Patents by Inventor Malika Boualleg

Malika Boualleg has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 11951456
    Abstract: A process for preparing a catalyst for the hydrogenation of aromatic or polyaromatic compounds comprising nickel, copper and a support comprising at least one refractory oxide, comprising the following steps: bringing the support into contact with a solution containing at least one copper precursor and one nickel precursor; drying the catalyst precursor at a temperature of less than 250° C.; reducing the catalyst precursor by bringing said precursor into contact with a reducing gas at a temperature of between 150° C. and 250° C.; bringing the catalyst precursor into contact with a solution comprising a nickel precursor; a step of drying the catalyst precursor at a temperature of less than 250° C.; reducing the catalyst precursor by bringing said precursor into contact with a reducing gas at a temperature of between 150° C. and 250° C.
    Type: Grant
    Filed: January 8, 2020
    Date of Patent: April 9, 2024
    Assignee: IFP ENERGIES NOUVELLES
    Inventors: Malika Boualleg, Anne-Agathe Quoineaud
  • Patent number: 11779915
    Abstract: A process for preparing a selective hydrogenation catalyst comprising nickel, copper and a support comprising at least one refractory oxide, comprising the following steps: bringing the support into contact with a solution containing at least one copper precursor and one nickel precursor; drying the catalyst precursor at a temperature of less than 250° C.; reducing the catalyst precursor by bringing said precursor into contact with a reducing gas at a temperature of between 150° C. and 250° C.; bringing the catalyst precursor into contact with a solution comprising a nickel precursor; a step of drying the catalyst precursor at a temperature of less than 250° C.; reducing the catalyst precursor by bringing said precursor into contact with a reducing gas at a temperature of between 150° C. and 250° C.
    Type: Grant
    Filed: January 8, 2020
    Date of Patent: October 10, 2023
    Assignee: IFP Energies nouvelles
    Inventors: Malika Boualleg, Anne-Agathe Quoineaud
  • Publication number: 20230201809
    Abstract: A process for preparing a catalyst comprising nickel and copper, comprising the following steps: impregnating the porous support with a volume of a butanol solution of between 0.2 and 0.8 times the total pore volume of the support; maturing the impregnated porous support for 0.5 to 40 hours; impregnating the matured impregnated support with a solution comprising a precursor of the nickel active phase; impregnating the support with a solution containing a copper precursor and a nickel precursor.
    Type: Application
    Filed: May 18, 2021
    Publication date: June 29, 2023
    Applicant: IFP Energies nouvelles
    Inventor: Malika BOUALLEG
  • Publication number: 20230191387
    Abstract: A process for preparing a catalyst comprising an active phase based on nickel and an alumina support, which process comprises the following steps: a) said support is impregnated with a volume V1 of a butanol solution of between 0.2 and 0.8 times the total pore volume TPV of said support in order to obtain an impregnated support; b) the impregnated support obtained at the end of step a) is left to mature for 0.5 to 40 hours; c) the matured impregnated support obtained at the end of step b) is impregnated with a solution comprising at least one precursor of the nickel active phase in order to obtain a catalyst precursor; d) the catalyst precursor obtained at the end of step c) is dried at a temperature below 250° C.
    Type: Application
    Filed: May 18, 2021
    Publication date: June 22, 2023
    Applicant: IFP Energies nouvelles
    Inventor: Malika BOUALLEG
  • Publication number: 20230129143
    Abstract: Catalyst for the hydrogenation of aromatic compounds capable of being obtained by the process comprising at least the following stages: a) the alumina support is brought into contact with at least one organic additive; b) the alumina support is brought into contact with at least one nickel metal salt, the melting point of said metal salt of which is between 20° C. and 150° C.; c) the solid mixture obtained on conclusion of stages a) and b) is heated with stirring; d) the catalyst precursor obtained on conclusion of stage c) is dried; e) a stage of heat treatment of the dried catalyst precursor obtained on conclusion of stage d) is carried out.
    Type: Application
    Filed: December 4, 2020
    Publication date: April 27, 2023
    Applicant: IFP Energies nouvelles
    Inventors: Malika BOUALLEG, Laetitia JOTHIE
  • Publication number: 20230047217
    Abstract: A selective hydrogenation catalyst that can be obtained by the process comprising at least the following steps: a) the alumina support is brought into contact with at least one organic additive; b) the alumina support is brought into contact with at least one nickel metal salt, the melting point of said metal salt of which is between 20° C. and 150° C.; c) the solid mixture obtained on conclusion of steps a) and b) is heated with stirring; d) the catalyst precursor on conclusion of step c) is dried; e) a step of heat treatment of the dried catalyst precursor obtained on conclusion of step d) is carried out.
