NON-COMBUSTION HEATING TYPE FLAVOR INHALATION ARTICLE, AND NON-COMBUSTION HEATING TYPE FLAVOR INHALATION SYSTEM
A non-combustion heating type flavor inhalation article includes: an aerosol-generating segment; and a mouthpiece segment adjacent to the aerosol-generating segment. The mouthpiece segment includes a filter material, and a breakable capsule within the filter material, the breakable capsule having a single-layered core-shell structure. The capsule is spherical or approximately spherical with a diameter of 3.0 mm to 4.5 mm. The capsule has a stress of 2 N or more and 6 N or less against a displacement of 0.5 mm within 4 minutes from 10 minutes of storage under a condition of 45° C. and 90% RH.
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The present invention contains subject matter related to PCT Application No. PCT/JP2023/029756, filed Aug. 17, 2023, and based upon and claiming the benefit of priority from prior Japanese Patent Application No. 2022-138385, filed Aug. 31, 2022, the entire contents of each are incorporated herein by reference.
FIELDThe present invention relates to a non-combustion heating type flavor inhalation article and a non-combustion heating type flavor inhalation system.
BACKGROUNDA non-combustion heating type flavor inhalation article, which is used with heat generated by an electric heater or the like without combustion, is known.
It is also known that a flavorant-enclosing breakable capsule (c.f., for example, WO 2014/171433) is set within the filter material of a combustion type flavor inhalation article such as a cigarette (c.f., for example, WO 2018/011660). A user breaks the capsule by crushing it with fingers or teeth from outside the filter material so as to cause the flavorant in the capsule to be released into the filter material, thereby making the flavor during the inhalation changeable upon breakage of the capsule.
It has become recognized that a non-combustion heating type flavor inhalation article shows, for example, the following characteristics with inhalation by a user, which constitute differences from a combustion type flavor inhalation article such as a cigarette.
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- A vaporized flavor component which moves from the aerosol-generating segment to the downstream segment during use (during the inhalation) has a high temperature.
- Water vapor accounts for a large proportion among all vaporized components.
As such, in response to inhalation by a user, the inside of the filter material of a non-combustion heating type flavor inhalation article becomes hot and humid. For a combustion type flavor inhalation article in which a capsule is provided inside the filter material, inhalation by a user easily creates a high-temperature and high-humidity condition around the capsule. From the above, it is presumed that a capsule within the filter material of a non-combustion heating type flavor inhalation article can be easily softened in response to inhalation by a user.
In instances where a user of the non-combustion heating type flavor inhalation article that has been subjected to at least one inhalation action is to break a capsule, this capsule, which has been softened, may give the user a misperception that there is no capsule in the filter material or an already broken capsule is contained.
Note that it is generally very likely that a multi-layered capsule will incur a higher cost than a single-layered capsule.
SUMMARYAccording to one embodiment of the present invention, a non-combustion heating type flavor inhalation article includes: an aerosol-generating segment; and a mouthpiece segment adjacent to the aerosol-generating segment. The mouthpiece segment includes a filter material, and a breakable capsule within the filter material. The breakable capsule has a single-layered core-shell structure. The capsule is spherical or approximately spherical with a diameter of 3.0 mm to 4.5 mm. The capsule has a stress of 2 N or more and 6 N or less against a displacement of 0.5 mm within 4 minutes from 10 minutes of storage under a condition of 45° C. and 90% RH.
As shown in
The non-combustion heating type flavor inhalation system 10 includes a heater 12 and a rod (non-combustion heating type flavor inhalation article) 14 adapted to be attached to and detached from an insertion part 42 of the heater 12. The heater 12 is intended for repeated use and the rod 14 is discarded after one use.
The heater 12 includes a box-shaped housing 22, a battery unit (e.g., a secondary battery) 24, a switch 26 for activating the heater 12, a pressure sensing part 28, a heat transfer part (heat transfer tube) 30, a heater element 32 provided around the heat transfer part 30, and a controller 34.
The housing 22 includes the insertion part 42 and a vent hole 44. The insertion part 42 is formed into a cylindrically recessed shape corresponding to the shape of the rod 14. The vent hole 44 permits communication between the outside of the housing 22 and the insertion part 42, and supplies air to the rod 14 inserted into the insertion part 42.
The housing 22 is provided with the battery unit 24, the switch 26, the pressure sensing part 28, the heat transfer part (heat transfer tube) 30, the heater element 32 provided around the heat transfer part 30, and the controller 34.
In one example, the battery unit 24 is formed as a secondary battery assembly which includes a secondary battery or a combination of multiple secondary batteries. The battery unit 24 supplies electric power to, for example, the pressure sensing part 28, the heater element 32, the controller 34, and so on.
The switch 26 is exposed to the outside of the housing 22 and is arranged at a position next to the insertion hole of the insertion part 42.
The pressure sensing part 28 is constituted by, for example, a pressure sensor (pressure sensitive sensor), and it is in one example provided within the insertion part 42 (within the vent hole 44).
The heat transfer part 30 is made of a metal material and formed into a hollow cylindrical shape. The metal material for the heat transfer part 30 is preferably a metal having a high thermal conductivity, such as gold, silver, copper, aluminum, or an alloy using one or more of these metals.
