass powder process for making ceramic billets for semiconductor dopants. The powder process uses a unique combination of steps for packing, compacting and heat treating the powders. The resulting billets may be tailored in composition to provide a variety of densities, rigidities and B2O3 evolution rates. Further, the resulting wafers have a large diameter to meet the needs of semiconductor production.
    Type: Grant
    Filed: October 19, 2005
    Date of Patent: May 24, 2011
    Inventor: Jame E. Rapp
  • Publication number: 20110114530
    Abstract: The present invention provides a method for producing a silica container, wherein the method comprises: a step of forming a preliminarily molded substrate, wherein a first powdered raw material (silica particles) is fed to an inner wall of an outer frame having aspiration holes while rotating the outer frame, a step of forming a preliminarily molded intermediate layer, wherein a second powdered raw material (silica particles) added with an aluminum compound or a crystal nucleating agent as an additive is fed to an inner wall of the preliminarily molded substrate, and a step of forming an inner layer, wherein the preliminarily molded substrate and the preliminarily molded intermediate layer are degassed by aspiration from a peripheral side with heating from an inside thereby forming a substrate and an intermediate layer, and while a third powdered raw material having a high silica purity is spread from inside the substrate having the formed intermediate layer with heating from the inside thereby forming an inn
    Type: Application
    Filed: March 24, 2010
    Publication date: May 19, 2011
    Applicant: SHIN-ETSU QUARTZ PRODUCTS CO., LTD.
    Inventors: Shigeru Yamagata, Tomomi Usui
  • Patent number: 7842227
    Abstract: A drying jig of the present invention is a drying jig for a pillar-shaped honeycomb molded body having a large number of cells longitudinally placed in parallel with one another with a cell wall therebetween, comprising: a fixing member for preventing separation or opening of the drying jig; and a piling member which enables the drying jig to be piled up in multi stage at the time of drying.
    Type: Grant
    Filed: February 27, 2007
    Date of Patent: November 30, 2010
    Assignee: Ibiden Co., Ltd.
    Inventors: Kenichiro Kasai, Kazuya Naruse
  • Publication number: 20100210444
    Abstract: A method of sintering large refractory ceramic articles is disclosed. The method includes supporting a green refractory body on a plurality of support plates, the support plates in turn being supported by a plurality of support members having arcuate upper and lower surfaces. A setter material is disposed between the green refractory body to be sintered and the support plates. As the refractory body is sintered, the density of the article increases. Concurrently, the dimensions of the body decrease, which shrinkage, unless otherwise accommodated, may cause fracture of the body. The support plates and the structure of the support members, move to prevent the development of detrimental stresses in the refractory body as it sinters.
    Type: Application
    Filed: February 12, 2010
    Publication date: August 19, 2010
    Inventor: Randy L. Rhoads
  • Patent number: 7708933
    Abstract: A drying jig circulating apparatus includes a drying jig assembling apparatus for assembling a drying jig on a movable table, a drying apparatus for drying a ceramic molded body held by the drying jig, and a drying jig disassembling apparatus for disassembling the drying jig on a movable table, and a drying jig circulating conveyor for transporting the drying jig from the disassembling apparatus to the assembling apparatus. The drying jig is configured by two or more separate jigs with a fixing member that integrates the separate jigs, or formed by one openable jig with a fixing member for maintaining a closed state. The drying jig assembling apparatus further includes a molded body mounting mechanism, a ceramic molded body holding mechanism, and a jig delivering mechanism. The drying jig disassembling apparatus further includes a jig receiving mechanism, a jig releasing mechanism, and a molded body taking-out mechanism.
    Type: Grant
    Filed: October 30, 2007
    Date of Patent: May 4, 2010
    Assignee: Ibiden Co., Ltd.
    Inventors: Kenichiro Kasai, Kazuya Naruse
  • Publication number: 20100098573
    Abstract: The present disclosure relates to the sintering cycle method and apparatus of a kind of box-type sintering machine, which is peculiarly applicable to the production of lightweight aggregate using fly ash or industrial waste by sintering process. This apparatus includes four conveying systems, ignition station #1, ignition station #2, one tilt discharger, and one crusher; the box-type sintering stacking line A and B are straight and parallel, sharing one coarse dust collector; each box-type sintering stacking line is equipped with overhead workstation gantry crane rails and cranes, and each crane comprises two parts, i.e., hoist system and single rail trolley system; each box-type sintering stacking line has multiple sinter boxes; each sinter box has an air chamber below, under which there is the air chamber pipeline connected to the coarse dust collector.
