Abstract: Fireproofing compositions are provided. The compositions comprise a hydratable cementitious binder and polystyrene aggregate falling within particular particle size distribution limits. The compositions can also include an air entraining agent and a fibrous material. On addition of water, the compositions form settable, sprayable slurries which can be pumped to the point of application. The slurries are capable of spray application to steel structural members and adhere to the member in the slurried state and after setting. Excellent fire and heat protection is provided to the member despite the organic nature of the polystyrene aggregate.

Abstract: Sprayable fireproofing compositions for structural members such as steel columns are provided, as well as a method of applying multiple coatings thereof. The compositions comprise a Portland cement-based material, stucco, and an accelerator. The compositions eliminate the long setting times typical of Portland cement-based materials, and improve the hangability thereof. The product is produced by dry blending a mixture of Portland cement, stucco (calcium sulfate hemi-hydrate) and optionally, a stucco set retarder and shredded polystyrene aggregate. Upon the addition of water, sprayable slurries are formed which can be pumped to the point of application. An accelerator is added in close proximity to the point of injection. Other additives may also be included, such as starch, adhesives and cement strength enhancers. The slurries adhere to the structural member in the slurried state and after setting to provide excellent fire and heat protection.

Abstract: The present invention relates to a packaging and dispensing system especially suitable for semi-fluid or fluid cement admixtures. The admixture is encapsulated in a material, such as gelatin or wax, which ruptures, shatters, or disintegrates in the wet cementitious mixture during a period of mechanical mixing. The present invention also contemplates a method of modifying the properties of cementitious mixtures by adding thereto an encapsulated admixture in a predetermined amount sufficient to provide a modified cementitious composition having the desired properties.

Abstract: Disclosed is an air turn for supporting and optionally drying a web, the air turn comprising a plurality of air bars having a wing type foil with an adjustable web-to-foil gap and multiple relief holes. The apparatus of the invention allows for the ability to control the air vortex off the lower air turn in an air turn array and to control the pressure between the web and foil, thereby eliminating web flutter.

Abstract: A shielding device such as for a primer fuse is disclosed. The shielding device is multi-layered, and combines the shielding affectivity of metal foil with electrically conductive adhesive and a dielectric film. Upon application of the shielding device, the primer in the base of the shell is shielded, yet an electrical connection can be made upon firing the pin to fire the round without requiring removal of the shielding device.

Abstract: Apparatus and method for reducing web slot infiltration in web floatation drying apparatus, including a moveable web slot assembly which moves according to the position of the running web in the dryer. In one embodiment, the dryer includes a web steering assembly which steers the web in a substantially straight sinusoidal path. The moveable web slot is in communication with the steering assembly so that the slot moves to accommodate the position of the steered web.

Abstract: Apparatus for the non-contact drying of a web of material with a combination of infrared radiation and heated air. The apparatus includes a dryer enclosure in which is mounted a plurality of air bars in air-receiving communication with upper and lower headers both above and below the web for the contactless convection drying of the web. Mounted between the air bars are infrared gas fired burners. In order to accommodate the infrared burners between the air bars, spacers are fitted on the header system supplying air to the air bars. The drying surface of the web is thus alternately heated by infrared radiation and then scrubbed by high velocity air to remove the moist boundary layer. Since the burners are completely enclosed, all heat energy is captured in the exhaust system of the dryer assembly and a portion can be used to supply hot convention air back to the dryer.

Abstract: A web threading system for threading a web through a dryer and an optional chill roll stand. The web attaches to a lock up roll threading bar. A lock up roll threading bar is carried between a pair of parallel dryer chains to lead and thread the web through the dryer environment, and through and about optional chill rolls in a chill stand. A locking mechanism is provided for the lock up roll threading bar to engage the web for ready attachment or disengagement of the web from the lock up roll threading bar before and after the threading process.

Abstract: A compact efficient air flotation dryer with a built-in afterburner for combustion of solvent-laden air within a dryer-enclosed combustion chamber. An internal exhaust fan propels internal solvent-laden air across a burner where it combusts, causing a heat rise. Heated, combusted air is routed to a recirculating supply air fan which provides for pressurized heated air for air bars for drying a web. Heated air in excess of that required to dry the web is vented externally and helps to maintain desired solvent concentration levels Variable parameters such as fan speed, burner temperatures, air box pressures, exhaust air rate, solvent concentration, supply air flow, supply air temperature and damper vane position are monitored, and the components are actuated to effect a high level of clean up efficiency.

Abstract: Electromagnetic absorber having serrations on a surface or surfaces thereof to reduce reflectivity of incident electromagnetic waves thereon. The serrations form a plurality of fins, the height of adjacent fins being spaced by a small distance. Preferably the total absorber wedge height is greater than about 1 wavelength at the lowest design frequency and the height between the serration tips is less than 1/4 wavelength at the lowest design frequency.