In one example, the heater element 32 is constituted by a general heating wire such as a nichrome wire. The heater element 32 is arranged, for example, cylindrically around the heat transfer part 30. Note that the heating mode adopted by the heater element 32 is not limited to the mode that utilizes Joule heat from electrical resistance, and it may adopt, for example, an induction heating (IH) mode or a mode utilizing a chemical reaction that produces oxidation heat, etc. For adopting the IH mode, the filler 62 in an aerosol-generating segment 52 is covered by, for example, a magnetic metal thin film. For adopting a mode utilizing a chemical reaction, the material and the shape of the heat transfer part may be selected. The heater element 32 in such cases is also capable of heating the aerosol-generating segment 52 without burning it.
The controller 34 receives a supply of power from the battery unit 24 and controls the switch 26, the pressure sensing part 28, the heater element 32, etc. The controller 34 controls the pressure sensing part 28 to sense whether or not the rod 14 has been properly inserted into the insertion part 42 and to further sense the negative pressure in the insertion part 42 (in the vent hole 44). Accordingly, the controller 34 may take control so that power is not supplied to the heater element 32 if the rod 14 has not been properly inserted into the insertion part 42. The controller 34 may also count the number of inhalation actions by the user. The controller 34 causes the power from the battery unit 24 to be supplied to the heater element 32 to adjust the temperature of the heater element 32 within an appropriate range. The controller 34 controls the heater element 32 to heat the later-described aerosol-generating segment 52 of the rod 14 at, for example, 30° C. to 400° C., or preferably 100° C. to 400° C., or more preferably 150° C. to 250° C.
In one example, the rod (non-combustion heating type flavor inhalation article) 14 shown in
The circumferential length of the rod 14 is not particularly limited, but in one example it is preferably 16 mm to 25 mm, or more preferably 21 mm to 23 mm. The overall length (horizontal length) of the rod 14 is not particularly limited, but in one example it is preferably 50 mm to 100 mm, or more preferably 50 mm to 70 mm.
The rod 14 includes the aerosol-generating segment (tobacco part) 52, a mouthpiece segment 54, and tipping paper (mouthpiece lining paper) 56.
In one example, the aerosol-generating segment 52 includes a tobacco-containing filler 62 and a wrapper 64 made of paper which, for example, cylindrically wraps the filler 62.
The tobacco-containing filler 62 is formed of dried leaf tobacco or a sheet-shaped crushed tobacco plant cut into approximately 1 mm×3 mm pieces to fill in random orientations. The filler 62 may contain, for example, 0 wt % to 30 wt % of an aerosol source (glycerin, propylene glycol (PG), 1,3-butanediol), and a flavoring material.
The mouthpiece segment 54 according to this embodiment includes a first segment 72, a second segment 74, a third segment 76, a capsule 78, and a wrapper 80.
The first segment 72 is formed of a cardboard (thickness: 200 μm to 500 μm) processed into a cylindrical paper tube. The cardboard may be paper made of a wood pulp raw material, such as ordinary paper, or may be a sheet made of a plasticizer (triacetin)-treated and compressed cellulose acetate fiber.
The second segment 74 includes a hollow rod 82 and an inner plug wrapper 84. The hollow rod 82 is formed by, for example, densely filling cellulose acetate fibers with a hollow center. The inner plug wrapper 84 is constituted mainly by paper and wraps the outer periphery of the hollow rod 82. The cellulose acetate-filled layer has a high density. Accordingly, air and aerosol during inhalation (smoking) flow through the hollow portion inside the hollow rod 82 and do not easily flow into the fiber-filled layer.
Note that the rod 82 may be formed with a solid center, instead of having a hollow structure.
The cellulose acetate fibers of the hollow rod 82 in the second segment 74 are cured upon addition of, for example, 6 mass % to 20 mass % of a suitable plasticizer including triacetin or the like with respect to the mass of the cellulose acetate. The hollow portion of the second segment 74 has an inner diameter of, for example, 1.0 mm to 5.0 mm.
The third segment 76 includes a solid rod (filter material) 92 and an inner plug wrapper 94. The solid rod 92 is provided by filling, for example, cellulose acetate fibers at an appropriate density. The inner plug wrapper 94 is constituted mainly by paper and wraps the outer periphery of the solid rod 92.
Note that the solid rod 92 in the third segment 76 may be formed at the same filling density as that of the cellulose acetate fibers of the hollow rod 82 in the second segment 74, or may be formed at a different filling density. Also, the cellulose acetate fibers of the solid rod 92 in the third segment 76 preferably contain, for example, a suitable plasticizer including triacetin or the like as in the hollow rod 82 in the second segment 74.
Here, the long fibers of cellulose acetate that have been plasticized by the plasticizer preferably have a filament denier of 3.0 dpf (denier per filament) or more and 12.0 dpf or less. Also, the long fibers of cellulose acetate that have been plasticized by the plasticizer preferably have a filling density of 130 [mg/cc] or less. Further, the long fibers of cellulose acetate that have been plasticized by the plasticizer preferably have a filling density of 100 [mg/cc] or more. Setting the filling density of the cellulose acetate long fibers plasticized by the plasticizer in such a range can facilitate the fixing of the capsule 78 in the right position and also prevent the capsule 78 from easily popping out at the time of pressing a later-described cutout segment 98.
