Target Composition Patents (Class 204/298.13)
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Patent number: 8753491Abstract: It is an object to provide a method for packaging a target material with which a thin film that is less contaminated with an impurity in the air such as a compound containing a hydrogen atom can be formed. In addition, it is an object to provide a method for mounting a target with which a thin film that is less contaminated with an impurity can be formed. In order to achieve the objects, a target material in a target is not exposed to the air and kept sealed after being manufactured until a deposition apparatus on which the target is mounted is evacuated.Type: GrantFiled: November 12, 2010Date of Patent: June 17, 2014Assignee: Semiconductor Energy Laboratory Co., Ltd.Inventors: Shunpei Yamazaki, Toru Takayama, Keiji Sato
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Publication number: 20140158532Abstract: Provided is a high-purity copper-manganese-alloy sputtering target comprising 0.05 to 20 wt. % of Mn, 2 wt ppm or less of C, and the remainder being Cu and inevitable impurities, wherein in formation of a film on a wafer by sputtering the target, the number of particles composed of C, at least one element selected from Mn, Si, and Mg, or a compound composed of C and at least one element selected from Mn, Si, and Mg and having a diameter of 0.20 ?m or more is 30 or less on average. Particle generation during sputtering can be effectively suppressed by thus adding an appropriate amount of Mn element to copper and controlling the amount of carbon. In particular, a high-purity copper-manganese-alloy sputtering target that is useful for forming semiconductor copper alloy line having a self-diffusion suppression function is provided.Type: ApplicationFiled: September 5, 2012Publication date: June 12, 2014Applicant: JX NIPPON MINING & METALS CORPORATIONInventors: Kenichi Nagata, Tomio Otsuki, Takeo Okabe, Nobuhito Makino, Atsushi Fukushima
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Publication number: 20140158951Abstract: [Object] Provided are: a Zn—Si—O-based oxide sintered body, which suppresses abnormal discharge and so forth when used as a sputtering target, or suppresses a splash phenomenon when used as a tablet for vapor deposition; a method for producing the Zn—Si—O-based oxide sintered body; and the like. [Solution] The Zn—Si—O-based oxide sintered body contains zinc oxide as a main component and Si, and is characterized in that a Si content is 0.1 to 10 atomic % with an atomic ratio of Si/(Zn+Si), the Si element is contained in a wurtzite-type zinc oxide phase to form a solid solution, and the oxide sintered body does not contain a SiO2 phase and zinc silicate (Zn2SiO4) as a spinel-type composite oxide phase.Type: ApplicationFiled: July 3, 2012Publication date: June 12, 2014Applicant: SUMITOMO METAL MINING CO., LTD.Inventors: Yasunori Yamanobe, Kentaro Sogabe, Makoto Ozawa
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Patent number: 8747626Abstract: A method for forming and protecting high quality bismuth oxide films comprises depositing a transparent thin film on a substrate comprising one of Si, alkali metals, or alkaline earth metals. The transparent thin film is stable at room temperature and at higher temperatures and serves as a diffusion barrier for the diffusion of impurities from the substrate into the bismuth oxide. Reactive sputtering, sputtering from a compound target, or reactive evaporation are used to deposit a bismuth oxide film above the diffusion barrier.Type: GrantFiled: November 30, 2011Date of Patent: June 10, 2014Assignee: Intermolecular, Inc.Inventors: Guowen Ding, Mohd Fadzli Anwar Hassan, Hien Minh Huu Le, Zhi-Wen Sun
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Patent number: 8747633Abstract: In one embodiment, a method for manufacturing a tantalum sputtering target includes a first knead forging step, a first heating step, a second knead forging step, a cold rolling step, and a second heating step. In the first knead forging step, a tantalum material is subjected to two sets or more of knead forging, each of the sets being cold forging in directions parallel to and perpendicular to a thickness direction. In the second knead forging step, one set or more of knead forging is performed after the first heating step, each of the steps being cold forging in the directions parallel to and perpendicular to the thickness direction.Type: GrantFiled: May 14, 2012Date of Patent: June 10, 2014Assignees: Kabushiki Kaisha Toshiba, Toshiba Materials Co., Ltd.Inventors: Nobuaki Nakashima, Yoshiki Orimoto
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Publication number: 20140151216Abstract: A sputtering apparatus includes a chamber. A substrate supporting part is disposed in the chamber. A plurality of targets face the substrate supporting part. A target supporting part is disposed under each of the targets to hold the target. A first ground part is disposed between two target supporting parts adjacent to each other and includes a cover separable therefrom. A second ground part is disposed between two target supporting parts adjacent to each other, except for where the first ground part is disposed.Type: ApplicationFiled: May 22, 2013Publication date: June 5, 2014Applicant: SAMSUNG DISPLAY CO., LTD.Inventors: Sang-Woo Sohn, Hyung-Jun Kim