    Type: Application
    Filed: October 16, 2009
    Publication date: April 22, 2010
    Applicant: Beijing STICH Science and Technology Company Ltd.
    Inventor: Zhengfu Fan
  • Patent number: 7687013
    Abstract: A circulating apparatus includes a firing jig assembling apparatus, a firing furnace, a firing jig disassembling apparatus, and a transporting conveyor. The firing jig assembling apparatus includes a lid member attaching mechanism that attaches the lid member to a predetermined position of the firing jig placed on the table or the conveyor; and a jig delivering mechanism that delivers the firing jig which has the ceramic molded body being mounted thereon and the lid member being attached thereto, to the firing furnace. The firing jig disassembling apparatus further includes a jig receiving mechanism that receives the firing jig which has the fired ceramic molded body being mounted thereon and the lid member being attached thereto, from the firing furnace; and a lid member detaching mechanism that detaches the lid member from the firing jig placed on the table or the conveyor with the lid member being attached thereto.
    Type: Grant
    Filed: October 29, 2007
    Date of Patent: March 30, 2010
    Assignee: Ibiden Co., Ltd.
    Inventors: Tsuyoshi Kawai, Takamitsu Saijo, Kenichiro Kasai
  • Publication number: 20100074729
    Abstract: A stack of substantially parallel ceramic plates (22) separated and interconnected by ceramic spacers (26, 27) forming a seal structure (20) with a length (L), a width (W), and a thickness (T). The spacers are narrower in width than the plates, and may be laterally offset from spacers in adjacent rows to form a space (28) in a row that aligns with a spacer in another adjacent row. An adjacent plate bends into the space when the seal structure is compressed in thickness. The spacers may have gaps (60, 62) forming a stepped or labyrinthine cooling flow path (66) within the seal structure. The spacers of each row may vary in lateral separation, thus providing a range of compressibility that varies along the width of the seal structure.
    Type: Application
    Filed: February 6, 2009
    Publication date: March 25, 2010
    Applicant: SIEMENS ENERGY, INC.
    Inventors: Gary B. Merrill, Jay A. Morrison
  • Publication number: 20100062396
    Abstract: A method for manufacturing a multipart assembly of sintered oxide ceramic material, including one first component which at least partially surrounds one second component in such a manner that detaching the first component from the second component is not possible without destroying the first and/or second component. The assembly is produced by producing a single-part first shaped part and a single-part second shaped part from an oxide ceramic blank, whereby the first shaped part and the second shaped part are enlarged to compensate for the shrinkage during sintering, and assembling the sintered shaped part as second component with the first shaped part and subsequently sintering them together.
    Type: Application
    Filed: December 21, 2007
    Publication date: March 11, 2010
    Applicant: DEGUDENT GMBH
    Inventors: Elmar Hock, Stefan Fecher, Lothar Volkl
  • Patent number: 7632452
    Abstract: A degreasing furnace loading apparatus including a molded body moving mechanism configured to move a plurality of ceramic molded bodies simultaneously, and a transporting table configured to transport a degreasing jig for mounting the ceramic molded bodies thereon to a degreasing furnace. The molded body moving mechanism is configured to simultaneously place the plurality of ceramic molded bodies on the degreasing jig, such that each of the ceramic molded bodies is placed to have predetermined intervals therebetween.
    Type: Grant
    Filed: November 14, 2007
    Date of Patent: December 15, 2009
    Assignee: Ibiden Co., Ltd.
    Inventors: Takamitsu Saijo, Kenichiro Kasai
  • Patent number: 7597838
    Abstract: A ceramic matrix composite with a ceramic matrix and a gradient layering of coating on ceramic fibers. The coating typically improves the performance of the composite in one direction while degrading it in another direction. For a SiC-SiC ceramic matrix composite, a BN coating is layered in a gradient fashion or in a step-wise fashion in different regions of the article comprising the ceramic. The BN coating thickness is applied over the ceramic fibers to produce varying desired physical properties by varying the coating thickness within differing regions of the composite, thereby tailoring the strength of the composite in the different regions. The coating may be applied as a single layer as a multi-layer coating to enhance the performance of the coating as the ceramic matrix is formed or infiltrated from precursor materials into a preform of the ceramic fibers.
