Patents Assigned to The United States of Americas as represented by the United States Department of Energy
  • Patent number: 8270554
    Abstract: Methods of producing cesium-131. The method comprises dissolving at least one non-irradiated barium source in water or a nitric acid solution to produce a barium target solution. The barium target solution is irradiated with neutron radiation to produce cesium-131, which is removed from the barium target solution. The cesium-131 is complexed with a calixarene compound to separate the cesium-131 from the barium target solution. A liquid:liquid extraction device or extraction column is used to separate the cesium-131 from the barium target solution.
    Type: Grant
    Filed: May 19, 2009
    Date of Patent: September 18, 2012
    Assignee: The United States of America, as represented by the United States Department of Energy
    Inventors: David H. Meikrantz, John R. Snyder
  • Patent number: 8263030
    Abstract: A method for the controllable dissolution of one or more alkali metals from a vessel containing a one or more alkali metals and/or one or more partially passivated alkali metals. The vessel preferably comprising a sodium, NaK or other alkali metal-cooled nuclear reactor that has been used. The alkali metal, preferably sodium, potassium or a combination thereof, in the vessel is exposed to a treatment liquid, preferably an acidic liquid, more preferably citric acid. Preferably, the treatment liquid is maintained in continuous motion relative to any surface of unreacted alkali metal with which the treatment liquid is in contact. The treatment liquid is preferably pumped into the vessel containing the one or more alkali metals and the resulting fluid is extracted and optionally further processed. Preferably, the resulting off-gases are processed by an off-gas treatment system and the resulting liquids are processed by a liquid disposal system.
    Type: Grant
    Filed: March 7, 2011
    Date of Patent: September 11, 2012
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventors: Jeffrey Donald Jones, Kirk John Dooley, David Donald Tolman
  • Patent number: 8246767
    Abstract: The invention relates to a composition and heat treatment for a high-temperature, titanium alloyed, 9 Cr-1 Mo steel exhibiting improved creep strength and oxidation resistance at service temperatures up to 650° C. The novel combination of composition and heat treatment produces a heat treated material containing both large primary titanium carbides and small secondary titanium carbides. The primary titanium carbides contribute to creep strength while the secondary titanium carbides act to maintain a higher level of chromium in the finished steel for increased oxidation resistance, and strengthen the steel by impeding the movement of dislocations through the crystal structure. The heat treated material provides improved performance at comparable cost to commonly used high-temperature steels such as ASTM P91 and ASTM P92, and requires heat treatment consisting solely of austenization, rapid cooling, tempering, and final cooling, avoiding the need for any hot-working in the austenite temperature range.
    Type: Grant
    Filed: September 12, 2008
    Date of Patent: August 21, 2012
    Assignee: The United States of America, as represented by the United States Department of Energy
    Inventors: Paul D. Jablonski, David Alman, Omer Dogan, Gordon Holcomb, Christopher Cowen
  • Patent number: 8241600
    Abstract: A method of catalytically reforming a reactant gas mixture using a pyrochlore catalyst material comprised of one or more pyrochlores having the composition A2B2-y-zB?yB?zO7-?, where y>0 and z?0. Distribution of catalytically active metals throughout the structure at the B site creates an active and well dispersed metal locked into place in the crystal structure. This greatly reduces the metal sintering that typically occurs on supported catalysts used in reforming reactions, and reduces deactivation by sulfur and carbon. Further, oxygen mobility may also be enhanced by elemental exchange of promoters at sites in the pyrochlore. The pyrochlore catalyst material may be utilized in catalytic reforming reactions for the conversion of hydrocarbon fuels into synthesis gas (H2+CO) for fuel cells, among other uses.
    Type: Grant
    Filed: August 31, 2011
    Date of Patent: August 14, 2012
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventors: David A. Berry, Dushyant Shekhawat, Daniel Haynes, Mark Smith, James J. Spivey
  • Patent number: 8242284
    Abstract: The present disclosure relates to novel compounds having the structural Formulas (1a,1b), stereoisomers, tautomers, racemics, prodrugs, metabolites thereof, or pharmaceutically acceptable salt and/or solvate thereof as chemotherapy agents for treating of cancer, particularly androgen-independent prostate cancer. The disclosure also relates to methods for preparing said compounds, and to pharmaceutical compositions comprising said compounds.
    Type: Grant
    Filed: August 24, 2010
    Date of Patent: August 14, 2012
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventors: Andrei A. Gakh, Mykhaylo V. Vovk, Nina V. Mel'nychenko, Volodymyr A. Sukach
  • Patent number: 8227105
    Abstract: The invention relates to a unique battery having a physicochemically active membrane separator/electrolyte-electrode monolith and method of making the same. The Applicant's invented battery employs a physicochemically active membrane separator/electrolyte-electrode that acts as a separator, electrolyte, and electrode, within the same monolithic structure. The chemical composition, physical arrangement of molecules, and physical geometry of the pores play a role in the sequestration and conduction of ions. In one preferred embodiment, ions are transported via the ion-hoping mechanism where the oxygens of the Al2O3 wall are available for positive ion coordination (i.e. Li+). This active membrane-electrode composite can be adjusted to a desired level of ion conductivity by manipulating the chemical composition and structure of the pore wall to either increase or decrease ion conduction.