    Type: Application
    Filed: December 4, 2020
    Publication date: February 16, 2023
    Applicant: IFP Energies nouvelles
    Inventors: Malika BOUALLEG, Laetitia JOTHIE
  • Patent number: 11577964
    Abstract: Process for preparing alumina gel in a single precipitation step consisting of dissolving an aluminium precursor, aluminium chloride, in water, at a temperature of 10° C. to 90° C. such that the pH of the solution is from 0.5 to 5, for a period of 2 to 60 minutes, then adjusting the pH to 7.5 to 9.5 by adding a basic precursor, sodium hydroxide, to the solution obtained to obtain a suspension, at a temperature of 5° C. to 35° C., and for 5 minutes to 5 hours, followed by a filtration step, said process not comprising any washing steps. Also, novel alumina gel having a high dispersibility index, in particular a dispersibility index of more than 80%, a crystallite dimension of 0.5 to 10 nm, a chlorine content of 0.001% to 2% by weight and a sodium content of 0.001% to 2% by weight, the percentages by weight being expressed with respect to the total weight of the alumina gel.
    Type: Grant
    Filed: September 3, 2020
    Date of Patent: February 14, 2023
    Assignee: IFP Energies Nouvelles
    Inventors: Malika Boualleg, Olivier Lafon
  • Patent number: 11554358
    Abstract: The present invention relates to the field of solid materials for the adsorption of lithium. In particular, the present invention relates to a novel process for preparing a solid crystalline material formed preferably in extrudate form, of formula (LiCl)x.2Al(OH)3,nH2O with n being between 0.01 and 10, x being between 0.4 and 1, comprising a step a) to precipitate boehmite under specific conditions of temperature and pH, a step to place the precipitate obtained in contact with a specific quantity of LiCl, at least one forming step preferably via extrusion, said process also comprising a final hydrothermal treatment step, all allowing an increase in lithium adsorption capacity and in the adsorption kinetics of the materials obtained compared to prior art materials, when used in a process to extract lithium from saline solutions.
    Type: Grant
    Filed: May 23, 2017
    Date of Patent: January 17, 2023
    Assignees: ERAMET, IFP ENERGIES NOUVELLES
    Inventors: Malika Boualleg, Fabien Burdet, Yohan Florent Oudart
  • Publication number: 20220314206
    Abstract: Catalyst comprising a nickel-based active phase and an alumina support, characterized in that: the nickel is distributed both on a crust at the periphery of the support, and in the core of the support, the thickness of said crust being between 2% and 15% of the diameter of the catalyst; the nickel density ratio between the crust and the core is strictly greater than 3; said crust comprises between 40% and 80% by weight of nickel element relative to the total weight of nickel contained in the catalyst; the size of the nickel particles in the catalyst is less than 7 nm.
    Type: Application
    Filed: July 16, 2020
    Publication date: October 6, 2022
    Applicant: IFP Energies Nouvelles
    Inventors: Anne-Claire DUBREUIL, Vincent COUPARD, Malika BOUALLEG
  • Publication number: 20220288569
    Abstract: Catalyst comprising a nickel-based active phase and an alumina support, characterized in that: the nickel is distributed both on a crust at the periphery of the support, and in the core of the support, the thickness of said crust being between 2% and 15% of the diameter of the catalyst; the nickel density ratio between the crust and the core is strictly greater than 3; said crust comprises between 40% and 80% by weight of nickel element relative to the total weight of nickel contained in the catalyst.
    Type: Application
    Filed: July 16, 2020
    Publication date: September 15, 2022
    Applicant: IFP Energies Nouvelles
    Inventors: Anne-Claire DUBREUIL, Vincent COUPARD, Malika BOUALLEG, Carine CHOLLET, Alexandre JOUVE
  • Publication number: 20220280922
    Abstract: Catalyst comprising nickel and copper, in a proportion of 1% to 50% by weight of nickel element relative to the total weight of the catalyst, in a proportion of 0.5% to 15% by weight of copper element relative to the total weight of the catalyst, and an alumina support, said catalyst being characterized in that: the mole ratio between nickel and copper is between 0.5 and 5 mol/mol; at least one portion of the nickel and copper is in the form of a nickel-copper alloy; the nickel content in the nickel-copper alloy is between 0.5% and 15% by weight of nickel element relative to the total weight of the catalyst, the size of the nickel particles in the catalyst is less than 7 nm.