In this embodiment, the capsule 78 is arranged within the solid rod 92 in the third segment 76. It is not a limitation to arrange the capsule 78 within the third segment 76 but the capsule 78 may also be arranged within the first segment 72 or the second segment 74. It is also possible to arrange the capsule 78 in, for example, the third segment 76 and at least one of the first segment 72 and the second segment 74. As such, one or more capsules 78 may be disposed in the single mouthpiece segment 54.
In one example, the capsule 78 includes a shell and a content liquid containing a flavorant. For the present embodiment, it is preferable to constitute the capsule 78 from a shell and a content liquid within the shell. The shell may employ, for example, any of starch, dextrin, polysaccharide, agar, gellan gum, gelatin, various natural gelling agents, glycerin, sorbitol, calcium chloride, etc., and may further contain a flavorant and a coloring agent. The capsule 78 may be colored so that the user can recognize the capsule 78 so as to crush it even if it is enclosed within the inner plug wrapper 94 and the tipping paper 56 which are not transparent. In such a form, the shell preferably contains a coloring agent, such as Blue No. 1.
As the flavorant of the content liquid, any flavorant for a smoking article such as menthol, plant essential oil, etc. may be used. Typical examples of the flavorant include: menthol; leaf tobacco extract; natural plant flavors (e.g., cinnamon, sage, herb, chamomile, kudzu (Pueraria lobata), sweet hydrangea leaf, clove, lavender, cardamom, caryophyllus, nutmeg, bergamot, geranium, honey essence, rose oil, lemon, orange, cassia bark, caraway, jasmine, ginger, coriander, vanilla extract, spearmint, peppermint, cassia, coffee, celery, cascarilla, sandalwood, cocoa, ylang-ylang, fennel, anise, licorice, St John's bread, prune extract, and peach extract); saccharides (e.g., glucose, fructose, isomerized saccharide, and caramel); cocoa (e.g., powder and extract); esters (e.g., isoamyl acetate, linalyl acetate, isoamyl propionate, and linalyl butyrate); ketones (e.g., menthone, ionone, damascenone, and ethyl maltol); alcohols (e.g., geraniol, linalool, anethole, and eugenol); aldehydes (e.g., vanillin, benzaldehyde, and anisaldehyde); lactones (e.g., γ-undecalactone and γ-nonalactone); animal flavorants (e.g., musk, ambergris, civet, and castoreum); and hydrocarbons (e.g., limonene and pinene). Each of these flavorants may be used alone, or the flavorants may be used in any combination.
As a solvent of the content liquid, any solvent suitable for a flavorant may be used, and examples of such a solvent include medium chain fatty acid triglyceride (MCT) (more specifically, tricaprylic/capric acid glycerin), propylene glycol, water, and ethanol. The content liquid may further contain other solvents, and other additives such as a pigment, an emulsifier, and a thickener.
It is preferable for the capsule 78 according to the present embodiment to have a core-shell structure in which the shell is formed of a single layer, and to be breakable for a given pressure (stress) range in a given displacement range.
The method for manufacturing the capsule 78 is not particularly limited. For example, use of a dropping method enables the manufacture of the capsule 78 having a seamless shell. This method employs two concentric nozzles to concurrently discharge a content liquid from the inner nozzle and a fluidic shell material from the outer nozzle so that the shell liquid can seamlessly enclose the content liquid. Note that the capsule 78 may also be provided in a form in which a content liquid (without a coloring agent) is enclosed by a capsule main body containing a coloring agent, so that the coloring agent will seep and move into the content liquid from the capsule main body to make a colored content liquid during storage. Also, different nozzles may be employed for the content liquid, and in this case, a single-shelled capsule 78 may be produced using three concentric nozzles to concurrently discharge an inner content liquid from the inner nozzle, an outer content liquid from the intermediate nozzle, and a fluidic shell material from the outer nozzle. By separating the inner content liquid and the outer content liquid from each other, content liquids differing in properties can be discharged at different temperature and viscosity values. For example, a liquid containing a dissolved water-soluble flavorant may be adopted as the inner content liquid and a liquid containing a dissolved lipid-soluble flavorant may be adopted as the outer content liquid. Also, an emulsifier may be contained in the inner content liquid or the outer content liquid.
It is preferable for the capsule 78 according to the present embodiment to have a shell ratio (the ratio of the weight of the shell to the weight of the capsule 78) of 25 wt % or less.
It is preferable for the capsule 78 according to the present embodiment to be provided without, for example, a water-resistant coating and/or a heat-resistant coating around its outer periphery. The capsule 78 can therefore be manufactured at a low cost.
The capsule 78 may have, for example, a shape of a sphere or a shape of a substantial sphere. Such a sphere may either be a sphere having a substantially circular cross-section or an ellipsoid having an elliptical or substantially elliptical cross-section. The capsule 78 preferably has a shape of a sphere that is substantially circular in cross-section. The capsule 78 in the case of being a sphere having a substantially circular cross-section may have a diameter of 3.0 mm to 4.5 mm.
The second segment 74 and the third segment 76 which contains the capsule 78 are arranged in sequence, and the wrapper 80 wraps the second segment 74 and the third segment 76 so as to couple them together.