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Patent number: 8741114Abstract: There is provided a hard film excellent in wear resistance. The hard film in accordance with the present invention includes (TiaCrbAlcLd) (BxCyNz) in terms of composition, in which the L is at least one of Si and Y, and the a, b, c, d, x, y, and z each denote the atomic ratio, and satisfy: 0.1?a<0.3; 0.3<b<0.6; 0.2?c<0.35; 0.01?d<0.1; a+b+c+d=1; x?0.1; y?0.1; 0.8?z?1; and x+y+z=1.Type: GrantFiled: May 29, 2013Date of Patent: June 3, 2014Assignee: Kobe Steel, LtdInventor: Kenji Yamamoto
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Patent number: 8741077Abstract: Titanium-tungsten alloys are described comprising tungsten ranging from about 9% to about 20% by weight, and titanium ranging from about 91% to about 80% by weight, exhibiting a yield strength of at least 120,000 psi, and a ductility of at least 20% elongation. Methods of making the alloy, and products made with the alloys are also disclosed herein.Type: GrantFiled: February 22, 2011Date of Patent: June 3, 2014Assignee: Dynamet Technology, Inc.Inventors: Stanley Abkowitz, Susan M. Abkowitz, Harvey Fisher, Patricia J. Schwartz
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Publication number: 20140145185Abstract: A sputtering target including a sintered body including In, Ga and Mg, the sintered body including one or more compounds selected from a compound represented by In2O3, a compound represented by In(GaMg)O4, a compound represented by Ga2MgO4 and a compound represented by In2MgO4, and having an atomic ratio In/(In+Ga+Mg) of 0.5 or more and 0.9999 or less and an atomic ratio (Ga+Mg)/(In+Ga+Mg) of 0.0001 or more and 0.5 or less.Type: ApplicationFiled: June 28, 2012Publication date: May 29, 2014Inventors: Kazuaki Ebata, Shigekazu Tomai, Kota Terai, Shigeo Matsuzaki, Koki Yano
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Publication number: 20140144775Abstract: Disclosed is an MgO target for sputtering, which can accelerate a film formation rate even when MgO is used as a target for sputtering in the formation of an MgO film. The MgO target for sputtering, which includes MgO and an electroconductive material as main components, and in which the electroconductive material is capable of imparting orientation to a MgO film when the MgO film containing the electroconductive material is formed by a DC sputtering.Type: ApplicationFiled: June 29, 2012Publication date: May 29, 2014Applicants: NIPPON TUNGSTEN CO., LTD., UBE MATERIALS INDUSTRIES, LTD.Inventors: Satoru Sano, Yoshihiro Nishimura, Takayuki Watanabe, Yuuzou Katou, Akira Ueki, Shinzo Mitomi, Masanobu Takasu, Yusuke Hara, Takaaki Tanaka
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Publication number: 20140147940Abstract: A sputtering target for a conductive oxide, such as SrRuO3, to be used for the sputter deposition of a conductive film that is to be in contact with a ferroelectric material in an integrated circuit. The sputtering target is formed by the sintering of a powder mixture of the conductive oxide with a sintering agent of an oxide of one of the constituents of the ferroelectric material. For the example of lead-zirconium-titanate (PZT) as the ferroelectric material, the sintering agent is one or more of a lead oxide, a zirconium oxide, and a titanium oxide. The resulting sputtering target is of higher density and lower porosity, resulting in an improved sputter deposited film that does not include an atomic species beyond those of the ferroelectric material deposited adjacent to that film.Type: ApplicationFiled: November 25, 2013Publication date: May 29, 2014Applicant: Texas Instruments IncorporatedInventors: Mark Robert Visokay, Scott Robert Summerfelt
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Publication number: 20140145124Abstract: A sputtering target including an oxide A and InGaZnO4, the oxide A having a diffraction peak in regions A to K at 2?=7.0° to 8.4°, 30.6° to 32.0°, 33.8° to 35.8°, 53.5° to 56.5°, 56.5° to 59.5°, 14.8° to 16.2°, 22.3° to 24.3°, 32.2° to 34.2°, 43.1° to 46.1°, 46.2° to 49.2°, and 62.7° to 66.7°.Type: ApplicationFiled: April 27, 2012Publication date: May 29, 2014Inventors: Misa Sunagawa, Masayuki Itose, Mami Nishimura, Masashi Kasami
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Patent number: 8734619Abstract: A method including directing a first radiation at a first copper-indium-gallium (CIG) sputtering target in a reactive copper indium gallium selenide (CIGS) sputtering process, detecting a first reflected radiation from the first CIG target and determining the amount of selenium poisoning of the first CIG target based on the first reflected radiation.Type: GrantFiled: March 2, 2011Date of Patent: May 27, 2014Assignee: Hanergy Holding Group Ltd.Inventor: John Corson
