Patents Represented by Attorney George A. Kap
  • Patent number: 5755947
    Abstract: Underplating between a metallic plating base and a photoresist deposited reon can be reduced or eliminated by a method of fabricating a microstructure which includes the steps of:(a) depositing a plating base on the adhesion layer;(b) depositing on the plating base a sacrificial layer of a material that reduces or eliminates underplating on the plating base compared to underplating in absence of the sacrificial layer;(c) depositing a photoresist on the sacrificial layer;(d) exposing, developing and removing the exposed photoresist from the substrate to uncover a portion of the sacrificial layer;(e) removing the sacrificial layer portion from the substrate to uncover a portion of the plating base; and(f) depositing a metallic material on the uncovered plating base under the influence of electrical current.
    Type: Grant
    Filed: January 31, 1996
    Date of Patent: May 26, 1998
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: Robert W. McElhanon, William K. Burns
  • Patent number: 5708116
    Abstract: A reaction product of a liquid monomeric allyletherfluoroalkylene benzene d a liquid polymethylhydrosiloxane, which reaction product in a cured, solid state has dielectric constant below about 2.5.
    Type: Grant
    Filed: May 31, 1995
    Date of Patent: January 13, 1998
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: James R. Griffith, Henry S. W. Hu
  • Patent number: 5705087
    Abstract: This invention pertains to hydrocarbon fuel composition and deicing compoion prepared with a compound selected from the group consisting of acetals, ketals, esters, derivatives thereof and mixtures thereof; and a process for deicing a substrate using the noted deicing composition.
    Type: Grant
    Filed: May 31, 1996
    Date of Patent: January 6, 1998
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: George W. Mushrush, Dennis Hardy
  • Patent number: 5702586
    Abstract: Process of smoothing or polishing a diamond surface to reduce asperities reon to a level as low as about 20 nm from the horizontal by implanting the diamond surface with ions to form a non-diamond carbon damage layer on or below the diamond surface below the disparity depth and dissolving the non-diamond carbon by submerging the non-diamond carbon in a liquid having sufficient electric field to dissolve the non-diamond carbon.
    Type: Grant
    Filed: June 28, 1994
    Date of Patent: December 30, 1997
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: Pehr E. Pehrsson, Michael L. Marchywka
  • Patent number: 5629248
    Abstract: A preferred embodiment of a sulfide glass with improved mechanical and optical properties such as extended transmission in the infrared region of radiation having wavelengths of up to about 15 microns, Tg in the range of 370.degree.-550.degree. C., and thermal stability of 100.degree.-300.degree. C., containing, on mol basis, 36-72% germanium sulfide, 2-38% gallium sulfide and/or indium sulfide, and 26-62% of at least one modifier containing an alkaline earth sulfide. A process for making glass of improved mechanical and optical properties comprises the steps of mixing glass components, including an alkaline earth modifier in elemental or sulfide form; melting the glass components in an inert vessel contained in a sealed ampoule to form a molten mixture; cooling the molten glass mixture to a solid state; annealing the solid glass; and cooling the annealed glass to about room temperature.
    Type: Grant
    Filed: October 10, 1995
    Date of Patent: May 13, 1997
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: Ishwar D. Aggarwal, Celia I. Merzbacher, Barry B. Harbison, John M. Jewell
  • Patent number: 5619093
    Abstract: In a system containing an electron field emitter array characterized by aying diamond powder to a substrate and affixing the powder thereto, the diamond powder being composed of particles having sharp tips which are adapted to emit electrons in a vacuum and in an electric field, which electrons impact a phosphor layer disposed on an anode spaced above the tips of the diamond powder particles.
    Type: Grant
    Filed: March 31, 1995
    Date of Patent: April 8, 1997
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: John W. Glesener, Arthur A. Morrish
  • Patent number: 5599751
    Abstract: A sulfide glass with improved mechanical and optical properties such as ended transmission in the infrared region of radiation having wavelengths of up to about 15 microns; Tg in the region of 410.degree.-550.degree. C.; and thermal stability of 100.degree.-300.degree. C. based on the difference between T.sub.g and T.sub.x, comprising, on mol basis, 20-90% germanium sulfide, 0-60% gallium sulfide, and 5-60% of at least one modifier in sulfide form. A process for improving mechanical and optical properties of a sulfide glass based on gallium sulfide and/or germanium sulfide comprises the steps of mixing glass components, including a modifier in elemental or sulfide form; melting the glass components to form a molten mixture; cooling the molten glass mixture to a solid state; annealing the solid glass; and cooling the annealed glass to about room temperature.