Then, the first segment 72 and a set of the second segment 74 and the third segment 76 wrapped by the wrapper 80 are arranged in sequence, the aerosol-generating segment 52 is placed on the first segment 72 side, and the resultant is wrapped by the tipping paper (mouthpiece lining paper) 56 having a paste (e.g., a vinyl-acetate-based paste) applied to substantially the entire inner surface thereof. The tipping paper 56 is constituted mainly by paper. In other words, the outer peripheries of the aerosol-generating segment 52 and the first segment 72, the second segment 74, and the third segment 76 of the mouthpiece segment 54 are wrapped with the tipping paper 56. The mouthpiece segment 54 is thus connected to the aerosol-generating segment 52 containing the tobacco filler 62 by means of the tipping paper (mouthpiece lining paper) 56. Note that the end of the tipping paper 56 may be aligned with the end of the wrapper 64 (the end 14a of the rod 14), or may be located between the distal end and the proximal end of the wrapper 64 as shown in
The total thickness of the wrappers (the inner
plug wrapper 94, the wrapper 80, and the tipping paper 56) that constitute the outer periphery of the mouthpiece segment 54 is equal to or less than a predetermined thickness, and in one example, it is preferably equal to or less than 100 μm. A too-large total thickness of the wrappers of the mouthpiece segment 54 is avoided so that the capsule 78 is kept easily perceivable at the time of pressing it from outside the mouthpiece segment 54.
After the aerosol-generating segment 52 and the mouthpiece segment 54 are connected together by the tipping paper 56, one or more perforations 58 (air vent portions) for introducing air are formed at positions of the mouthpiece segment 54 which correspond to, for example, the first segment 72. The perforations 58 penetrate through the paper tube of the first segment 72. Preferably, each perforation 58 is formed to have a size of approximately 0.5 mm×1.5 mm.
It is preferred that multiple of the perforations 58 are formed in a radial arrangement as viewed along the central axis of the rod 14. The present embodiment assumes the multiple perforations 58 arranged in one row, i.e., provided at regular intervals on an annular ring. The multiple perforations 58 may be arranged in two rows, i.e., provided at regular intervals on two annular rings. The multiple perforations 58 may also be discontinuously or irregularly arranged in one or two rows.
Note that the perforations 58 are formed at positions which come outside the insertion hole of the insertion part 42 of the heater 12 in a state where the end 14a of the rod 14 has been inserted into the insertion part 42 of the heater 12.
The solid rod 92 is, up to a mouthpiece end 14b of the mouthpiece segment 54, filled with a fiber-filled layer. The mouthpiece end 14b of the mouthpiece segment 54 of the rod 14 has a similar appearance to the mouthpiece end of a conventional cigarette.
Effects of the non-combustion heating type flavor inhalation system 10 will be described.
As shown in
The controller 34 measures the time from the start of various control operations for the pressure sensing part 28, the heater element 32, etc. The controller 34 detects a negative pressure in the housing 22 via the pressure sensing part 28 to count the number of inhalation actions performed by the user. Upon elapse of a predetermined time or upon the number of inhalation actions by the user reaching a predetermined number, the controller 34 performs control to stop the heating of the heater element 32.
In this way, the heating type flavor inhalation system 10 finishes the non-combustion heating type flavor inhalation operation for one rod 14. The user may then remove the used rod 14 from the insertion part 42 and insert the new rod 14 into the insertion part 42 to operate the heater 12 as described above, so that the user can taste the tobacco flavor from the new rod 14 again.
It has been confirmed with the cases of the present embodiment that if, for example, a user who uses the above described heater 12 and rod 14 performs one or more inhalation actions from the mouthpiece end 14b in the above manner, the inside of the solid rod (filter material) 92 of the third segment 76, that is, the vicinity of the outer periphery of the capsule 78, becomes hot and humid.
Now, turning to
A rheometer 100 (Sun RHEO METER CR-3000EX-L (Sun Scientific Co., Ltd.)) shown in
The rheometer 100 includes a pair of disks 102 and 104 which are vertically separate from each other. The pair of disks 102 and 104 have respective surfaces 102a and 104a which face each other and are parallel to each other. These surfaces 102a and 104a each have a diameter of 15 mm. The upper disk 104 is connected with a pressing shaft 106 which makes an axial movement along the vertical direction at, for example, a constant speed. The pressing shaft 106 and the upper disk 104 are adapted to be non-rotatable about the axis of the pressing shaft 106. The lower disk 102 is fixed. As such, the axial movement of the pressing shaft 106 causes the upper surface 104a to approach or separate from the lower surface 102a.
Here, it is assumed that the pressing shaft 106 of the rheometer 100, namely, the upper surface 104a, is controlled to move downward at a constant speed of 20 mm/min.
The cutout segment 98 was put between the surfaces 102a and 104a of the rheometer 100 shown in
Referring to
The repulsive force represented by the vertical axis in
In applying an external force from above and below toward the central axis of the cutout segment 98 in order to break the capsule 78 in the filter material (solid rod) 92, compression takes place in the order of the tipping paper 56, the wrapper 80, the inner plug wrapper 94, the filter material 92, and the capsule 78. Here, the compression makes the tipping paper 56, the wrapper 80, the inner plug wrapper 94, and the filter material 92 thinner while the outer diameter of the capsule 78 is substantially maintained. Then, after the tipping paper 56, the wrapper 80, the inner plug wrapper 94, and the filter material 92 have been compressed, or while they are being compressed, the capsule 78 is compressed and deformed. The capsule 78 here is compressed so as to be changed from the spherical shape to a flat shape while the tipping paper 56, the wrapper 80, the inner plug wrapper 94, and the filter material 92 are maintained in the appropriately thinned state or are further thinned.