    Type: Grant
    Filed: December 30, 2004
    Date of Patent: October 6, 2009
    Assignee: General Electric Company
    Inventors: Suresh Subramanian, James Dale Steibel, Douglas Melton Carper, Toby George Darkins, Jr.
  • Publication number: 20090243163
    Abstract: A method for making a composite magnetic-dielectric disc assembly includes forming a dielectric ceramic cylinder, forming a magnetic ceramic rod, assembling the magnetic ceramic rod coaxially inside the dielectric ceramic cylinder to form a rod-and-cylinder assembly, kilning (firing) the rod-and-cylinder assembly, slicing the rod-and-cylinder assembly to form a plurality of composite magnetic-dielectric disc-shaped assemblies. The magnetic-dielectric disc assemblies can be used in manufacturing, for example, circulators, isolators or similar electronic components. Accordingly, the method for making the disc assemblies can be included as part of a method for making such electronic components.
    Type: Application
    Filed: March 26, 2008
    Publication date: October 1, 2009
    Applicant: SKYWORKS SOLUTIONS, INC.
    Inventors: Jingmin Zheng, David B. Cruickshank, David M. Firor
  • Patent number: 7595019
    Abstract: Method of making an electrochemical device for the recovery of oxygen from an oxygen-containing feed gas comprising (a) preparing a green electrochemical device by assembling a green electrolyte layer, a green anode layer in contact with the green electrolyte layer, a green cathode layer in contact with the green electrolyte layer, a green anode-side gas collection interconnect layer in contact with the green anode layer, and a green cathode-side feed gas distribution interconnect layer in contact with the green cathode layer; and (b) sintering-the green electrochemical device by heating to yield a sintered electrochemical device comprising a plurality of sintered layers including a sintered anode-side gas collection interconnect layer in contact with the anode layer and adapted to collect oxygen permeate gas, wherein each sintered layer is bonded to an adjacent sintered layer during sintering.
    Type: Grant
    Filed: March 1, 2005
    Date of Patent: September 29, 2009
    Assignee: Air Products and Chemicals, Inc.
    Inventors: Raymond Ashton Cutler, Kent Neal Hutchings, Merrill Anderson Wilson, Ronald Almy Hollis, Dale M. Taylor
  • Publication number: 20090239434
    Abstract: A method of producing a fiber-reinforced carbide-ceramic component includes producing a carbonaceous article from at least one unidirectional tape by pyrolysis, infiltrating the carbonaceous article with carbide former, and coating the at least one unidirectional tape with a coating material being volatile in pyrolysis and/or providing the at least one unidirectional tape with a transverse thread system including transverse threads composed of a material being volatile in pyrolysis. A fiber-reinforced carbide ceramic component is also provided.
    Type: Application
    Filed: June 5, 2009
    Publication date: September 24, 2009
    Applicants: SGL CARBON AG, DEUTSCHES ZENTRUM FUR LUFT- UND RAUMFAHRT E. V.
    Inventors: Bodo Benitsch, Bernhard Heidenreich, Christian Zuber
  • Publication number: 20090191102
    Abstract: A microreactor assembly [100] is provided comprising a fluidic interconnect backbone [10] and plurality of fluidic microstructures. Interconnect input/output ports [12] of the fluidic interconnect backbone [10] are interfaced with microchannel input/output ports [14] of the fluidic microstructures at a plurality of non-polymeric interconnect seals [50]. Interconnect microchannels [15] are defined entirely by the fluidic interconnect backbone [10] and extend between the non-polymeric interconnect seals [50] without interruption by additional sealed interfaces. At least one of the fluidic microstractures [20, 30, 40] may comprise a mixing microstructure formed by a molding process. Another of the fluidic microstructures [20, 30, 40] may comprise an extruded reactor body. Still another fluidic microstructure [20, 30, 40] may comprise a quench-flow or hydrolysis microreactor formed by a hot-pressing method.