    Type: Application
    Filed: July 16, 2020
    Publication date: September 8, 2022
    Applicant: IFP Energies Nouvelles
    Inventors: Anne-Claire DUBREUIL, Malika BOUALLEG
  • Publication number: 20220266225
    Abstract: Nickel and copper catalyst, and an alumina support: nickel distributed both in the core of and on a crust at the periphery of the support, crust thickness being 2% to 15% of catalyst diameter; nickel density ratio between the crust and the core greater than 3; crust contains more than 25% by weight of nickel element relative to total weight of nickel in the catalyst; mole ratio between nickel and copper is 0.5 to 5, at least one portion of nickel and copper is a nickel-copper alloy; nickel content in the nickel-copper alloy is 0.5% to 15% by weight of nickel element relative to total weight of the catalyst; size of the nickel particles in the catalyst is less than 7 nm.
    Type: Application
    Filed: July 16, 2020
    Publication date: August 25, 2022
    Applicant: IFP Energies nouvelles
    Inventors: Anne-Claire DUBREUIL, Malika BOUALLEG
  • Publication number: 20220250041
    Abstract: Catalyst comprising nickel and sulfur on an alumina support, said catalyst being characterized in that: the nickel is distributed both on a crust at the periphery of the support, and in the core of the support, the thickness of said crust being between 2% and 15% of the diameter of the catalyst; the nickel density ratio between the crust and the core is strictly greater than 3; said crust comprises more than 25% by weight of nickel element relative to the total weight of nickel contained in the catalyst, the size of the nickel particles in the catalyst, measured in oxide form, is between 7 and 25 nm.
    Type: Application
    Filed: July 16, 2020
    Publication date: August 11, 2022
    Applicant: IFP Energies nouvelles
    Inventors: Anne-Claire DUBREUIL, Vincent COUPARD, Malika BOUALLEG
  • Patent number: 11370976
    Abstract: Process for hydrogenating at least one aromatic or polyaromatic compound contained in a hydrocarbon feedstock having a final boiling point of less than or equal to 650° C., said process being performed in the gas phase or in the liquid phase at a temperature of between 30 and 350° C., at a pressure of between 0.1 and 20 MPa, at a hydrogen/(aromatic compounds to be hydrogenated) mole ratio of between 0.1 and 10 and at an hourly space velocity (HSV) of between 0.05 and 50 h?1, in the presence of a catalyst comprising an active phase comprising nickel, said active phase not comprising any group VIB metal, and a support comprising an amorphous mesoporous alumina having a connectivity (Z) of greater than 2.7, the connectivity being determined from the nitrogen adsorption/desorption isotherms.
    Type: Grant
    Filed: June 13, 2018
    Date of Patent: June 28, 2022
    Assignee: IFP Energies Nouvelles
    Inventors: Malika Boualleg, Anne-Claire Dubreuil
  • Patent number: 11364490
    Abstract: Method for preparing a catalyst comprising a bimetallic active phase made of nickel and copper, and a support comprising a refractory oxide, comprising the following steps: a step of bringing the support into contact with a solution containing a nickel precursor is carried out; a step of bringing the support into contact with a solution containing a copper precursor is carried out; a step of drying the catalyst precursor at a temperature lower than 250° C. is carried out; the catalyst precursor obtained is supplied to a hydrogenation reactor, and a step of reduction by bringing said precursor into contact with a reducing gas at a temperature lower than 200° C. for a period greater than or equal to 5 minutes and less than 2 hours is carried out.