Abstract: A novel intermediate useful in the synthesis of ethylenediaminetriacetic acid (ED3A) or its salts. N,N'-ethylenediaminediacetic acid (ED2AH.sub.2) or a salt containing up to one equivalent of base cation is condensed with formaldehyde to form a stable 5-membered ring intermediate. The addition of cyanide across this cyclic material forms ethylenediamine N,N'-diacetic acid-N'-cyanomethyl or salts thereof (mononitrile-diacid), which is a useful intermediate in the production or ED3A. The nitrile in aqueous solutions may be spontaneously cyclized to form 2-oxo-1,4-piperazinediacetic acid (3KP) or salts thereof. In the presence of excess base, salts of ED3A are formed in excellent yield and purity.

Abstract: A novel intermediate useful in the synthesis of ethylenediaminetriacetic acid (ED3A) or its salts. A salt of N,N'-ethylenediaminediacetic acid (ED2AH.sub.2) is condensed with formaldehyde to form a stable 5-membered ring intermediate. The addition of cyanide across this cyclic material forms ethylenediamine N,N'-diacetic acid-N'-cyanomethyl or salts thereof (mononitrile-diacid), which is a useful intermediate in the production of ED3A. The nitrile in aqueous solutions may be spontaneously cyclized to form 2-oxo-1,4-piperazinediacetic acid (3KP) or salts thereof. In the presence of excess base, salts of ED3A are formed in excellent yield and purity.

Abstract: A method of producing a synthetic detergent soap base, comprising neutralizing n-acyl sarcosine at an elevated temperature with a fatty acid salt to the desired pH, and allowing the mixture to cool. The resulting product is non-irritating and non-drying, and exhibits apparent skin substantivity and pleasant skin feel.

Abstract: A process for producing iminodiacetonitrile (IDAN) from glycolonitrile and ammonia or its salt is disclosed. In the batch process, pH is controlled with the addition of ammonia or suitable acids. In the continuous process, glycolonitrile and ammonia are reacted in near stoichiometric amounts at a temperature from about 90.degree. C. to about 180.degree. C.

Abstract: A novel intermediate useful in the synthesis of ethylenediaminetriacetic acid (ED3A) or its salts. A salt of N,N'-ethylenediaminediacetic acid (ED2AH.sub.2) is condensed with formaldehyde to form a stable 5-membered ring intermediate. The addition of cyanide across this cyclic material forms ethylenediamine N,N'-diacetic acid-N'-cyanomethyl or salts thereof (mononitrile-diacid), which is useful intermediate in the production of ED3A. The nitrile in aqueous solutions may be spontaneously cyclized to form 2-oxo-1,4-piperazindeiacetic acid (3KP) or salts thereof. In the presence of excess base, salts of ED3A are formed in excellent yield and purity.

Abstract: A high temperature control damper for use in an air flotation dryer with built-in afterburner or any other high temperature environment. Two damper blades are mounted between high temperature bearings and rotate in an insulated housing. The inner ends of the damper engage in a ship-lap joint, and the outer ends of the damper engage against sealing flanges.

Abstract: N-methyliminodiacetic acid is separated from mixtures of N-methyliminodiacetic acid and sodium sulfate formed by acidification of solutions of its disodium salt with sulfuric acid. Thus the disodium salt is acidified with sulfuric acid to a ph of about 2 and concentrated by evaporating water so as to crystallize sodium sulfate. The sodium sulfate is separated, and the resulting mother liquor is cooled to precipitate N-methyliminodiacetic acid, which is then separated.

Abstract: Fe(III) complexes having high bulk density and a process for the production of the same without the generation of heavy metal-contaminated effluents are disclosed. Solid complexes of EDTANaFe and EDTAKFe having high bulk densities are formed by reaction with ferric sulfate containing low chromium levels, followed by total drying of the resulting mixture in the same processing equipment without the prior separation of the sulfate salts formed.

Abstract: An apparatus is provided which both floatingly supports a web, and maintains the web in a substantially straight path as it travels through a dryer. The apparatus comprises a steerable air bar assembly comprising: i) one or more adjustable air bars, each having an elongated surface from which air may be discharged, said surface being in opposing relation to the running web, and each having two ends; ii) air supply means, in fluid communication with the air bars; and iii) adjustment means for altering the orientation of the elongated surfaces of the adjustable air bars with respect to the running web. In a preferred embodiment the orientation of the surfaces is adjusted such that each said surface rotates about an axis which is substantially parallel to the longitudinal centerline of the running web. Said steerable air bar assembly is positioned in a web dryer such that the web is guided through the dryer in a substantially straight path.

Abstract: A process for the purification of mandelic acid N,N-diethylamide, DEM, by forming a crystalline adduct of DEM with a calcium halide and water.