    Type: Application
    Filed: January 28, 2009
    Publication date: July 30, 2009
    Inventors: Jean-Pierre Henri Rene Lereboullet, Olivier Lobet, Yann P. M. Nedelec, Ronan Tanguy
  • Patent number: 7547370
    Abstract: A method for manufacturing a multilayer ceramic electronic element includes the steps of forming ceramic green sheets having superior surface smoothness and small variations in thickness at a high speed, in which defects such as pinholes are prevented from occurring, and providing internal electrodes and step-smoothing ceramic paste on the ceramic green sheets with high accuracy. The method includes the steps of applying ceramic slurry to a base film by a die coater followed by drying performed in a drying furnace for forming the ceramic green sheets, and performing gravure printing of conductive paste and ceramic paste onto the ceramic green sheets by using a first and a second gravure printing apparatus, respectively. Accordingly, the internal electrodes are formed, and the step-smoothing ceramic paste is provided in regions other than those in which the internal electrodes are formed.
    Type: Grant
    Filed: December 15, 2006
    Date of Patent: June 16, 2009
    Assignee: Murata Manufacturing Co., Ltd.
    Inventors: Shingo Okuyama, Hiroyoshi Takashima, Akira Hashimoto, Shinichi Kokawa
  • Publication number: 20090108507
    Abstract: The disclosed invention relates to a method of manufacture of transparent ceramics such as yttrium aluminum garnet by tape casting. The method entails forming a mixture of ceramic oxide, dispersant and organic solvent, milling the mixture to produce a first slurry, mixing the first slurry with an organic binder and a plasticizer to form a treated slurry, milling the treated slurry to produce milled slurry, tape casting the milled slurry to produce cast tape, drying the cast tape to produce dried tape, stacking portions of dried tape to form an assembly, compressing the assembly to produce a preform, heating the preform to produce a green preform, and sintering the green preform to produce transparent yttrium aluminum garnet. The method may be used to produce a unitary ceramic product having differing transparent sections as well as transparent ceramic product having a dopant gradient across a portion of the thickness of the product.
    Type: Application
    Filed: September 11, 2008
    Publication date: April 30, 2009
    Applicant: The Penn State Research Foundation
    Inventors: Gary L. Messing, Elizabeth R. Kupp, Sang-Ho Lee, Garnia Y. Juwondo, Adam J. Stevenson
  • Publication number: 20090071379
    Abstract: A process for treating fly ash to render it highly usable as a concrete additive. A quantity of fly ash is obtained that contains carbon and which is considered unusable fly ash for concrete based upon foam index testing. The fly ash is mixed with a quantity of spray dryer ash (SDA) and water to initiate a geopolymerization reaction and form a geopolymerized fly ash. The geopolymerized fly ash is granulated. The geopolymerized fly ash is considered usable fly ash for concrete according to foam index testing. The geopolymerized fly ash may have a foam index less than 40%, and in some cases less than 20%, of the foam index of the untreated fly ash. An optional alkaline activator may be mixed with the fly ash and SDA to facilitate the geopolymerization reaction. The alkaline activator may contain an alkali metal hydroxide, carbonate, silicate, aluminate, or mixtures thereof.
    Type: Application
    Filed: November 21, 2008
    Publication date: March 19, 2009
    Inventor: Chett Boxley
  • Publication number: 20090020924
    Abstract: Methods, apparatus, and systems of fabricating ordered or hierarchically ordered small-scale structures (e.g. micro- or sub-micro size) without the need for lithographic techniques or external fields. The methods use irreversible solvent evaporation to deposit the solute on a surface. A spherical lens is brought down into contact with the droplet. By selection and control of one or more relevant parameters, various characteristics or features of the resulting structures can be controlled. Nano-scale structures or materials can be formed or included in the micro- or sub-micro-scale formed structures. The nano-scale structures or materials can self-assembly in hierarchical order by selection and control of certain process parameters.
    Type: Application
    Filed: February 21, 2008
    Publication date: January 22, 2009
    Applicant: IOWA STATE UNIVERSITY RESEARCH FOUNDATION, INC.
    Inventor: Zhiqun Lin
  • Patent number: 7476356
    Abstract: Firing of ceramic cores (1) is important in order to achieve manufacturing processes. These ceramic cores (1) are generally formed in a “green” state which has limited mechanical strength and may be distorted during the firing process by non-uniform thermal effects, etc. By providing a tube or containment 2 which is located on a saggar base 3 and surrounded by firing media 4, it is possible to achieve an initial pre-firing step whereby the “green” state core 1 is located through a stem 1a in an initial partial depth 5 of firing media 4 in the tube or containment 2 until it achieves a sufficient mechanical strength to enable positional adjustment. Thus, the green core will be pre-fired in a kiln solely supported through the stem 1a and then the core adjusted using a tool such as an engineering rule.