    Type: Grant
    Filed: April 5, 2019
    Date of Patent: June 21, 2022
    Assignee: IFP Energies Nouvelles
    Inventors: Malika Boualleg, Anne-Agathe Quoineaud
  • Patent number: 11338279
    Abstract: A method for preparing a catalyst with a bimetallic active phase made of nickel and copper, and a support comprising a refractory oxide, wherein the method involves: a) placing the support in contact with at least one solution containing a nickel precursor; b) placing the support in contact with a solution containing a copper precursor; wherein a) and b) are carried out separately in any order; c) drying the catalyst precursor at the end of a) and b), or b) and a), at a temperature less than 250° C.; and d) supplying the catalyst precursor obtained at the end of c), into a hydrogenation reactor, and carrying out a reduction step by placing the precursor in contact with a reducing gas at a temperature of less than 200° C. and for a period greater than or equal to 5 minutes and less than 2 hours.
    Type: Grant
    Filed: April 5, 2019
    Date of Patent: May 24, 2022
    Assignee: IFP Energies nouvelles
    Inventors: Malika Boualleg, Anne-Agathe Quoineaud
  • Publication number: 20220072516
    Abstract: A process for preparing a catalyst for the hydrogenation of aromatic or polyaromatic compounds comprising nickel, copper and a support comprising at least one refractory oxide, comprising the following steps: bringing the support into contact with a solution containing at least one copper precursor and one nickel precursor; drying the catalyst precursor at a temperature of less than 250° C.; reducing the catalyst precursor by bringing said precursor into contact with a reducing gas at a temperature of between 150° C. and 250° C.; bringing the catalyst precursor into contact with a solution comprising a nickel precursor; a step of drying the catalyst precursor at a temperature of less than 250° C.; reducing the catalyst precursor by bringing said precursor into contact with a reducing gas at a temperature of between 150° C. and 250° C.
    Type: Application
    Filed: January 8, 2020
    Publication date: March 10, 2022
    Applicant: IFP Energies Nouvelles
    Inventors: Malika BOUALLEG, Anne-Agathe QUOINEAUD
  • Publication number: 20220062886
    Abstract: A process for preparing a selective hydrogenation catalyst comprising nickel, copper and a support comprising at least one refractory oxide, comprising the following steps: bringing the support into contact with a solution containing at least one copper precursor and one nickel precursor; drying the catalyst precursor at a temperature of less than 250° C.; reducing the catalyst precursor by bringing said precursor into contact with a reducing gas at a temperature of between 150° C. and 250° C.; bringing the catalyst precursor into contact with a solution comprising a nickel precursor; a step of drying the catalyst precursor at a temperature of less than 250° C.; reducing the catalyst precursor by bringing said precursor into contact with a reducing gas at a temperature of between 150° C. and 250° C.
    Type: Application
    Filed: January 8, 2020
    Publication date: March 3, 2022
    Applicant: IFP Energies nouvelles
    Inventors: Malika BOUALLEG, Anne-Agathe QUOINEAUD
  • Publication number: 20210154654
    Abstract: A method for preparing a catalyst with a bimetallic active phase made of nickel and copper, and a support comprising a refractory oxide, wherein the method involves: a) placing the support in contact with at least one solution containing a nickel precursor; b) placing the support in contact with a solution containing a copper precursor; wherein a) and b) are carried out separately in any order; c) drying the catalyst precursor at the end of a) and b), or b) and a), at a temperature less than 250° C.; and d) supplying the catalyst precursor obtained at the end of c), into a hydrogenation reactor, and carrying out a reduction step by placing the precursor in contact with a reducing gas at a temperature of less than 200° C. and for a period greater than or equal to 5 minutes and less than 2 hours.
    Type: Application
    Filed: April 5, 2019
    Publication date: May 27, 2021
    Applicant: IFP Energies nouvelles
    Inventors: Malika BOUALLEG, Anne-Agathe QUOINEAUD
  • Publication number: 20210154653
    Abstract: Method for preparing a catalyst comprising a bimetallic active phase made of nickel and copper, and a support comprising a refractory oxide, comprising the following steps: a step of bringing the support into contact with a solution containing a nickel precursor is carried out; a step of bringing the support into contact with a solution containing a copper precursor is carried out; a step of drying the catalyst precursor at a temperature lower than 250° C. is carried out; the catalyst precursor obtained is supplied to a hydrogenation reactor, and a step of reduction by bringing said precursor into contact with a reducing gas at a temperature lower than 200° C. for a period greater than or equal to 5 minutes and less than 2 hours is carried out.
    Type: Application
    Filed: April 5, 2019
    Publication date: May 27, 2021
    Applicant: IFP Energies Nouvelles
    Inventors: Malika BOUALLEG, Anne-Agathe QUOINEAUD