    Type: Grant
    Filed: February 28, 1995
    Date of Patent: February 4, 1997
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: Barry B. Harbison, John M. Jewell, Celia I. Merzbacher, Ishwar D. Aggarwal
  • Patent number: 5593732
    Abstract: A nontoxic antifouling system is provided at ambient conditions on a subste which has a solid release layer bonded to a solid bonding layer which in turn is bonded to said substrate. The release layer has excellent release property and is bonded to the bonding layer. The bonding layer contains a component which is believed to react with the same or a similar component in the release layer to enhance the desired bond therebetween. The bonding layer is tougher than the release layer but its release property is inferior to that of the release layer.
    Type: Grant
    Filed: April 28, 1995
    Date of Patent: January 14, 1997
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventor: James R. Griffith
  • Patent number: 5587210
    Abstract: A process for making diamond and diamond products includes the steps of ianting ions in a diamond substrate to form a damaged layer of non-diamond carbon below the top surface of the substrate, heating the substrate to about 600-1200.degree. C. growing diamond on the top surface of the heated substrate by chemical vapor deposition, and electrochemically etching the damaged layer to separate the grown diamond from the substrate along the damage layer. The diamond product consists of a first diamond layer and a second diamond layer attached to the first layer. The second layer contains damage caused by ions traversing the second layer.
    Type: Grant
    Filed: June 28, 1994
    Date of Patent: December 24, 1996
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: Michael J. Marchywka, Pehr E. Pehrsson
  • Patent number: 5529841
    Abstract: A field test kit for determining quantity of hydrogen sulfide in a liquid st sample. The test kit includes a test container with an opening for a liquid test sample containing hydrogen sulfide gas and a cap provided over the opening. The cap has colorimetric particulate indicator on its top inside surface. A silicone barrier disposed over the indicator protects the indicator from contact with the test sample.
    Type: Grant
    Filed: September 29, 1994
    Date of Patent: June 25, 1996
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventor: Rex A. Neihof
  • Patent number: 5525538
    Abstract: An amorphous compound is changed to single crystal structure by heating at an elevated temperature in an inert atmosphere or in an atmosphere of a forming gas, the amorphous compound is composed of at least one Group III-A element of the Periodic Table and at least one Group V-A element, the amorphous compound having an excess over stoichiometric amount of at least one Group V-A element. The single crystal phase compound, intrinsically doped with at least one element from Group V-A, has the properties of high conductivity for a semiconductor without using any extrinsic dopant and a non-alloyed ohmic contact with a metal.
    Type: Grant
    Filed: March 8, 1995
    Date of Patent: June 11, 1996
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: Mark E. Twigg, Mohammad Fatemi, Bijan Tadayon
  • Patent number: 5525800
    Abstract: A fiber optic sensor for detecting at least one chemical by evanescent wave spectroscopy comprises a generator of a light signal, a mirror for introducing the light signal into a fiber, a clad optical chalcogenide glass fiber, a mirror for directing the light signal from the fiber into a detector, and a detector for detecting chemicals by the fiber. The fiber comprises a core and a clad having lower refractive index than the core enveloping and being in continuous contact with the core, at least one region on the fiber completely or partially devoid of the clad, and a polymer disposed in the region having affinity for the chemical(s). There being a different polymer in each region if there is more than one region.
    Type: Grant
    Filed: October 31, 1994
    Date of Patent: June 11, 1996
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: Jasbinder S. Sanghera, Pablo C. Pureza, Ishwar D. Aggarwal, Gregory Nau
  • Patent number: 5519278
    Abstract: A method for reducing and/or shifting stress in at least one outer end poon of an actuator made from a piezoelectric material. The actuator is affixed to a substrate by an adhesive bond and adapted to cycle between an expanded and contracted positions, which creates stresses in the actuator and in the bond. The method includes the step of doping at least one outer portion of the actuator with a metal oxide to reduce piezoelectric activity therein. In a preferred embodiment, the doped outer portion has a gradient composition varying from the maximum at the end of the actuator to essentially zero concentration at a point inward of the end. The system includes a doped piezoelectric actuator adhesively bonded to a substrate and electrodes attached to the actuator for receiving electrical energy, the actuator containing a metal oxide dopant in the outer portions thereof.
    Type: Grant
    Filed: December 23, 1994
    Date of Patent: May 21, 1996
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: Manfred Kahn, Peter Matic, George C. Kirby, III
  • Patent number: 5502345
    Abstract: An actuator including a unitary ceramic element capable of bending in resse to an applied voltage. The ceramic has a first region of lower resistivity in contact with a second region of higher resistivity. There is no seam where said regions contact each other. The first region contains an additive in an amount needed to reduce resistivity thereof relative to said second region. The second region is devoid of additive or contains a different additive that raises resistivity thereof or contains the same additive in a different amount than in the first region.