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Publication number: 20140138242Abstract: Described are methods of fabricating lithium sputter targets, lithium sputter targets, associated handling apparatus, and sputter methods including lithium targets. Various embodiments address adhesion of the lithium metal target to a support structure, avoiding and/or removing passivating coatings formed on the lithium target, uniformity of the lithium target as well as efficient cooling of lithium during sputtering. Target configurations used to compensate for non-uniformities in sputter plasma are described. Modular format lithium tiles and methods of fabrication are described. Rotary lithium sputter targets are also described.Type: ApplicationFiled: April 20, 2012Publication date: May 22, 2014Applicant: VIEW, INC.Inventors: Martin John Neumann, Disha Mehtani, Sridhar Kailasam, Trevor Frank, Todd Martin, Jason Satern, Que Anh Song Nguyen, Dhairya Shrivastava, Martin John Neumann, Anshua A. Pradhan, Robert T. Rozbicki
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Publication number: 20140140884Abstract: Provided are high-purity yttrium and a high-purity yttrium sputtering target each having a purity, excluding rare earth elements and gas components, of 5 N or more and containing 1 wt ppm or less of each of Al, Fe, and Cu; a method of producing high-purity yttrium by molten salt electrolysis of a raw material being a crude yttrium oxide having a purity, excluding gas components, of 4N or less at a bath temperature of 500° C. to 800° C. to obtain yttrium crystals, desalting treatment, water washing, and drying of the yttrium crystals, and then electron beam melting for removing volatile materials to achieve a purity, excluding rare earth elements and gas components, of 5N or more; and a technology capable of efficiently and stably providing high-purity yttrium, a sputtering target composed of the high-purity yttrium, and a metal-gate thin film mainly composed of the high-purity yttrium.Type: ApplicationFiled: September 15, 2011Publication date: May 22, 2014Applicant: JX NIPPON MINING & METALS CORPORATIONInventor: Masahiro Takahata
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Patent number: 8729702Abstract: A trench is opened in a dielectric layer. The trench is then lined with a barrier layer and a metal seed layer. The metal seed layer is non-uniformly doped and exhibits a vertical doping gradient varying as a function of trench depth. The lined trench is then filled with a metal fill material. A dielectric cap layer is then deposited over the metal filled trench. Dopant from the non-uniformly doped metal seed layer is then migrated to an interface between the metal filled trench and the dielectric cap layer to form a self-aligned metal cap.Type: GrantFiled: November 20, 2012Date of Patent: May 20, 2014Assignees: STMicroelectronics, Inc., International Business Machines CorporationInventors: Chengyu Niu, Andrew Simon, Keith Kwong Hon Wong, Yun-Yu Wang
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Patent number: 8728287Abstract: A cathode sputtering target includes: between 30 and 40 atomic % of a metal, between 2 and 10 atomic % of nitrogen, and between 35 and 50 atomic % of oxygen. The remainder up to 100% is constituted by at least one element selected from the group that comprises phosphorous (P), boron (B), silicon (Si), germanium (Ge), gallium (Ga), sulphur (S) and aluminium (Al). Also provides a method of manufacturing a thin film from the target, and an electrochemical device comprising the thin film.Type: GrantFiled: March 26, 2008Date of Patent: May 20, 2014Assignee: H.E.F.Inventors: Michel Martin, Philippe Maurin-Perrier, Olivier Blandenet
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Patent number: 8728358Abstract: An amorphous film comprising indium, tin, calcium and oxygen, wherein tin is contained at a ratio of 5 to 15% based on an atomicity ratio of Sn/(In+Sn+Ca) and calcium is contained at a ratio of 0.1 to 2.0% based on an atomicity ratio of Ca/(In+Sn+Ca), and remnant is indium and oxygen, is provided. The film can be crystallized by annealing at 260° C. or lower in which resistivity of the film will be 0.4 m?cm or less. In this manner, an ITO thin film for use as a display electrode or the like in a flat panel display can be made into an amorphous ITO film by way of sputter deposition without heating the substrate or adding water during deposition. This ITO film can be crystallized by annealing at a low temperature and will have low resistivity. Methods of producing such films and sintered compacts are provided.Type: GrantFiled: August 23, 2012Date of Patent: May 20, 2014Assignee: JX Nippon Mining & Metals CorporationInventors: Masakatsu Ikisawa, Masataka Yahagi, Kozo Osada, Takashi Kakeno
