Abstract: Process for the preparation of sodium fluoride from sodium hydroxide solution and hydrogen fluoride or hydrofluoric acid, characterized in that <45% strength by weight, preferably 20 to 40% strength by weight, sodium hydroxide solution and hydrogen fluoride or hydrofluoric acid are introduced separately into a saturated NaF solution in which 4 to 50% by weight, preferably 5 to 30% by weight, of solid NaF are suspended and whose temperature is in the range from 20 to 80° C., preferably 30 to 60° C.
Type:
Grant
Filed:
July 30, 1999
Date of Patent:
June 26, 2001
Assignee:
Bayer Aktiengesellschaft
Inventors:
Günter Lailach, Andreas Bulan, Günter Buss
Abstract: The present invention relates to cleaning compositions which, as powder or as aqueous formulation, comprise sodium bicarbonate and, as dispersants, polyaspartic acids and/or salts thereof, to the use of these cleaning compositions for the abrasive cleaning of hard surfaces, and also to a method of cleaning surfaces contaminated with deposits using these cleaning compositions.
Type:
Grant
Filed:
September 14, 1999
Date of Patent:
June 12, 2001
Assignee:
Bayer Aktiengesellschaft
Inventors:
Manfred Gerlach, Bernhard Lehmann, Hartwig Wendt, Herbert Emde, Urban Recht
Abstract: Described is a process and, respectively, a composition for protecting articles which come into contact with salt water or brackish water. The compositions comprise as central component thiacloprid.
Type:
Grant
Filed:
March 29, 2000
Date of Patent:
June 12, 2001
Assignee:
Bayer Aktiengesellschaft
Inventors:
Martin Kugler, Franz Kunisch, Oliver Kretschik
Abstract: The present invention relates to boron-containing carbosilanes, a process for their preparation, boron-containing oligo- or polycarbosilazanes, a process for their preparation and their use and silicon borocarbonitride ceramics and a process for their preparation.
Abstract: In the reaction of aromatic compounds with nitrating acids comprising HNO3 and, if appropriate, H2SO4 and/or H2O and/or H3PO4 to form aromatic nitro compounds, according to the invention an amount of from 0.5 to 20,000 ppm of one or more surface-active substances from the group of the anionic, cationic, zwitterionic or nonionic surface-active substances is added to the reaction mixture.
Type:
Grant
Filed:
April 26, 2000
Date of Patent:
June 5, 2001
Assignee:
Bayer Aktiengesellschaft
Inventors:
Bernd-Michael König, Johannes Dühr, Hans-Joachim Raatz, Manfred Kaczorowski
Abstract: The present invention discloses a tantalum powder for capacitors and a method for making said tantalum powder wherein agglomerated tantalum powder is produced by means of thermal agglomeration of starting tantalum powders in the presence of hydrogen.
Abstract: Using the process according to the invention, it is possible to provide, with few reaction steps, a novel route to &agr;-substituted ring systems which optionally have further substituents.
Type:
Grant
Filed:
August 31, 1999
Date of Patent:
May 22, 2001
Assignee:
Bayer Aktiengesellschaft
Inventors:
Christoph Gürtler, Manfred Jautelat, Helmut Greiving, Herbert Hugl
Abstract: A method for cleaning a surface by flooding and thereby cleaning a surface contaminated with deposits with a mixture containing water, wood chippings, and optionally, polyaspartic acid or a derivative of a polyaspartic acid.
Abstract: The present invention relates to a process for preparing fluorine-containing phenethylamines which is characterized in that, in a first step, a substituted bromobenzene is reacted with an N-vinylimide in the presence of a palladium catalyst, in a second step, the resulting substituted &bgr;-iminovinylbenzene is hydrogenated catalytically and in a third step, the substituted &bgr;-iminovinylbenzene obtained in the second step is cleaved. This process also provides access to novel &bgr;-iminovinyl- and &bgr;-iminoethylbenzenes.
Abstract: An improved process for preparing quinolone- and naphthyridonecarboxylic acids and esters thereof from benzoyl chlorides and nicotinoyl chlorides, respectively, in which the reaction carried out in the presence of a non-polar to slightly polar solvent without separation of intermediaries that form during the process.
Type:
Grant
Filed:
June 11, 1999
Date of Patent:
May 8, 2001
Assignee:
Bayer Aktiengesellschaft
Inventors:
Norbert Lui, Hans Panskus, Herbert Müller
Abstract: The invention relates to a novel method for preparing 3-hydroxy-2-methylbenzoic acid by reacting disodium 3-amino-1,5-naphthalinedisulfonic acid with aqueous potassium hydroxide solution at a pressure of at least 100 bar.
Abstract: A process for the preparation of iminodisuccinic acid alkali metal salts by reaction of maleic acid and ammonia in an aqueous medium in the presence of alkali metal hydroxides and working up thereof.