    Type: Grant
    Filed: August 29, 1994
    Date of Patent: March 26, 1996
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: Manfred Kahn, Carl C. Wu, Saadi Zain
  • Patent number: 5486495
    Abstract: A germanate glass ceramic article which has better thermal and physical perties than the competing materials of zinc sulfide, spinel, and sapphire is made by mixing germanate ceramic glass components; melting the components to form a molten mass; cooling the molten mass to form a solid glass article; nucleating the solid article by heating it in the range of about 630.degree.-790.degree. C. for about 1-16 hours to develop nuclei in the article; and crystallizing the nucleated article by heating it, after nucleation, in the range of about 1/2 minute to about 8 hours to grow the nuclei to crystallites having an average diameter of less then about 1000 nanometer (nm); and cooling to form the glass ceramic.
    Type: Grant
    Filed: December 23, 1994
    Date of Patent: January 23, 1996
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: John M. Jewell, Barry B. Harbison, Ishwar D. Aggarwal, Shyam S. Bayya
  • Patent number: 5481189
    Abstract: The magnetic sensor of this invention is characterized by a magnet suspen on a torsion bar or wire and by a tunneling tip separated from one end of the magnet, a gap between the tip and the magnet that is small enough to support a tunneling current, an electrical source for imposing a constant biasing voltage across the gap, an electrical force to maintain the magnet and the tip sufficiently close so that a constant tunneling current is maintained therebetween, a feedback circuit to monitor current changes in the gap that result from rotation of the magnet due to changes in the surrounding magnetic field, and at least one recorder to record changes in the magnetic field.
    Type: Grant
    Filed: February 7, 1994
    Date of Patent: January 2, 1996
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: Daniel DiLella, Richard J. Colton
  • Patent number: 5470373
    Abstract: Oxidation resistant particles composed of copper and at least one metal having a valence of +2 or +3 and having an intermediate lattice energy for the metal in its hydroxide form. The metal is selected from nickel, cobalt, iron, manganese, cadmium, zinc, tin, magnesium, calcium and chromium. In one embodiment, the phases of copper and at least one metal in the particles are separate and the concentration of the metal is greater near the surface of the particles than inwardly thereof. Process for making the oxidation resistant copper particles includes the steps of dissolving a copper salt and a salt of at least one of the metals in a suitable solvent or diluent; forming primary particles of copper and at least one metal in basic form by mixing a base and the salt solution; separating, washing and drying the primary particles; reducing the primary particles to metallic form; and heat treating the particles in metallic form at an elevated temperature.
    Type: Grant
    Filed: November 15, 1993
    Date of Patent: November 28, 1995
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: Alan S. Edelstein, Forrest H. Kaatz, Vincent G. Harris
  • Patent number: 5469369
    Abstract: A method and a system using that method are provided which employ a pattern ecognition algorithm to improve sensitivity in detecting hazardous vapors. The algorithm enables the discrimination of vapors of interest from non-hazardous substances at higher concentrations in varying relative humidity. A weight vector is generated corresponding to a N-space representation of a class comprising known vapors of interest, and a N-space representation of the unknown vapor is used to generate an unknown pattern vector. By calculating the dot product of the unknown pattern vector and the weight vector a determination can be made as to whether the unknown vapor is within the class. The weight vector is generated by selecting a training set comprising a subset of the known vapors of interest and background vapors and generating an N-space representation of the training set so as to create an associated weight vector.
    Type: Grant
    Filed: November 2, 1992
    Date of Patent: November 21, 1995
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: Susan L. Rose-Pehrsson, Daniel Di Lella, Jay W. Grate
  • Patent number: 5449553
    Abstract: A nontoxic antifouling system is provided at ambient conditions on a subste which has a solid release layer bonded to a solid bonding layer which in turn is bonded to said substrate. The release layer has excellent release property and is bonded to the bonding layer. The bonding layer contains a component which is believed to react with the same or a similar component in the release layer to enhance the desired bond therebetween. The bonding layer is tougher than the release layer but its release property is inferior to that of the release layer.
    Type: Grant
    Filed: March 28, 1994
    Date of Patent: September 12, 1995
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventor: James R. Griffith
  • Patent number: 5419785
    Abstract: An amorphous compound is changed to single crystal structure by heating at an elevated temperature in an inert atmosphere or in an atmosphere of a forming gas, the amorphous compound is composed of at least one Group III-A element of the Periodic Table and at least one Group V-A element, the amorphous compound having an excess over stoichiometric amount of at least one Group V-A element. The single crystal phase compound, intrinsically doped with at least one element from Group V-A, has the properties of high conductivity for a semiconductor without using any extrinsic dopant and a non-alloyed ohmic contact with a metal.
    Type: Grant
    Filed: April 12, 1994
    Date of Patent: May 30, 1995
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: Mark E. Twigg, Mohammad Fatemi, Bijan Tadayon