    Type: Grant
    Filed: March 6, 2006
    Date of Patent: January 13, 2009
    Assignee: Rolls-Royce plc
    Inventors: Jamie C McGourlay, Bhupendra A Prajapati
  • Publication number: 20080251976
    Abstract: A spacer for forming a gap in a device includes a predetermined geometric shape and is less than about 500 micrometers in a broadest dimension. A plurality of spacers can be fabricated where each spacer of the plurality of spacers has a predetermined geometric shape, the same predetermined geometric shape, or a variety of predetermined geometric shapes. The spacers of the plurality of spacers can also include a polydispersity of about 1.0005. The spacer can be positioned between two components of a device to provide accurate spacing of the components.
    Type: Application
    Filed: April 13, 2007
    Publication date: October 16, 2008
    Inventors: Jason P. Rolland, Ginger D. Rothrock
  • Publication number: 20080174054
    Abstract: A wafer chuck for use in a lithographic apparatus, which includes a low-thermal expansion glass ceramic substrate, a silicon silicon carbide layer, and a bonding layer comprising silicate having a strength of at least about 5 megapascals, the bonding layer attaching the silicon silicon carbide layer to the substrate is described. Also, a method of forming a wafer chuck for use in a lithographic apparatus, which includes coating a portion of one or both of a low-thermal expansion glass ceramic substrate and a silicon silicon carbide layer with a bonding solution, and contacting the substrate and the silicon silicon carbide layer to bond the substrate and the silicon silicon carbide layer together is described.
    Type: Application
    Filed: January 24, 2007
    Publication date: July 24, 2008
    Applicant: ASML Holding N.V.
    Inventors: Matthew Lipson, Robert D. Harned, Geoffrey O'Connor, Timothy O'Neil
  • Publication number: 20080118894
    Abstract: Process for producing an inorganic-inorganic composite material, in which an open-pore, crystalline oxide ceramic shaped part is produced from an oxide ceramic powder or a powder of an oxide ceramic mixture after shape-imparting processing and presintering, an infiltration substance is applied to this shaped part in vacuo and at room temperature, and the oxide ceramic is sintered in a densifying manner under an air atmosphere and at ambient pressure to form an inorganic-inorganic composite material.
    Type: Application
    Filed: January 27, 2005
    Publication date: May 22, 2008
    Inventors: Frank Rothbrust, Christian Ritzberger, Wolfram Holand, Volker Rheinberger
  • Patent number: 7153464
    Abstract: A ceramic matrix composite (CMC) structure, and method of forming same, the structure having internal air flow channels and cooling holes created by the process of sewing or stitching a fugitive fiber or thread into plies of ceramic cloth, preferably prior to consolidation of the ceramic cloth with a CMC slurry, followed by heating to convert the slurry material to a hardened ceramic component part of a predetermined shape. Upon heating the infiltrated and consolidated ceramic cloth to about between 1100 and 2100 degrees Fahrenheit, such as by hot pressing the structure containing the fugitive fibers therein, the fugitive fibers disintegrate, leaving channels and cooling holes wherever the stitched fugitive fiber or thread was previously located. Thus, the channels and cooling holes flow between plies as well as across the surface of the top and bottom plies.
    Type: Grant
    Filed: December 1, 2003
    Date of Patent: December 26, 2006
    Assignee: General Electric Company
    Inventors: Michael Lee Millard, Horace Richardson, Jr.
  • Patent number: 7140085
    Abstract: A capacitive vacuum measuring cell includes first and second ceramic housing bodies (1, 4) joined by an edge seal (3). A thin ceramic membrane (2) is supported between first and second housing bodies (1, 4) by the edge seal (3) at a small distance from the first housing body (1) creating a reference vacuum chamber (25) therebetween. An electrically conductive material (7) coats opposing surfaces of the first housing body (1) and the membrane (2) to form a capacitor. A measurement vacuum chamber (26) is provided between the membrane (2) and the second housing body (4). A port (5) communicates with the second housing body (4) to connect the measurement vacuum chamber (26) of the measuring cell to the medium to be measured. The membrane (2) is made from an Al2O3 slurry that is sintered in a first heating step, cooled, and then reheated to smooth the membrane.
