Patents Examined by Kenneth A Bratland, Jr.
  • Patent number: 11846038
    Abstract: A method of growing a semi-insulating SiC single crystal ingot, the method comprising the steps of: (1) placing a dopant coated with silicon carbide (SiC) and a carbon-based material into a reaction vessel containing a seed crystal fixed thereto; and (2) growing a SiC single crystal on the seed crystal, thereby yielding a high-quality semi-insulating SiC single crystal ingot with a uniform thickness-based doping concentration. In addition, another embodiment relates to a method of growing a semi-insulating silicon carbide single crystal ingot, the method comprising the steps of: (a) placing in a reaction vessel, a composition comprising a carbon-containing polymer resin, a solvent, a dopant, and silicon carbide (SiC); (b) solidifying the composition; and (c) growing a SiC single crystal ingot on a seed crystal fixed to the reaction vessel, thereby yielding a high-quality semi-insulating SiC single crystal ingot with a uniform thickness-based doping concentration.
    Type: Grant
    Filed: July 26, 2019
    Date of Patent: December 19, 2023
    Assignee: SENIC Inc.
    Inventors: Jung Woo Choi, Jung-Gyu Kim, Kap-Ryeol Ku, Sang Ki Ko, Byung Kyu Jang
  • Patent number: 11834753
    Abstract: The present invention relates to a heating method for a reactor (1) for epitaxial deposition; the reactor (1) comprises a susceptor (2) and an inductor (4); the inductor (4) is adapted to heat the susceptor (2) by electromagnetic induction when it is electrically powered; the inductor (4) comprises a plurality of turns (41-47); during heating of the susceptor (2) from a first temperature to a second temperature, the position of one or more turns (43) of the inductor (4) with respect to the susceptor (2) and to the other turns of the inductor (4) is changed. The turns (43) are actuated by means of an appropriate actuation system (61, 62, 63).
    Type: Grant
    Filed: July 9, 2021
    Date of Patent: December 5, 2023
    Assignee: LPE S.p.A.
    Inventors: Vincenzo Ogliari, Silvio Preti, Franco Preti
  • Patent number: 11837479
    Abstract: An advanced temperature control system and method are described for a wafer carrier in a plasma processing chamber. In one example a heat exchanger provides a temperature controlled thermal fluid to a fluid channel of a workpiece carrier and receives the thermal fluid from the fluid channel. A proportional valve is between the heat exchanger and the fluid channel to control the rate of flow of thermal fluid from the heat exchanger to the fluid channel. A pneumatic valve is also between the heat exchanger and the fluid channel also to control the rate of flow of thermal fluid from the heat exchanger and the fluid channel. A temperature controller receives a measured temperature from a thermal sensor of the carrier and controls the proportional valve and the pneumatic valve in response to the measured temperature to adjust the rate of flow of the thermal fluid.
    Type: Grant
    Filed: July 22, 2016
    Date of Patent: December 5, 2023
    Assignee: Applied Materials, Inc.
    Inventors: Fernando M. Silveira, Chunlei Zhang, Phillip Criminale, Jaeyong Cho
  • Patent number: 11828000
    Abstract: A process for producing a monocrystalline layer of LNO material comprises the transfer of a monocrystalline seed layer of YSZ material to a carrier substrate of silicon material followed by epitaxial growth of the monocrystalline layer of LNO material.
    Type: Grant
    Filed: March 26, 2019
    Date of Patent: November 28, 2023
    Assignee: Soitec
    Inventor: Bruno Ghyselen
  • Patent number: 11827999
    Abstract: Embodiments of the present disclosure generally relate to silicon carbide coated base substrates, silicon carbide substrates thereof, and methods for forming silicon carbide coated base substrates. In some embodiments, a method includes introducing a first silicon-containing precursor to a process chamber at a first temperature of about 800° C. to less than 1,000° C. to form a first silicon carbide layer on a base substrate. The method includes introducing a second silicon-containing precursor, that is the same or different than the first silicon-containing precursor, to the process chamber at a second temperature of about 1,000° C. to about 1,400° C. to form a second silicon carbide layer on the first silicon carbide layer.