Note that it is assumed here that the repulsive force from the tipping paper 56, the wrapper 80, and the inner plug wrapper 94 which occurs against the pressing of the cutout segment 98 is negligibly small as compared to the repulsive force of the filter material 92 or the capsule 78.
In the example shown in
Supposing that the pressing operation by the rheometer 100 for the cutout segment 98 represents a finger pushing action by the user, it can be presumed that the user would recognize the repulsive force from the shell of the capsule 78 at the inflection point α through the fingers, etc. It is also presumed that, after the inflection point α, the user would then feel that the user is deforming the shell of the capsule 78 via the tipping paper 56, the wrapper 80, the inner plug wrapper 94, and the filter material 92.
In the example shown in
In the example shown in
Note that the experiment for measuring the repulsive force of the cutout segment 98 shown in
As shown in
Note, additionally, that even in instances where the cutout segment 298 shown in
The experiment for measuring the repulsive force of the cutout segment 298 shown in
Based on the foregoing, it is presumed that the cutout segment 98 of the rod 14 would show an inflection point α as shown in
Therefore, it is preferable that the capsule 78 for use in the rod 14 of the heating type flavor inhalation system 10 give a large repulsive force at the initial compression stage under the hot and humid condition as discussed above.
Note that a variation in the temperature and the humidity in the device 110 by, for example, ±several % with respect to the target temperature and humidity condition (e.g., 45° C. and 90% RH) is tolerated.
Here, as the subject capsules 78, three kinds of capsules having the same or substantially the same outer diameter but differing in composition were prepared and subjected to the above described measurement using the above described rheometer 100 without the presence of the tipping paper 56, the wrapper 80, the inner plug wrapper 94, and the filter material 92 (cf.,
As shown in
The first capsule 78a and the second capsule 78b were broken at approximately 1.5 mm, whereas the third capsule 78c was broken at a point beyond 2 mm.
A rod 14 including the first capsule 78a, a rod 14 including the second capsule 78b, and a rod 14 including the third capsule 78c were prepared. These capsules 78a, 78b, and 78c were not exposed to a hot and humid environment such as the 45° C. and 90% RH condition as discussed above. Then, sensory evaluation (blind evaluation) on the feeling of breaking the capsules 78a, 78b, and 78c in the respective rods 14 were conducted by seven experts and
The employed scoring criteria were “5” for the best feeling of breaking to “1” for the worst feeling of breaking. The experimental results shown in
The first capsule 78a was evaluated as giving a better feeling of breaking than the second capsule 78b and the third capsule 78c. The second capsule 78b was evaluated as giving a better feeling of breaking than the third capsule 78c but a worse feeling of breaking than the first capsule 78a. The third capsule 78c was evaluated as giving a worse feeling of breaking than each of the second capsule 78b and the third capsule 78c.
As noted above, the first capsule 78a was evaluated as giving a better feeling of breaking than each of the second capsule 78b and the third capsule 78c.
Presumably, this is attributable to its large stress against the displacement as shown in
Also, the first capsule 78a shows a high stress against the initial displacement as compared to the second capsule 78b and the third capsule 78c. Thus, it is presumed that the user would perceive the first capsule 78a to be adequately hard. That is, it is presumed that, in the state where the first capsule 78a is adopted in the mouthpiece segment 54 of the rod 14, the user can easily recognize the inflection point corresponding to the point α as shown in
Presumably, the displacement of the first capsule 78a that was produced from the start of its deformation to the breakage was neither too small nor too large. Thus, it is presumed that the first capsule 78a was successfully broken within a range of displacement for which the user had an increasing expectation, between the point at which the user became aware of pressing the first capsule 78a with fingers, teeth, or the like and the point of breakage of the first capsule 78a. Therefore, it is presumed that the user gave a favorable evaluation to the first capsule 78a (the rod 14 including the first capsule 78a).
It is also presumed that the time from the start of deformation to the breakage of the first capsule 78a was neither too short nor too long. Thus, it is presumed that the first capsule 78a was successfully broken within a period of time for which the user had an increasing expectation, between the point at which the user became aware of pressing the first capsule 78a with fingers, teeth, or the like and the point of breakage of the first capsule 78a. Therefore, it is presumed that the user gave a favorable evaluation to the first capsule 78a (the rod 14 including the first capsule 78a).
As noted above, the second capsule 78b was evaluated as giving a better feeling of breaking than the third capsule 78c, while it was evaluated as giving a worse feeling of breaking than the first capsule 78a.
As shown in
It is also presumed that, with the use of the second capsule 78b, the stress at the breakage would be small and the difference in the height H between the point β and the point γ as shown in
As noted above, the third capsule 78c was evaluated as giving a worse feeling of breaking than each of the second capsule 78b and the third capsule 78c.