    Type: Grant
    Filed: July 11, 2003
    Date of Patent: November 28, 2006
    Assignee: Inficon GmbH
    Inventors: Per Bjoerkman, Ray Olsson
  • Patent number: 7128870
    Abstract: A method for manufacturing multilayer ceramic electronic components includes the steps of removing organic materials from multilayer ceramic bodies having internal electrodes and ceramic layers, and then sintering the multilayer ceramic bodies. After finishing the removing step, it is preferable that the amount of the remaining organic materials in the multilayer ceramic body is 0.5 to 8.5 weight %, more preferably 1.0 to 5.0 weight %. The removing process may be performed in a neutral, a reductive or inert atmosphere. It is also preferable that the organic materials removing temperature of the internal electrodes are controlled to be higher than that of the ceramic layer.
    Type: Grant
    Filed: June 24, 2003
    Date of Patent: October 31, 2006
    Assignee: Taiyo Yuden Co., Ltd.
    Inventor: Koji Otsuka
  • Patent number: 7108827
    Abstract: The present invention relates to a ceramic sheet having uniform quality over its entire surface with a decreased number of defects such as foreign matters and flaws. When the ceramic sheet was divided into sections of 30 mm square or smaller, each divided section has 5 or less defects detected based on an image obtained with a charge coupled device (CCD) camera. The present invention also relates to a method of producing the ceramic sheet. In this method, a green sheet or a calcined sheet mainly including spherical ceramic particles having an average particle diameter of 0.1 to less than 5 ?m was used as a spacer. By using this spacer, the green sheet for ceramic sheet slides smoothly on the spacer surface when it shrinks in baking, and the friction resistance between the green sheet for ceramic sheet and the spacer is lowered. In this manner, the method of the present invention can mass-produce the above-described high quality ceramic sheets.
    Type: Grant
    Filed: April 6, 1999
    Date of Patent: September 19, 2006
    Assignee: Nippon Shokubai Co., Ltd.
    Inventors: Kazuo Hata, Norikazu Aikawa, Keijirou Takasaki
  • Patent number: 6727200
    Abstract: A dielectric ceramic powder and multilayer ceramic capacitors made from the powders are disclosed. A dielectric start powder mixture includes at least ninety weight percent essentially pure barium titanate powder having an average particle size of from 0.2 to 1.2 microns; from 0.2 to 2.5 weight percent of barium lithium borosilicate; from 0.1 to 0.3 weight percent of MnCO3; 0.4 to 1.50 weight percent Nb205 or a niobate compound, or a molar equivalent of Ta2O5 or a tantalum compound as a grain growth inhibitor; and, 0.4 to 1.2 weight percent of gadolinium oxide (Gd2O3). The start powder mixture is calcined and then sintered in an open zirconia setter at from 950° C. to 1,025° C. to produce a dielectric ceramic body that satisfies X7R capacitor performance characteristics; that includes no hazardous heavy metal oxides; and, that may include silver-palladium electrodes having 85 weight percent or more of silver.
    Type: Grant
    Filed: October 29, 2001
    Date of Patent: April 27, 2004
    Assignee: MRA Laboratories, Inc.
    Inventors: Galeb H. Maher, Samir Maher
  • Patent number: 6723673
    Abstract: The invention includes a dielectric ceramic powder mixture comprising at least ninety weight percent essentially pure barium titanate powder having an average particle size of from 0.2 to 1.2 microns; from 0.2 to 2.5 weight percent of barium lithium borosilicate flux; from 0.1 to 0.3 weight percent of MnCO3; a grain growth inhibitor such as niobium oxide or other niobate compound; and, 0.4 to 1.2 weight percent of an additive selected from the group consisting of a rare earth oxide, yttrium oxide, a combination of rare earth oxides, and a combination of yttrium oxide and rare earth oxides, such that ions of the additive(s) have an average ionic radius of about 0.97 angstroms. The dielectric ceramic powder provides a start powder for making very low firing multilayer ceramic capacitors satisfying X7R performance requirements.
    Type: Grant
    Filed: April 9, 2003
    Date of Patent: April 20, 2004
    Assignee: MRA Laboratories, Inc.
    Inventors: Galeb H. Maher, Samir Maher, James M. Wilson