Abstract: LMFP cathode materials are made in a mechanochemical/solid state process. The precursors are dried in a preliminary step to reduce the water content of the precursors of less than 1% by weight and preferably less than 0.25% by weight. The dried precursors are then dry milled and calcined to form particles of an olivine LMFP. The product has excellent specific capacity and capacity retention.

Abstract: The present invention relates to a continuous-feed furnace assembly and processes for preparing and continuously thermally exfoliating graphite oxide to give a highly exfoliated graphite.

Abstract: A method for processing a thermoplastic material that comprises a microwave-sensitive polymeric region, wherein the method includes exposing the microwave-sensitive polymeric region to microwaves; wherein the exposing results in an increase in the temperature of the polymeric region; and processing the thermoplastic material is disclosed.

Abstract: The present invention relates to a nitrate salt-based process for preparing a graphite oxide. The invention nitrate salt-based process employs starting materials comprising a sulfuric acid, an inorganic nitrate salt, an amount of water, a first amount of chlorate salt, and a graphite.

Abstract: The present invention relates to a nitrate salt-based process for preparing a graphite oxide. The invention nitrate salt-based process employs starting materials comprising a sulfuric acid, an inorganic nitrate salt, an amount of water, a first amount of chlorate salt, and a graphite.

Abstract: The present invention relates to a nitrate salt-based process for preparing a graphite oxide. The invention nitrate salt-based process employs starting materials comprising a sulfuric acid, an inorganic nitrate salt, an amount of water, a first amount of chlorate salt, and a graphite.

Abstract: The present invention relates to a process for preparing a graphite oxide while purging chlorine dioxide. The invention process employs starting materials comprising a sulfuric acid, a nitric acid, a chlorate salt, and a graphite and further employs an inert purge gas.

Abstract: A two step method for preparing a filler composition, the filler composition useful to prepare a nanocomposite polymer and an epoxy nanocomposite coating. First, disperse a water dispersible filler material in a liquid comprising water, but without any added intercalation agent, to form a dispersion. Second, replace at least a portion of the water of the liquid with an organic solvent so that the water concentration of the liquid is less than six percent by weight to form the filler composition, the average size of at least one dimension of the filler material being less than two hundred nanometers upon examination by transmission electron microscopy of a representative freeze dried sample of the dispersion of the first step. A nanocomposite polymer can be prepared by mixing the filler composition with one or more polymer, polymer component, monomer or prepolymer to produce a polymer containing the filler composition.

Abstract: A microwave-sensitive thermoplastic composition that includes a microwave-receptive additive; and a thermoplastic polymer; wherein the microwave-receptive additive is selected from the group consisting of sepiolite clay, molecular sieves formed from ammonium ion salts or hydrogen ion salts, aluminophosphates, silicoaluminophasphates, silicotitanates, organo-modified clays, molecular sieves or zeolites having a caged organic microwave receptive material, and combinations thereof.

Abstract: The instant invention generally provides polymer pi-bond-philic filler composite comprising a molecularly self-assembling material and a pi-bond-philic filler, and a process of making and an article comprising the polymer pi-bond-philic filler composite. The instant invention also generally provides a process of separating a pi-bond-philic gas from a separable gas mixture comprising the pi-bond-philic gas.

Abstract: A process for preparing oxidized graphite that provides exfoliated graphene, preferably with high surface area. The process uses considerably less chlorate than previously known systems.

Abstract: A two step method for preparing a filler composition, the filler composition useful to prepare a nanocomposite polymer and an epoxy nanocomposite coating. First, disperse a water dispersible filler material in a liquid comprising water, but without any added intercalation agent, to form a dispersion. Second, replace at least a portion of the water of the liquid with an organic solvent so that the water concentration of the liquid is less than six percent by weight to form the filler composition, the average size of at least one dimension of the filler material being less than two hundred nanometers upon examination by transmission electron microscopy of a representative freeze dried sample of the dispersion of the first step. A nanocomposite polymer can be prepared by mixing the filler composition with one or more polymer, polymer component, monomer or prepolymer to produce a polymer containing the filler composition.

Abstract: A method for preparing a filler composition useful for preparing a nanocomposite polymer is provided. The method includes a first step of dispersing a water dispersible filler material in a liquid comprising water to form a dispersion and a second step of replacing at least a portion of the water of the liquid with an organic solvent. The resulting filler composition features a water concentration of the liquid of less than six percent by weight, and the average size of at least one dimension of the filler material is less than two hundred nanometers upon examination by transmission electron microscopy of a representative freeze dried sample of the dispersion of the first step. A nanocomposite polymer, particularly and epoxy resin composition, can be prepared by mixing the above-made filler composition with one or more polymer, polymer component, monomer or prepolymer.

Abstract: The present invention relates to a nitrate salt-based process for preparing a graphite oxide. The invention nitrate salt-based process employs starting materials comprising a sulfuric acid, an inorganic nitrate salt, an amount of water, a first amount of chlorate salt, and a graphite.

Abstract: The present invention relates to a process for preparing a graphite oxide while purging chlorine dioxide. The invention process employs starting materials comprising a sulfuric acid, a nitric acid, a chlorate salt, and a graphite and further employs an inert purge gas.

Abstract: A microwave-sensitive thermoplastic composition that includes a microwave-receptive additive; and a thermoplastic polymer; wherein the microwave-receptive additive is selected from the group consisting of sepiolite clay, molecular sieves formed from ammonium ion salts or hydrogen ion salts, aluminophosphates, silicoaluminophasphates, silicotitanates, organo-modified clays, molecular sieves or zeolites having a caged organic microwave receptive material, and combinations thereof.

Abstract: The polymer composition is a flame retardant composition comprising an organic polymer and nanographene. Suitable organic polymers include polymers such as polyolefins and polyvinyl chloride. Preferably, the nanographene should have an aspect ratio greater than equal to about 1000:1, should have a surface area greater than or equal to about 100 m2/gram nitrogen surface absorption area, and be expanded.

Abstract: A process for preparing oxidized graphite that provides exfoliated graphene, preferably with high surface area. The process uses considerably less chlorate than previously known systems.

Abstract: The present invention relates to a continuous-feed furnace assembly and processes for preparing and continuously thermally exfoliating graphite oxide to give a highly exfoliated graphite.

Abstract: A method of formulating a microwave-heatable thermoplastic composition designed to have a selected heating rate. The method may include: selecting at least one of a microwave receptive additive, a microwave receptive additive particle size, and a concentration of the microwave receptive additive; selecting at least two inputs selected from the group consisting of a thermoplastic polymer composition, a microwave power, an electric field strength, a maximum allowable temperature of the thermoplastic polymer composition, a processing temperature of the thermoplastic polymer composition, and a thermal diffusivity of the thermoplastic polymer composition; and mixing a microwave receptive additive with a thermoplastic polymer to form the microwave-heatable thermoplastic composition having a selected heating rate based on the selecting at least one and the selecting at least two.