    Type: Grant
    Filed: January 12, 2021
    Date of Patent: November 28, 2023
    Assignee: Applied Materials, Inc.
    Inventors: Yen Lin Leow, Xinning Luan, Hui Chen, Kirk Allen Fisher, Shawn Thomas
  • Patent number: 11821108
    Abstract: The present invention relates to a method for reducing lateral growth as well as growth of the bottom surface of crystals in a crystal growing process, wherein before the crystal seed undergoes a growing process the method includes a step of wrapping the crystal seed with metal foil so that all the side surfaces as well as the bottom surface of the crystal seed are surrounded by the foil.
    Type: Grant
    Filed: June 20, 2022
    Date of Patent: November 21, 2023
    Assignee: Instytut Wysokich Cisnien Polskiej Akademii Nauk
    Inventors: Karolina Grabianska, Robert Kucharski, Michal Bockowski
  • Patent number: 11814747
    Abstract: Gas-phase reactor systems and methods suitable for use with precursors that are solid phase at room temperature and pressure are disclosed. The systems and methods as described herein can be used to, for example, form amorphous, polycrystalline, or epitaxial layers (e.g., one or more doped semiconductor layers) on a surface of a substrate.
    Type: Grant
    Filed: April 15, 2020
    Date of Patent: November 14, 2023
    Assignee: ASM IP Holding B.V.
    Inventors: John Tolle, Joseph P. Margetis
  • Patent number: 11795573
    Abstract: A method of manufacturing a group III nitride crystal according to a first aspect includes: preparing a seed substrate; generating a group III element oxide gas; supplying the group III element oxide gas; supplying a nitrogen element-containing gas; supplying an oxidizing gas containing nitrogen element containing at least one selected from the group consisting of NO gas, NO2 gas, N2O gas, and N2O4 gas; and growing the group III nitride crystal on the seed substrate.
    Type: Grant
    Filed: June 28, 2021
    Date of Patent: October 24, 2023
    Assignees: OSAKA UNIVERSITY, PANASONIC HOLDINGS CORPORATION
    Inventors: Yusuke Mori, Masashi Yoshimura, Masayuki Imanishi, Akira Kitamoto, Junichi Takino, Tomoaki Sumi, Yoshio Okayama
  • Patent number: 11795572
    Abstract: A method of manufacturing a silicon carbide ingot, includes a preparing operation of adjusting internal space of a reactor in which silicon carbide raw materials and a seed crystal are disposed to have a high vacuum atmosphere, a proceeding operation of injecting an inert gas into the internal space, heating the internal space by moving a heater surrounding the reactor to induce the silicon carbide raw materials to sublimate, and growing the silicon carbide ingot on the seed crystal, and a cooling operation of cooling the temperature of the internal space to room temperature. The moving of the heater has a relative position which becomes more distant at a rate of 0.1 mm/hr to 0.48 mm/hr based on the seed crystal.
    Type: Grant
    Filed: May 25, 2021
    Date of Patent: October 24, 2023
    Assignee: SENIC INC.
    Inventors: Byung Kyu Jang, Jong Hwi Park, Eun Su Yang, Jung Woo Choi, Sang Ki Ko, Kap-Ryeol Ku, Jung-Gyu Kim
  • Patent number: 11795568
    Abstract: A production apparatus for a metal oxide single crystal according to one aspect of the present invention includes: a furnace having an interior heated to a temperature of 1,500° C. or more in an oxidative atmosphere, a heater heating the interior of the furnace, an inlet pipe being disposed in a lower part of the furnace and connecting an interior and an exterior of the furnace, an exhaust pipe being disposed in an upper part of the furnace and connecting an interior and an exterior of the furnace, a duct being disposed above the furnace, and an exhaust fan and a harmful substance elimination device being disposed in the middle of the duct.