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Patent number: 8723175Abstract: A field effect transistor including a semiconductor layer including a composite oxide which contains In, Zn, and one or more elements X selected from the group consisting of Zr, Hf, Ge, Si, Ti, Mn, W, Mo, V, Cu, Ni, Co, Fe, Cr, Nb, Al, B, Sc, Y and lanthanoids in the following atomic ratios (1) to (3): In/(In+Zn)=0.2 to 0.8??(1) In/(In+X)=0.29 to 0.99??(2) Zn/(X+Zn)=0.29 to 0.99??(3).Type: GrantFiled: January 24, 2013Date of Patent: May 13, 2014Assignee: Idemitsu Kosan Co., Ltd.Inventors: Koki Yano, Hirokazu Kawashima, Kazuyoshi Inoue, Shigekazu Tomai, Masashi Kasami
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Publication number: 20140127467Abstract: A silver-based magnesium alloy thin film is provided for the semi-reflective coating layer of optical discs. This alloy has moderate to high reflectivity and reasonable corrosion resistance in the ambient environment.Type: ApplicationFiled: January 10, 2014Publication date: May 8, 2014Applicant: TARGET TECHNOLOGY COMPANY, LLCInventor: Han H. Nee
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Publication number: 20140124365Abstract: In a method of forming a cylindrical sputter target assembly, comprising the steps of: (a) providing a cylindrical backing tube; (b) providing a cylindrical sputter target, the inner diameter of which is larger than the outer diameter of the backing tube; (c) arranging the sputter target about the backing tube; and (d) bonding the sputter target to the backing tube by providing a solder layer between the backing tube and the sputter target; In accordance with the invention step (d) comprises directionally solidifying the solder layer.Type: ApplicationFiled: April 29, 2011Publication date: May 8, 2014Inventors: Dieter Wurczinger, David Daniel
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Publication number: 20140124366Abstract: High-purity erbium having a purity of 5N or higher excluding rare earth elements and gas components, and containing Al, Fe, Cu, and Ta each in an amount of 1 wtppm or less, W in an amount of 10 wtppm or less, carbon in an amount of 150 wtppm or less, alkali metals and alkali earth metals each in an amount of 1 wtppm or less, other transition metal elements in a total amount of 10 wtppm or less, and U and Th as radioactive elements each in an amount of 10 wtppb or less. An object of this invention is to provide a method of highly purifying erbium, which has a high vapor pressure and is difficult to refine in a molten state, as well as technology for efficiently and stably providing high-purity erbium obtained with the foregoing method, a sputtering target made of high-purity erbium, and a metal gate film having high-purity erbium as a main component thereof.Type: ApplicationFiled: September 15, 2011Publication date: May 8, 2014Applicant: JX NIPPON MINING & METALS CORPORATIONInventor: Masahiro Takahata
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Publication number: 20140110255Abstract: Cylindrical sputtering targets are provided. The cylindrical sputtering target can include a tubular member having a length in a longitudinal direction and defining a tube surface. A source material is positioned about the tube surface of the tubular member and forms a sputtering surface about the tubular member. The source material generally includes a plurality of first areas and a plurality of second areas, each first area comprising a first compound and each second area comprising a second compound that is different than the first compound.Type: ApplicationFiled: October 18, 2012Publication date: April 24, 2014Applicant: PRIMESTAR SOLAR, INC.Inventors: Scott Daniel Feldman-Peabody, Robert Dwayne Gossman, Mark Jeffrey Pavol
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Publication number: 20140110849Abstract: A copper-titanium alloy sputtering target comprising 3 at % or more and less than 15 at % of Ti and a remainder made up of Cu and unavoidable impurities, wherein a variation (standard deviation) in hardness is within 5.0 and a variation (standard deviation) in electric resistance is within 1.0 in an in-plane direction of the target. Provided are: a sputtering target for forming a copper-titanium alloy wiring line for semiconductors capable of causing the copper alloy wiring line for semiconductors to be equipped with a self-diffusion suppressive function, effectively preventing contamination around the wiring line caused by diffusion of active Cu, improving electromigration (EM) resistance, corrosion resistance and the like, enabling the arbitrary formation of a barrier layer in a simple manner, and uniformizing film properties; a copper-titanium alloy wiring line for semiconductors; and a semiconductor element and a device each equipped with the semiconductor wiring line.Type: ApplicationFiled: February 15, 2012Publication date: April 24, 2014Applicant: JX NIPPON MINING & METALS CORPORATIONInventors: Tomio Otsuki, Atsushi Fukushima