As shown in
It is also presumed that, with the use of the third capsule 78c, the stress at the breakage would be small and the difference in the height H between the point β and the point γ as shown in
Further, the displacement of the third capsule 78c that was produced from the start of its deformation to the breakage was larger than that of the first capsule 78a and that of the second capsule 78b. Thus, it is presumed that the third capsule 78c was broken at a point away from the peak of the range of displacement for which the user had an increasing expectation, between the point at which the user became aware of pressing the third capsule 78c and the point of breakage of the third capsule 78c. For example, it is presumed that since the user felt no breakage of the capsule 78 even by continuously pressing the exterior of the rod 14 toward the central axis with an appropriate stroke, the capsule 78 was broken after the user's expectation that the capsule will break shrunk. Therefore, it is presumed that the user gave a poor evaluation as compared to that given for the first capsule 78a and the second capsule 78b.
From a different perspective, it is presumed that the third capsule 78c might have been broken while the user remained unable to recognize the pressing of the third capsule 78c. It is thus presumed that the third capsule 78c was broken without increasing the user's expectation that the third capsule 78c will break. Therefore, it is presumed that the user gave a poor evaluation as compared to the first capsule 78a and the second capsule 78b.
Presumably, the displacement of the third capsule 78c that was produced from the start of its deformation to the breakage was too large (equal to or greater than 2 mm). Thus, it is presumed that the third capsule 78c was broken at the displacement for which the expectation of the user had shrunk, after the range of displacement for which the user had an increasing expectation, between the point at which the user became aware of pressing the first capsule 78a with fingers, teeth, or the like and the point of breakage of the third capsule 78c. It is therefore presumed that the user gave a poor evaluation for the feeling of breaking to the third capsule 78c (the rod 14 including the third capsule 78c).
It is also presumed that the time from the start of deformation to the breakage of the third capsule 78c was too long. Thus, it is presumed that the third capsule 78c was broken at the time point for which the expectation of the user had shrunk, after the period of time for which the user had an increasing expectation, between the point at which the user became aware of pressing the first capsule 78a with fingers, teeth, or the like and the point of breakage of the third capsule 78c. It is therefore presumed that the user gave a poor evaluation for the feeling of breaking to the third capsule 78c (the rod 14 including the third capsule 78c).
From the foregoing, it can be said that the most preferred form is that the rod 14 that includes the mouthpiece segment 54 with the third segment 76 in which the first capsule 78a according to the present embodiment is arranged is used together with the heater 12. More specifically, among the capsules 78 stored for 10 minutes under the condition of 45° C. and 90% RH, the capsule 78 to be employed within 4 minutes from the storage is preferably the first capsule 78a having a stress of 2 N or more against the displacement of 0.5 mm, which is larger than the stress of the second capsule 78b and the stress of the third capsule 78c. Also, the capsule 78 is preferably the first capsule 78a having a stress equal to or less than 6 N against the displacement of 5 mm, i.e., the largest repulsive force obtained in the current manufacturing technology. Note that it is more preferable for the first capsule 78a to show 2.5 N or more and 6 N or less against the displacement of 0.5 mm. Accordingly, it is possible to provide a rod 14, i.e., a non-combustion heating type flavor inhalation article, which allows the user who has performed at least one inhalation action and who intends to break the first capsule 78a to readily perceive the presence of the first capsule 78a.
Also, among the capsules 78 stored for 10 minutes under the condition of 45° C. and 90% RH, the capsule 78 to be employed within 4 minutes from the storage is preferably the first capsule 78a having a stress of 3 N or more and equal to or less than 20 N against the displacement of 1 mm, i.e., the largest repulsive force obtained in the current manufacturing technology, which is larger than the stress of the second capsule 78b and the stress of the third capsule 78c. It is more preferable for the first capsule 78a to show 4 N or more and 20 N or less against the displacement of 1 mm. The capsule 78 is preferably the first capsule 78a formed to be breakable at the displacement of 1 mm or more and 2 mm or less so that the user can receive a feeling that the stroke of the fingers or the teeth of the user after recognition is not too small or too large. Also with these features, it is possible to provide a rod 14, i.e., a non-combustion heating type flavor inhalation article, which allows the user who has performed at least one inhalation action and who intends to break the first capsule 78a to readily perceive the presence of the first capsule 78a.
For the shell of the first capsule 78a which is employed within 4 minutes from the 10-minute storage under the condition of 45° C. and 90% RH and which has a stress of 2 N or more and 6 N or less against the displacement of 0.5 mm and a stress of 3 N or more and 20 N or less against the displacement of 1 mm, it is possible to employ, for example, any of starch, dextrin, polysaccharide, agar, gellan gum, gelatin, carrageenan, various natural gelling agents, glycerin, sorbitol, calcium chloride, etc., and the shell may further contain a flavorant and a coloring agent. The first capsule 78a may be produced from appropriate materials in an appropriate recipe so as to satisfy the property that the first capsule 78a, if employed within 4 minutes from the 10-minute storage under the above described condition of 45° C. and 90% RH, would show a stress of 2 N or more and 6 N or less against the displacement of 0.5 mm and a stress of 3 N or more and 20 N or less against the displacement of 1 mm. The shell preferably contains gellan gum and starch, and further, the weight ratio between gellan gum and starch in the shell (gellan gum:starch) is preferably from 50:1 to 1:1, and more preferably from 10:1 to 3:2. Also, the gellan gum is preferably deacylated gellan gum, and the starch is preferably oxidized starch.