    Type: Grant
    Filed: December 20, 2021
    Date of Patent: October 24, 2023
    Assignees: FUJIKOSHI MACHINERY CORP., SHINSHU UNIVERSITY
    Inventors: Keigo Hoshikawa, Toshinori Taishi, Takumi Kobayashi, Yoshio Otsuka, Etsuko Ohba
  • Patent number: 11761080
    Abstract: Aspects of the present disclosure generally relate to oscillating a boundary layer of a flow of process gas in methods and systems for processing substrates. In one aspect, one or more of a pressure, a gas flow rate, and/or a height of a substrate are oscillated during processing. In one implementation, a method of processing a substrate includes conducting a processing operation on the substrate in an interior volume of a processing chamber. The conducting the processing operation on the substrate includes moving a flow of one or more process gases over a surface of the substrate. The method also includes oscillating a boundary layer of the flow of one or more process gases while the flow of one or more process gases moves over the surface of the substrate.
    Type: Grant
    Filed: January 5, 2021
    Date of Patent: September 19, 2023
    Assignee: Applied Materials, Inc.
    Inventors: Tsung-Han Yang, Christopher S. Olsen
  • Patent number: 11753739
    Abstract: A method of manufacturing a group-III nitride crystal includes: preparing a seed substrate; and supplying a group-III element oxide gas and a nitrogen element-containing gas at a supersaturation ratio (Po/Pe) greater than 1 and equal to or less than 5, then, growing a group-III nitride crystal on the seed substrate, wherein the Po is a supply partial pressure of the group-III element oxide gas, and the Pe is an equilibrium partial pressure of the group-III element oxide gas.
    Type: Grant
    Filed: September 20, 2021
    Date of Patent: September 12, 2023
    Assignees: PANASONIC HOLDINGS CORPORATION, OSAKA UNIVERSITY
    Inventors: Yusuke Mori, Masashi Yoshimura, Masayuki Imanishi, Akira Kitamoto, Junichi Takino, Tomoaki Sumi
  • Patent number: 11756788
    Abstract: A method for fabricating a metastable crystalline structure is provided. The method includes providing a base substrate, wherein the base substrate comprises an insulating layer. The method further includes providing a metastable seed crystal on the base substrate, wherein the metastable seed crystal has a predefined metastable crystal phase or a predefined metastable composition. The method further includes forming a template structure above the base substrate, wherein the template structure covers at least a part of the metastable seed crystal. The method further includes growing the metastable crystalline structure with the predefined metastable crystal phase or the predefined metastable composition of the seed crystal inside the template structure. The growing of the metastable crystalline structure is nucleated from the seed crystal. Crystalline structures produced by the methods described herein are also provided.
    Type: Grant
    Filed: July 13, 2020
    Date of Patent: September 12, 2023
    Assignee: International Business Machines Corporation
    Inventors: Philipp Staudinger, Heinz Schmid
  • Patent number: 11746437
    Abstract: A method for making LNO film, including the steps of identifying a substrate, identifying a deposition target, placing the substrate and deposition target in a deposition environment, evolving target material into the deposition environment, and depositing evolved target material onto the substrate to yield an LNO film. The deposition environment defines a temperature of between 500 degrees Celsius and 750 degrees Celsius and a pressure of about 10?6 Torr. A seed or buffer layer may be first deposited onto the substrate, wherein the seed layer is about 30 mole percent gold and about 70 LiNbO3.
    Type: Grant
    Filed: December 20, 2021
    Date of Patent: September 5, 2023
    Assignee: Purdue Research Foundation
    Inventors: Haiyan Wang, Robynn-Lynne Paldi, Aleem Siddiqui
  • Patent number: 11746438
    Abstract: The present invention provides an optical ZnS material and a preparation method thereof, wherein the preparation method comprises: charging zinc and sulfur into a first crucible and a feeding device of a chemical vapor deposition furnace, respectively; heating the first crucible, the second crucible and a deposition chamber, and charging sulfur into the second crucible through the feeding device; introducing an inert carrier gas into the first crucible, and introducing an inert carrier gas and hydrogen into the second crucible, flowing the carrier gas containing zinc vapor and sulfur vapor respectively into the deposition chamber through pipelines to deposit ZnS, and supplying the second crucible with sulfur regularly and quantitatively through the feeding device during the deposition process to maintain a saturated vapor pressure of sulfur in a range of 0.8 to 1.8 KPa.
    Type: Grant
    Filed: December 10, 2021
    Date of Patent: September 5, 2023
    Assignees: Sinoma Synthetic Crystals Co., Ltd., Beijing Sinoma Synthetic Crystals Co., Ltd.