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Publication number: 20140110256Abstract: Provided is a silicon target material in which particles are not easily generated during a sputtering process and to form a low-defect (high quality) silicon-containing film. A silicon target material having a specific resistance of 20 ?·cm or more at room temperature is used for forming a silicon-containing film. The silicon target material may be polycrystalline or noncrystalline. However, when the silicon target material is single-crystalline, a more stable discharge state can be obtained. Also, a single-crystal silicon in which crystals are grown by an FZ method is a preferable material as a highly-pure silicon target material because its content of oxygen is low. Further, a target material having n-type conductivity and containing donor impurities is preferable to obtain stable discharge characteristics. Only a single or a plurality of silicon target materials according to the present invention may be used for sputtering film formation of the silicon-containing film.Type: ApplicationFiled: December 23, 2013Publication date: April 24, 2014Applicant: Shin-Etsu Chemical Co., Ltd.Inventors: Hideo KANEKO, Yukio INAZUKI, Hiroki YOSHIKAWA
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Publication number: 20140110249Abstract: The purpose of the present invention is to provide a sputtering target with which a film having excellent characteristics can be obtained. A sputtering target (100) is constituted of a plurality of target members (10), a backing plate (20), a bonding agent (30), and protective members (50). The plurality of target members (10) and the backing plate (20) are bonded to each other with the bonding agent (30) therebetween. On a backing plate (20) surface that corresponds in position to gaps (15) between adjacent target members (10), grooves (40) are formed. Each of the grooves (40) is provided with the protective members (50), which are composed of the same material as that of the target members (10). The width (W2) of the protective members (50) is greater than the width (W1) of the gaps (15), and is less than the width (W3) of the grooves (40). The thickness (T4) of the protective members (50) is larger than the depth (D1) of the grooves (40).Type: ApplicationFiled: February 24, 2012Publication date: April 24, 2014Applicant: Sharp Kabushiki KaishaInventors: Yohsuke Kanzaki, Takatsugu Kusumi, Naohiro Tamari, Masao Moriguchi
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Patent number: 8702919Abstract: Sputtering targets are described that comprise: a) a target surface component comprising a target material; b) a core backing component having a coupling surface, a back surface and at least one open area, wherein the coupling surface is coupled to at least part of the target surface component; and wherein at least part of the target surface component fits into at least one open area of the core backing component. In some embodiments, the target surface component, the core backing component or a combination thereof have at least one surface area feature coupled to or located in the back surface of the core backing component, the target surface component or a combination thereof, wherein the surface area feature increases the cooling effectiveness of the target surface component.Type: GrantFiled: August 13, 2007Date of Patent: April 22, 2014Assignee: Honeywell International Inc.Inventors: Stephane Ferrasse, Werner H. Hort, Jaeyeon Kim, Frank C. Alford
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Publication number: 20140103268Abstract: A sputtering target including indium (In), tin (Sn) and zinc (Zn) and an oxide including one or more elements X selected from the following group X, the atomic ratio of the elements satisfying the following formulas (1) to (4): Group X: Mg, Si, Al, Sc, Ti, Y, Zr, Hf, Ta, La, Nd, Sm 0.10?In/(In+Sn+Zn)?0.85??(1) 0.01?Sn/(In+Sn+Zn)?0.40??(2) 0.10?Zn/(In+Sn+Zn)?0.70??(3) 0.70?In/(In+X)?0.Type: ApplicationFiled: May 7, 2012Publication date: April 17, 2014Inventors: Masayuki Itose, Mami Nishimura, Misa Sunagawa, Masashi Kasami, Koki Yano
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Publication number: 20140102879Abstract: [Object] To provide a method and an apparatus for manufacturing a variable resistance element by which a metal oxide layer having a desired resistivity can be precisely formed. [Solving Means] The method of manufacturing the variable resistance element according to an embodiment of the present invention includes a step of forming a first metal oxide having a first resistivity and a step of forming a second metal oxide having a second resistivity different from the first resistivity. The first metal oxide is formed on a substrate by sputtering, while sputtering a first target made of an oxide of metal, a second target made of the metal with a first power. The second metal oxide layer is formed on the first metal oxide layer by sputtering the second target with a second power different from the first power while sputtering the first target.Type: ApplicationFiled: June 7, 2012Publication date: April 17, 2014Applicant: ULVAC, INC.Inventors: Yutaka Nishioka, Kazumasa Horita, Natsuki Fukuda, Shin Kikuchi, Youhei Ogawa, Koukou Suu