    Type: Grant
    Filed: November 14, 2007
    Date of Patent: July 24, 2012
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventors: Rex E. Gerald, II, Katarina J. Ruscic, Devin N. Sears, Luis J. Smith, Robert J. Klingler, Jerome W. Rathke
  • Patent number: 8182870
    Abstract: A method and device for one or more small apertures, slits, nozzles and orifices, preferably having a high aspect ratio. In one embodiment, one or more alternating layers of sacrificial layers and blocking layers are deposited onto a substrate. Each sacrificial layer is made of a material which preferably allows a radiation to substantially pass through. Each blocking layer is made of a material which substantially blocks the radiation.
    Type: Grant
    Filed: May 29, 2008
    Date of Patent: May 22, 2012
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventor: Ali M. Khounsary
  • Patent number: 8161877
    Abstract: An electronic firing system comprising a control system, a charging system, an electrical energy storage device, a shock tube firing circuit, a shock tube connector, a blasting cap firing circuit, and a blasting cap connector. The control system controls the charging system, which charges the electrical energy storage device. The control system also controls the shock tube firing circuit and the blasting cap firing circuit. When desired, the control system signals the shock tube firing circuit or blasting cap firing circuit to electrically connect the electrical energy storage device to the shock tube connector or the blasting cap connector respectively.
    Type: Grant
    Filed: December 3, 2009
    Date of Patent: April 24, 2012
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventors: Steven J. Frickey, John M. Svoboda
  • Patent number: 8149128
    Abstract: A device and method for detecting ground potential rise (GPR) comprising positioning a first electrode and a second electrode at a distance from each other into the earth. The voltage of the first electrode and second electrode is attenuated by an attenuation factor creating an attenuated voltage. The true RMS voltage of the attenuated voltage is determined creating an attenuated true RMS voltage. The attenuated true RMS voltage is then multiplied by the attenuation factor creating a calculated true RMS voltage. If the calculated true RMS voltage is greater than a first predetermined voltage threshold, a first alarm is enabled at a local location. If user input is received at a remote location acknowledging the first alarm, a first alarm acknowledgment signal is transmitted. The first alarm acknowledgment signal is then received at which time the first alarm is disabled.
    Type: Grant
    Filed: March 10, 2009
    Date of Patent: April 3, 2012
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventors: Zachery W. Allen, Gary A. Zevenbergen
  • Patent number: 8130569
    Abstract: A device for storing data using nanoparticle shuttle memory having a nanotube. The nanotube has a first end and a second end. A first electrode is electrically connected to the first end of the nanotube. A second electrode is electrically connected to the second end of the nanotube. The nanotube has an enclosed nanoparticle shuttle. A switched voltage source is electrically connected to the first electrode and the second electrode, whereby a voltage may be controllably applied across the nanotube. A resistance meter is also connected to the first electrode and the second electrode, whereby the electrical resistance across the nanotube can be determined.
    Type: Grant
    Filed: April 27, 2010
    Date of Patent: March 6, 2012
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventor: Alex Karlwalter Zettl
  • Patent number: 8128735
    Abstract: A method for separating CO2 from a gas stream comprised of CO2 and other gaseous constituents using a zeolite sorbent in a swing-adsorption process, producing a high temperature CO2 stream at a higher CO2 pressure than the input gas stream. The method utilizes CO2 desorption in a CO2 atmosphere and effectively integrates heat transfers for optimizes overall efficiency. H2O adsorption does not preclude effective operation of the sorbent. The cycle may be incorporated in an IGCC for efficient pre-combustion CO2 capture. A particular application operates on shifted syngas at a temperature exceeding 200° C. and produces a dry CO2 stream at low temperature and high CO2 pressure, greatly reducing any compression energy requirements which may be subsequently required.
    Type: Grant
    Filed: October 21, 2009
    Date of Patent: March 6, 2012
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventors: Ranjani V. Siriwardane, Robert W. Stevens
  • Patent number: 8124009
    Abstract: Aeration drying and disinfecting grain crops in bulk and pretreating seeds includes passing through a bulk of grain crops and seeds disinfecting and drying agents including an ozone and air mixture and surrounding air, subdividing the disinfecting and drying agents into a plurality of streams spaced from one another in a vertical direction, and passing the streams at different heights through levels located at corresponding heights of the bulk of grain crops and seeds transversely in a substantially horizontal direction.
    Type: Grant
    Filed: December 24, 2008
    Date of Patent: February 28, 2012
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventors: Vitaliy G. Danchenko, Ronald T. Noyes, Larysa P. Potapovych
  • Patent number: 8122780
    Abstract: An Explosion Proof Vehicle (EPV) having an interior substantially filled with an inert fluid creating an interior pressure greater than the exterior pressure. One or more flexible tubes provide the inert fluid and one or more electrical conductors from a control system to the vehicle. The vehicle is preferably used in subsurface tank inspection, whereby the vehicle is submerged in a volatile fluid.