Type:
Grant
Filed:
June 1, 2000
Date of Patent:
March 27, 2001
Assignee:
Bayer Aktiengesellschaft
Inventors:
Torsten Groth, Winfried Joentgen, Paul Wagner, Frank Döbert, Eckhard Wenderoth, Thomas Roick
Abstract: The invention relates to a process for the preparation of specific salts of 1-substituted 2,4-diaminobenzenes by catalytic hydrogenation of 1-substituted 2,4-dinitrobenzenes and addition of the reaction product obtained after the hydrogenation and separated from the catalyst to an aqueous solution of an acid.
Type:
Grant
Filed:
April 11, 2000
Date of Patent:
March 20, 2001
Assignee:
Bayer Aktiengesellschaft
Inventors:
Lars Rodefeld, Alexander Klausener, Horst Behre
Abstract: The process according to the invention can be illustrated by way of example by the following equation:
The monosodium salt of the 3-cyano-2-hydroxy-5-fluoropyrid-6-one (cf. Formula (I)) and/or tautomers thereof are preferably employed in the process according to the invention.
The use of a basic catalyst enables significantly lower amounts of chlorinating agent to be employed in the chlorination according to the invention than is necessary, for example, for chlorination of the free dihydroxy compound according to EP-A 333 020. Furthermore, the product 2,6-dichloro-5-fluoronicotinonitrile is obtained in a high purity and high yields after hydrolysis, which is not the case if the conditions according to EP-A 333 020 are applied.
Basic catalysts which can be used for the process according to the invention are, for example, organic bases, for example aliphatic and aromatic amines and amides, and also inorganic bases, for example basic compounds of nitrogen and phosphorus and salts thereof.
Type:
Grant
Filed:
September 27, 1999
Date of Patent:
March 6, 2001
Assignee:
Bayer Aktiengesellschaft
Inventors:
Andreas Sattler, Guido Steffan, Bernd Griehsel
Abstract: Provided is a process for the preparation of specific 1-substituted 2,4-dinitrobenzenes by reaction of 1-halogeno-2,4-dinitrobenzenes with mono-alkali metal salts of specific diols, in which the 1-halogeno-2,4-dinitrobenzene and the mono-alkali metal salt of the diol are simultaneously added and reacted.
Type:
Grant
Filed:
April 11, 2000
Date of Patent:
March 6, 2001
Assignee:
Bayer Aktiengesellschaft
Inventors:
Lars Rodefeld, Alexander Klausener, Ferdinand Hagedorn
Abstract: The invention relates a tantalum powder free of alkali and fluorine, which for a relatively small primary particle size has comparatively large secondary particles and is suitable for producing capacitors with a specific charge of between 100,000 and 180,000 &mgr;FV/g at specific residual currents of less than 2nA/&mgr;FV.
Abstract: Acetophenones which are substituted on the aromatic ring by fluoroalkyl are prepared in a particularly advantageous, environmentally friendly and effective manner from fluoroalkylanilines and acetaldoxime by preparing from a fluoroalkylaniline a corresponding diazonium salt solution, and reacting this with acetaldoxime in the presence of at least one copper compound, without adding any buffer salts or reducing agents, carrying out the reaction at from 20 to 50° C. and in the presence of halide ions and subsequently heating to a temperature in the range from 70 to 110° C.
Type:
Grant
Filed:
November 1, 1999
Date of Patent:
February 6, 2001
Assignee:
Bayer Aktiengesellschaft
Inventors:
Wulf Kühnle, Albrecht Marhold, Guido Steffan
Abstract: The present invention relates to processes for the production of cobalt(II) carbonates corresponding to the general formula Co[(OH)2]a[CO3]1−a, cobalt(II) carbonates and cobalt(II) oxalate carbonates obtainable by the process and the use thereof.
Type:
Grant
Filed:
November 25, 1997
Date of Patent:
February 6, 2001
Assignee:
H. C. Stack GmbH & Co. KG
Inventors:
Astrid Görge, Juliane Messe-Marktscheffel, Dirk Naumann, Armin Olbrich, Frank Schrumpf
Abstract: The invention relates to melting pots provided with silicon protective layers, a process for applying the silicon protective layer and the use thereof.
Type:
Grant
Filed:
August 4, 1999
Date of Patent:
December 26, 2000
Assignee:
Bayer Aktiengesellschaft
Inventors:
Horst Lange, Wolfgang Krumbe, Heinz Gatzweiler
Abstract: An apparatus is described which consists of a rigid plate and a vacuum insulation panel, in which the vacuum insulation panel is fixed to the rigid plate by a polyurethane foam applied as a liquid reaction mixture, wherein the vacuum insulation panel contains open-cell rigid plastics foam and/or open-cell rigid plastics foam recyclate. A refrigerated cabinet element containing said apparatus is additionally described.