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Publication number: 20140102893Abstract: [Object] Provided are a Zn—Sn—O-based oxide sintered body which is used as a sputtering target or a tablet for vapor deposition and which is resistant to crack formation and the like during film formation, and a method for producing the same. [Solving means] The oxide sintered body is characterized in that tin is contained with an atomic ratio of Sn/(Zn+Sn) being 0.01 to 0.6, an average crystal particle diameter of the sintered body is 4.5 ?m or less, and a degree of orientation represented by I(222)/[I(222)+I(400)] is 0.52 or more, where I(222) and I(400) represent integrated intensities of the (222) plane and the (400) plane of a Zn2SnO4 phase measured by X-ray diffraction using the CuK? radiation.Type: ApplicationFiled: June 21, 2012Publication date: April 17, 2014Applicant: SUMITOMO METAL MINING CO., LTD.Inventors: Kentaro Sogabe, Makoto Ozawa
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Publication number: 20140102891Abstract: A method of manufacturing improved thin-film solar cells entirely by sputtering includes a high efficiency back contact/reflecting multi-layer containing at least one barrier layer consisting of a transition metal nitride. A copper indium gallium diselenide (Cu(InXGa1-X)Se2) absorber layer (X ranging from 1 to approximately 0.7) is co-sputtered from specially prepared electrically conductive targets using dual cylindrical rotary magnetron technology. The band gap of the absorber layer can be graded by varying the gallium content, and by replacing the gallium partially or totally with aluminum. Alternately the absorber layer is reactively sputtered from metal alloy targets in the presence of hydrogen selenide gas. RF sputtering is used to deposit a non-cadmium containing window layer of ZnS. The top transparent electrode is reactively sputtered aluminum doped ZnO. A unique modular vacuum roll-to-roll sputtering machine is described.Type: ApplicationFiled: December 12, 2013Publication date: April 17, 2014Applicant: MiaSoleInventor: Dennis R. Hollars
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Publication number: 20140102892Abstract: A sputtering target including indium (In) and zinc (Zn) and an oxide including one or more elements X selected from the following group X, the atomic ratio of the elements satisfying the following formulas (1) and (2): Group X: Mg, Si, Al, Sc, Ti, Y, Zr, Hf, Ta, La, Nd, Sm 0.30?In/(In+Zn)?0.90??(1) 0.70?In/(In+X)?0.99??(2).Type: ApplicationFiled: May 8, 2012Publication date: April 17, 2014Applicant: Idemitsu Kosan Co., Ltd.Inventors: Masayuki Itose, Mami Nishimura, Misa Sunagawa, Masashi Kasami, Koki Yano
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Patent number: 8696879Abstract: The invention provides methods and equipment for depositing a low-maintenance coating.Type: GrantFiled: September 3, 2010Date of Patent: April 15, 2014Assignee: Cardinal CG CompanyInventors: Kari B. Myli, Annette J. Krisko, John R. German, Klaus Hartig
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Publication number: 20140097084Abstract: Provided is a high-purity copper-manganese-alloy sputtering target comprising 0.05 to 20 wt % of Mn and the remainder being Cu and inevitable impurities. The high-purity copper-manganese-alloy sputtering target is characterized in that the in-plane variation (CV value) in Mn concentration of the target is 3% or less. It is thus possible to form a thin film having excellent uniformity by adding an appropriate amount of a Mn element to copper and reducing the in-plane variation of the sputtering target. In particular, there is provided a high-purity copper-manganese-alloy sputtering target which is useful for improving the yield and the reliability of semiconductor products which are making progress in a degree of refinement and integration.Type: ApplicationFiled: September 6, 2012Publication date: April 10, 2014Applicant: JX NIPPON MINING & METALS CORPORATIONInventors: Kenichi Nagata, Tomio Otsuki, Takeo Okabe, Nobuhito Makino, Atsushi Fukushima
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Publication number: 20140093672Abstract: Provided is a recording film for an optical information recording medium with which it is possible to meet all predetermined characteristics requirements and increase productivity while reducing the number of layers in the optical information recording medium. The present invention relates to a recording film for an optical information recording medium on which recording is performed by laser light irradiation, wherein the recording film for an optical information recording medium includes: Mn; at least one element (group X element) selected from the group consisting of Bi, Ag, Co, Cu, In, Sn, and Zn (group X); and oxygen (O). At least some of the Mn and at least some of the group X element are oxidized.Type: ApplicationFiled: May 30, 2012Publication date: April 3, 2014Applicant: Kabushiki Kaisha Kobe Seiko Sho (Kobe Steel, Ltd.)Inventors: Yoko Shida, Yuki Tauchi