The first capsule 78a suitable for the rod 14 of the heating type flavor inhalation system 10 according to the present embodiment has a shell ratio of 25 wt % or less, and the first capsule 78a is formed as a seamless member containing polysaccharide. Accordingly, it is possible to form the first capsule 78a with a hard shell, while keeping the shell weight relatively small, that is, while preventing the shell from becoming thicker. The shell thickness may be adjusted by changing the temperature, the viscosity, and the discharge amount of a fluidic shell material or a content liquid for producing the capsule in the dropping method.
It is preferable for the first capsule 78a to be employed such that the ratio of its diameter to the cross-section diameter of the filter material 92 be 45% or more and 70% or less. With the ratio of the diameter of the first capsule 78a to the cross-section diameter of the filter material 92 being 45% or more, the diameter of the first capsule 78a can have a suitable size which is larger than about half of the diameter of the mouthpiece segment 54. This allows the user to readily perceive the presence of the first capsule 78a. Also, with the ratio of the diameter of the first capsule 78a to the cross-section diameter of the filter material 92 being 70% or less, a too large pressure loss of the mouthpiece segment 54 before the breakage of the first capsule 78a can be avoided. If the ratio to the cross-section diameter of the filter material 92 exceeds 70%, troubles in inhalation actions may occur while it is easy to perceive the presence of the first capsule 78a before its breakage. As such, it is preferable that the ratio of the diameter of the first capsule 78a to the cross-section diameter of the filter material 92 be 70% or less.
Note that in the instance where the first capsule 78a is a sphere having a diameter of 3.0 mm, the mouthpiece segment 54 has a diameter of approximately 4.2 mm to 6.7 mm. In the instance where the first capsule 78a is a sphere having a diameter of 4.5 mm, the mouthpiece segment 54 has a diameter of approximately 6.4 mm to 10 mm. Thus, if the first capsule 78a is a sphere having a diameter of 3.0 mm to 4.5 mm, the mouthpiece segment 54 of the rod 14 has a diameter of approximately 4. mm to 10 mm.
Additionally, in the heating type flavor inhalation system 10, it is preferable for the filter material 92 of the third segment 76 of the rod 14 to have, for example, a suitably suppressed filling density since such a soft filter material 92 allows the user to easily recognize the capsule 78, which is harder than the filter material 92.
Generally, a plasticizer that may be contained in the filter material 92 becomes hard as its content increases. Although the filter material 92 may contain a plasticizer, it is preferred that the filter material 92 which encloses the first capsule 78a be formed to have a softness that permits the hardness of the first capsule 78a in the rod 14 to be easily perceivable after, for example, several inhalation actions with the heating type flavor inhalation system 10.
Moreover, in the heating type flavor inhalation system 10, it is preferable that the inner plug wrapper 94, the wrapper 80, and the tipping paper 56 of the third segment 76 of the rod 14 have, for example, a low basis weight and a property of flexibility so that the hardness of the first capsule 78a in the rod 14 can be easily perceived.
According to the present embodiment as described above, it is possible to provide a non-combustion heating type flavor inhalation article 14 which allows the user who has performed at least one inhalation action and who intends to break the first capsule 78a to readily perceive the presence of the first capsule 78a.
Note that the mouthpiece segment 54 may involve various modifications.
If the second segment 74 is absent, the first segment 72 and the third segment 76 may be arranged adjacent to each other.
If the first segment 72 and the second segment 74 are both absent, the third segment 76 may be connected to the aerosol-generating segment 52 for use. The third segment 76 is preferably formed of a paper material rather than cellulose acetate fibers.
According to other options, it is also preferred that the mouthpiece segment 54 be formed only of the third segment 76 including the first capsule 78a. Also, the solid rod (filter material) 92 of the third segment 76 may be formed of paper.
The hollow rod 82 of the second segment 74 may be formed of paper.
Preferably, at least one of the hollow rod 82 of the second segment 74 and the solid rod (filter material) 92 of the third segment 76 has an adsorbent.
It is also preferred that the hollow rod 82 of the second segment 74 and the solid rod (filter material) 92 of the third segment 76 be formed as a single segment, and the first capsule 78a be arranged in this single segment.
Note that, as shown in
Note that the heating mode adopted by the heater element 32 may be a mode that utilizes Joule heat from electrical resistance, and it may also adopt an induction heating (IH) mode or a mode utilizing a chemical reaction that produces oxidation heat, etc. In this case, a heat transfer part 30 suitably adapted for the heating mode is selected.
Additional advantages and modifications will readily occur to those skilled in the art. Therefore, the invention in its broader aspects is not limited to the specific details and representative embodiments shown and described herein. Accordingly, various modifications may be made without departing from the spirit or scope of the general inventive concept as defined by the appended claims and their equivalents.
According to the embodiments described above, the following can be said.
Appendix 11. A non-combustion heating type flavor inhalation article comprising:
-
- an aerosol-generating segment; and
- a mouthpiece segment adjacent to the aerosol-generating segment, the mouthpiece segment comprising
- a filter material, and
- a breakable capsule within the filter material, the breakable capsule having a single-layered core-shell structure,
- wherein:
- the capsule is spherical or approximately spherical with a diameter of 3.0 mm to 4.5 mm, and
- the capsule has a stress of 2 N or more and 6 N or less against a displacement of 0.5 mm within 4 minutes from 10 minutes of storage under a condition of 45° C. and 90% RH.