    Inventors: Xun Qian, Cunxin Huang, Hongtao Xiao, Xu Zhang, Kehong Zhang
  • Patent number: 11746415
    Abstract: The invention relates to a device (1) and method for applying a carbon layer, in particular a diamond layer, to a substrate (2, 2a) by means of chemical vapour deposition, comprising a deposition chamber (3) into which a process gas, in particular molecular hydrogen and/or a mixture of molecular hydrogen and a carbon-containing gas, such as methane can be supplied, wherein a gas inlet and gas activation element (7) is provided in the form of a hollow body with a flow channel (7b) for the process gas, a wall (7a) surrounding the flow channel (7b), and an outlet opening (16) feeding from the flow channel (7b) into the deposition chamber (3), and a heating device (8) is provided for heating the wall (7a) of the gas inlet and gas activation element (7).
    Type: Grant
    Filed: May 12, 2020
    Date of Patent: September 5, 2023
    Assignee: CARBONCOMPETENCE GMBH
    Inventors: Doris Steinmuller-Nethl, Detlef Steinmuller
  • Patent number: 11725303
    Abstract: Methods for purifying reaction precursors used in the synthesis of inorganic compounds and methods for synthesizing inorganic compounds from the purified precursors are provided. Also provided are methods for purifying the inorganic compounds and methods for crystallizing the inorganic compounds from a melt. ? and X-ray detectors incorporating the crystals of the inorganic compounds are also provided.
    Type: Grant
    Filed: June 8, 2021
    Date of Patent: August 15, 2023
    Assignee: Northwestern University
    Inventors: Mercouri G. Kanatzidis, Wenwen Lin
  • Patent number: 11718926
    Abstract: A method of single crystal growth includes disposing a polycrystalline source material in a chamber of a single crystal growth apparatus, disposing a seed layer in the chamber of the single crystal growth apparatus, wherein the seed layer is fixed below a lid of the single crystal growth apparatus, heating the polycrystalline source material by a heater of the single crystal growth apparatus to deposit a semiconductor material layer on the seed layer, and after depositing the semiconductor material layer, providing a coolant gas at a backside of the lid to cool down the seed layer and the semiconductor material layer.
    Type: Grant
    Filed: September 27, 2021
    Date of Patent: August 8, 2023
    Assignee: HON HAI PRECISION INDUSTRY CO., LTD.
    Inventor: Chung-Yi Chen
  • Patent number: 11718927
    Abstract: There is provided a method of manufacturing a crystal substrate, including: preparing a first crystal body which is a substrate comprising a single crystal of group III nitride produced by a vapor phase method and having a first main surface, and in which c-plane of the single crystal is curved in a concave spherical shape with a predetermined curvature; and growing a second crystal body comprising a single crystal of group III nitride on the first main surface, in a mixed melt containing an alkali metal and a group III element.
    Type: Grant
    Filed: March 14, 2019
    Date of Patent: August 8, 2023
    Assignee: SUMITOMO CHEMICAL COMPANY, LIMITED
    Inventors: Takehiro Yoshida, Masatomo Shibata, Seiji Sarayama, Takashi Sato, Naoya Miyoshi, Akishige Murakami
  • Patent number: 11708646
    Abstract: A silicon carbide single crystal manufacturing apparatus includes a crucible constituted by a crucible body and a crucible lid and a base having a crucible lid side surface supported by the lower surface of the crucible lid, and a seed crystal mounting surface on which the seed crystal is mounted and which is a surface on the opposite side of the crucible lid side surface, wherein the base is made of graphite material, the area of the seed crystal mounting surface is larger than the area of the crucible lid side surface, and the base has at least of a portion in which the cross-sectional area orthogonal to the vertical direction connecting the crucible lid side surface and the seed crystal mounting surface is gradually reduced, and a portion that is getting smaller gradually, from the surface of the seed crystal mounting surface toward the crucible lid side surface.
    Type: Grant
    Filed: December 27, 2021
    Date of Patent: July 25, 2023
    Assignee: SHOWA DENKO K.K.
    Inventor: Rimpei Kindaichi