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Publication number: 20140083847Abstract: Provided is a sintered sputtering target having a composition by atomic ratio represented by the formula: (Fe100-X—PtX)100-ACA (wherein A and X satisfy 20?A?50 and 35?X?55, respectively), wherein C particles are finely dispersed in a matrix alloy, and an oxygen content is 300 wt ppm or less. An object of the present invention is to provide an Fe—Pt based sputtering target having finely dispersed C particles and a low oxygen content, which allows manufacture of a granular structure magnetic thin film having excellent corrosion resistance, and further allows facilitation of ordering the L10 structure.Type: ApplicationFiled: July 20, 2012Publication date: March 27, 2014Applicant: JX Nippon Mining & Metals CorporationInventor: Atsushi Sato
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Patent number: 8679268Abstract: A ferromagnetic sputtering target comprising metal having a composition containing 20 mol % or less of Cr, and Co as the remainder; wherein the target structure includes a basis metal (A), and flat phases (B), containing 90 wt % or more of Co, within the basis metal (A), the average grain size of the phases (B) is 10 ?m or more and 150 ?m or less, and the average aspect ratio of the phases (B) is 1:2 to 1:10. Provided is a ferromagnetic sputtering target capable of inhibiting the generation of particles during sputtering, and improving the pass-through flux to achieve a stable electrical discharge with a magnetron sputtering device.Type: GrantFiled: September 30, 2010Date of Patent: March 25, 2014Assignee: JX Nippon Mining & Metals CorporationInventors: Shin-ichi Ogino, Atsushi Sato, Yuichiro Nakamura, Atsutoshi Arakawa
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Publication number: 20140072498Abstract: A method of manufacture is described that uses liquid phase reduction of silicon hydride, to produce silicon metal. Working in liquid phase permits a more compact plant design and offers significantly lower capital costs.Type: ApplicationFiled: November 13, 2013Publication date: March 13, 2014Applicant: Boston Silicon Materials, LLCInventor: Andrew Matheson
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Patent number: 8668785Abstract: Provided is a method of producing high purity ytterbium, wherein the high purity ytterbium is obtained by reducing crude ytterbium oxide in a vacuum with reducing metals composed of metals having a low vapor pressure, and selectively distilling ytterbium. Additionally provided are methods of achieving the high purification of ytterbium which has a high vapor pressure and is hard to refine in a molten state, and high purity ytterbium obtained thereby. Further provided is technology for efficiently and stably obtaining a sputtering target made of high purity material ytterbium, and a thin film for metal gates containing high purity material ytterbium.Type: GrantFiled: September 24, 2008Date of Patent: March 11, 2014Assignee: JX Nippon Mining & Metals CorporationInventors: Yuichiro Shindo, Kazuto Yagi
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Publication number: 20140061549Abstract: Disclosed is a process to reduce mixtures of at least one metal halide by molten metal reduction of the liquid phase metal halide in an alkali or alkaline earth metal to form a reaction product comprising at least one metal mixture and a halide salt coating, in which the at least one metal halide is in stoichiometric excess to the molten metal reductant and wherein the reductant is consumed in the reaction and does not need to be removed at the end of the reaction.Type: ApplicationFiled: November 13, 2013Publication date: March 6, 2014Applicant: Boston Electronic Materials, LLCInventor: Andrew Matheson
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Patent number: 8663440Abstract: The object of this invention is to provide a high quality titanium target for sputtering capable of reducing the impurities that cause generation of particles and abnormal discharge, which is free from fractures and cracks during high power sputtering (high rate sputtering), and capable of stabilizing the sputtering properties and effectively suppressing the generation of particles upon deposition. This invention is able to solve foregoing problems using a high purity titanium target for sputtering containing, as additive components, 3 to 10 mass ppm of S and 0.5 to 3 mass ppm of Si, and in which the purity of the target excluding additive components and gas components is 99.995 mass percent or higher.Type: GrantFiled: September 28, 2010Date of Patent: March 4, 2014Assignee: JX Nippon Mining & Metals CorporationInventors: Shiro Tsukamoto, Tomio Otsuki
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Patent number: 8663438Abstract: The invention relates to a target arrangement comprising a tubular-shaped carrier element and a hollow-cylindrical target having at least one target material, said target comprising at least one one-piece tube segment which at least partially surrounds the carrier element. Said carrier element and the tube segment are partially interconnected in a material fit by at least two plastically deformable compensating means. The invention also relates to a method for producing said type of target arrangement and a tubular segment.Type: GrantFiled: February 14, 2007Date of Patent: March 4, 2014Assignee: GFE Fremat GmbHInventors: Grit Hüttl, Folke Steinert, Joachim Wagner