The non-combustion heating type flavor inhalation article according to Appendix 1,
-
- wherein the capsule has a stress of 2.5 N or more and 6 N or less against the displacement of 0.5 mm within 4 minutes from the 10 minutes of storage under the condition of 45° C. and 90% RH.
The non-combustion heating type flavor inhalation article according to Appendix 1 or 2,
-
- wherein the capsule has a stress of 3 N or more and 20 N or less against a displacement of 1 mm within 4 minutes from the 10 minutes of storage under the condition of 45° C. and 90% RH.
The non-combustion heating type flavor inhalation article according to Appendix 3,
-
- wherein the capsule has a stress of 4 N or more and 20 N or less against the displacement of 1 mm within 4 minutes from the 10 minutes of storage under the condition of 45° C. and 90% RH.
The non-combustion heating type flavor inhalation article according to any one of Appendixes 1 to 4,
-
- wherein the capsule is breakable at a displacement of 1 mm or more and 2 mm or less.
The non-combustion heating type flavor inhalation article according to any one of Appendixes 1 to 5,
-
- wherein a ratio of a diameter of the capsule to a cross-section diameter of the filter material is 45% or more and 70% or less.
The non-combustion heating type flavor inhalation article according to any one of Appendixes 1 to 6, wherein:
-
- a shell ratio of the capsule is 25 wt % or less, and
- the capsule is a seamless member containing polysaccharide.
The non-combustion heating type flavor inhalation article according to any one of Appendixes 1 to 7, wherein:
-
- the filter material comprises a layer filled with cellulose acetate long fibers plasticized by a plasticizer, and
- a filling density of the cellulose acetate long fiber-filled layer is 130 [mg/cc] or less.
The non-combustion heating type flavor inhalation article according to Appendix 8, wherein:
-
- a filament denier of the cellulose acetate long fiber-filled layer is 3.0 dpf or more and 12.0 dpf or less.
The non-combustion heating type flavor inhalation article according to any one of Appendix 1 to 9, wherein:
-
- the capsule comprises a shell containing gellan gum and starch.
A non-combustion heating type flavor inhalation system comprising:
-
- the non-combustion heating type flavor inhalation article according to any one of Appendixes 1 to 10; and
- a heater configured to heat the aerosol-generating segment without burning.
Claims
1. A non-combustion heating type flavor inhalation article comprising:
- an aerosol-generating segment; and
- a mouthpiece segment adjacent to the aerosol-generating segment, the mouthpiece segment comprising a filter material, and a breakable capsule within the filter material, the breakable capsule having a single-layered core-shell structure,
- wherein:
- the capsule is spherical or approximately spherical with a diameter of 3.0 mm to 4.5 mm, and
- the capsule has a stress of 2 N or more and 6 N or less against a displacement of 0.5 mm within 4 minutes from 10 minutes of storage under a condition of 45° C. and 90% RH.
2. The non-combustion heating type flavor inhalation article according to claim 1,
- wherein the capsule has a stress of 2.5 N or more and 6 N or less against the displacement of 0.5 mm within 4 minutes from the 10 minutes of storage under the condition of 45° C. and 90% RH.
3. The non-combustion heating type flavor inhalation article according to claim 1,
- wherein the capsule has a stress of 3 N or more and 20 N or less against a displacement of 1 mm within 4 minutes from the 10 minutes of storage under the condition of 45° C. and 90% RH.
4. The non-combustion heating type flavor inhalation article according to claim 3,
- wherein the capsule has a stress of 4 N or more and 20 N or less against the displacement of 1 mm within 4 minutes from the 10 minutes of storage under the condition of 45° C. and 90% RH.
5. The non-combustion heating type flavor inhalation article according to claim 1,
- wherein the capsule is breakable at a displacement of 1 mm or more and 2 mm or less.
6. The non-combustion heating type flavor inhalation article according to claim 1,
- wherein a ratio of a diameter of the capsule to a cross-section diameter of the filter material is 45% or more and 70% or less.
7. The non-combustion heating type flavor inhalation article according to claim 1, wherein:
- a shell ratio of the capsule is 25 wt % or less, and
- the capsule is a seamless member containing polysaccharide.
8. The non-combustion heating type flavor inhalation article according to claim 1, wherein:
- the filter material comprises a layer filled with cellulose acetate long fibers plasticized by a plasticizer, and
- a filling density of the cellulose acetate long fiber-filled layer is 130 [mg/cc] or less.
9. The non-combustion heating type flavor inhalation article according to claim 8, wherein:
- a filament denier of the cellulose acetate long fiber-filled layer is 3.0 dpf or more and 12.0 dpf or less.
10. The non-combustion heating type flavor inhalation article according to claim 1, wherein:
- the capsule comprises a shell containing gellan gum and starch.
11. A non-combustion heating type flavor inhalation system comprising:
- the non-combustion heating type flavor inhalation article according to claim 1; and
- a heater configured to heat the aerosol-generating segment without burning.
Type: Application
Filed: Dec 9, 2024
Publication Date: Mar 27, 2025
Applicant: Japan Tobacco Inc. (Tokyo)
Inventor: Makoto AKAI (Tokyo)
Application Number: 18/973,119