    Type: Grant
    Filed: March 20, 2008
    Date of Patent: February 28, 2012
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventors: William T. Zollinger, Kerry M. Klingler, Scott G. Bauer
  • Patent number: 8114510
    Abstract: The invention is directed to a method for fabricating a mesoporous carbon material, the method comprising subjecting a precursor composition to a curing step followed by a carbonization step, the precursor composition comprising: (i) a templating component comprised of a block copolymer, (ii) a phenolic compound or material, (iii) a crosslinkable aldehyde component, and (iv) at least 0.5 M concentration of a strong acid having a pKa of or less than ?2, wherein said carbonization step comprises heating the precursor composition at a carbonizing temperature for sufficient time to convert the precursor composition to a mesoporous carbon material. The invention is also directed to a mesoporous carbon material having an improved thermal stability, preferably produced according to the above method.
    Type: Grant
    Filed: May 20, 2009
    Date of Patent: February 14, 2012
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventors: Sheng Dai, Xiqing Wang
  • Patent number: 8117537
    Abstract: A CAD/CAM method is disclosed for a computer system to capture and interchange schematic drawing and associated design information. The schematic drawing and design information are stored in an extensible, platform-independent format.
    Type: Grant
    Filed: February 2, 2007
    Date of Patent: February 14, 2012
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventors: Jeffrey L. Vell, Darius M. Siganporia, Arthur J. Levy
  • Patent number: 8116992
    Abstract: The invention relates to a method of determining bed velocity and solids circulation rate in a standpipe experiencing a moving packed bed flow, such as the in the standpipe section of a circulating bed fluidized reactor The method utilizes in-situ measurement of differential pressure over known axial lengths of the standpipe in conjunction with in-situ gas velocity measurement for a novel application of Ergun equations allowing determination of standpipe void fraction and moving packed bed velocity. The method takes advantage of the moving packed bed property of constant void fraction in order to integrate measured parameters into simultaneous solution of Ergun-based equations and conservation of mass equations across multiple sections of the standpipe.
    Type: Grant
    Filed: April 27, 2009
    Date of Patent: February 14, 2012
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventors: J. Christopher Ludlow, James L. Spenik
  • Patent number: 8111059
    Abstract: The disclosure herein provides an apparatus for location of a quantity of current vectors in an electrical device, where the current vector has a known direction and a known relative magnitude to an input current supplied to the electrical device. Mathematical constants used in Biot-Savart superposition equations are determined for the electrical device, the orientation of the apparatus, and relative magnitude of the current vector and the input current, and the apparatus utilizes magnetic field sensors oriented to a sensing plane to provide current vector location based on the solution of the Biot-Savart superposition equations. Description of required orientations between the apparatus and the electrical device are disclosed and various methods of determining the mathematical constants are presented.
    Type: Grant
    Filed: January 28, 2010
    Date of Patent: February 7, 2012
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventors: Paul E. King, Charles Rigel Woodside
  • Patent number: 8105974
    Abstract: A process of forming a hydrogen storage material, including the steps of: providing a first material of the formula M(BH4)X, where M is an alkali metal or an alkali earth metal, providing a second material selected from M(AlH4)x, a mixture of M(AlH4)x and MClx, a mixture of MClx and Al, a mixture of MClx and AlH3, a mixture of MHx and Al, Al, and AlH3. The first and second materials are combined at an elevated temperature and at an elevated hydrogen pressure for a time period forming a third material having a lower hydrogen release temperature than the first material and a higher hydrogen gravimetric density than the second material.
    Type: Grant
    Filed: June 16, 2009
    Date of Patent: January 31, 2012
    Assignees: Toyota Motor Engineering & Manufacturing North America, Inc., The United States of America as represented by the United States Department of Energy, Savannah River
    Inventors: Rana F. Mohtadi, Kenji Nakamura, Ming Au, Ragaiy Zidan
  • Patent number: 8081624
    Abstract: Wireless communication devices include a software-defined radio coupled to processing circuitry. The processing circuitry is configured to execute computer programming code. Storage media is coupled to the processing circuitry and includes computer programming code configured to cause the processing circuitry to configure and reconfigure the software-defined radio to operate on each of a plurality of communication networks according to a selected sequence. Methods for communicating with a wireless device and methods of wireless network-hopping are also disclosed.
    Type: Grant
    Filed: February 13, 2009
    Date of Patent: December 20, 2011
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventor: John W. Buttles
  • Patent number: 8071500
    Abstract: A catalyst for the oxidation of heavy metal contaminants, especially mercury (Hg), in an effluent stream is presented. The catalyst facilitates removal of mercury through the oxidation of elemental Hg into mercury (II) moieties. The active component of the catalyst is partially combusted coal, or “Thief” carbon, which can be pre-treated with a halogen. An untreated Thief carbon catalyst can be self-promoting in the presence of an effluent gas streams entrained with a halogen.
    Type: Grant
    Filed: July 13, 2010
    Date of Patent: December 6, 2011
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventors: Evan J. Granite, Henry W. Pennline