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Patent number: 8663439Abstract: A sputtering target for producing a metallic glass membrane characterized in comprising a structure obtained by sintering atomized powder having a composition of a ternary compound system or greater with at least one or more metal elements selected from Pd, Zr, Fe, Co, Cu and Ni as its main component (component of greatest atomic %), and being an average grain size of 50 ?m or less. The prepared metallic glass membrane can be used as a substitute for conventional high-cost bulk metallic glass obtained by quenching of molten metal. This sputtering target for producing the metallic glass membrane is also free from problems such as defects in the metallic glass membrane and unevenness of composition, has a uniform structure, can be produced efficiently and at low cost, and does not generate many nodules or particles. Further provided is a method for manufacturing such a sputtering target for forming the metallic glass membrane.Type: GrantFiled: November 4, 2005Date of Patent: March 4, 2014Assignees: JX Nippon Mining & Metals Corporation, Tohoku UniversityInventors: Atsushi Nakamura, Masataka Yahagi, Akihisa Inoue, Hisamichi Kimura, Shin-ichi Yamaura
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Patent number: 8663402Abstract: A sputtering target and surface processing method is provided. Intermetallic compounds, oxides, carbides, carbonitrides and other substances without ductility exist in the target surface in a highly ductile matrix phase at a volume ratio of 1 to 50%. The target surface is preliminarily subjected to primary processing of cutting work, and then subsequently subjected to finish processing via polishing. The sputtering target subject to this surface processing has an improved target surface with numerous substances without ductility and prevents or suppresses the generation of nodules and particles upon sputtering.Type: GrantFiled: February 11, 2011Date of Patent: March 4, 2014Assignee: JX Nippon Mining & Metals CorporationInventors: Yuichiro Nakamura, Akira Hisano
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Patent number: 8658009Abstract: This Cu alloy sputtering target includes, in terms of atomic percent: Al: 1% to 10%; and Ca: 0.1% to 2%, with the balance being Cu and 1% or less of inevitable impurities. This thin film transistor includes: a gate electrode layer joined to the surface of a glass substrate through an adhesion layer; a gate insulating layer; a Si semiconductor layer; an n-type Si semiconductor layer; a barrier layer; a wire layer composed of a drain electrode layer and a source electrode layer, both of which are mutually divided; a passivation layer; and a transparent electrode layer, wherein the barrier layer is formed by sputtering under an oxidizing atmosphere using the Cu alloy sputtering target.Type: GrantFiled: October 22, 2009Date of Patent: February 25, 2014Assignees: Mitsubishi Materials Corporation, Ulvac, Inc.Inventors: Kazunari Maki, Kenichi Yaguchi, Yosuke Nakasato, Satoru Mori
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Publication number: 20140048414Abstract: Provided are a sputtering target which has excellent machinability and is capable of forming a compound film that mainly contains Cu and Ga and a method for producing the sputtering target. The sputtering target of the present invention has a component composition that contains 20 to 40 at % of Ga, 0.1 to 3 at % of Sb, and the balance composed of Cu and unavoidable impurities. A method for producing the sputtering target includes a step of producing a starting material powder that is obtained by pulverizing at least Cu, Ga and Sb as simple substances or an alloy that contains two or more of these elements; and a step of subjecting the starting material powder to hot processing in a vacuum, in an inert atmosphere or in a reducing atmosphere, wherein Ga is contained in the starting material powder in the form of a Cu—Ga alloy or in the form of a Ga—Sb alloy.Type: ApplicationFiled: April 20, 2012Publication date: February 20, 2014Applicant: Mitsubishi Materials CorporationInventors: Shoubin Zhang, Masahiro Shoji
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SPUTTERING TARGET AND ORGANIC LIGHT-EMITTING DISPLAY DEVICE INCLUDING BLACK MATRIX DEPOSITED THEREBY
Publication number: 20140048782Abstract: A sputtering target and an organic light-emitting display device including a black matrix deposited thereby. The sputtering target is used in a sputtering process for depositing a black matrix in an organic light-emitting display device. The sputtering target has a cermet structure in which a metal and a metal oxide are mixed.Type: ApplicationFiled: August 8, 2013Publication date: February 20, 2014Applicant: SAMSUNG CORNING PRECISION MATERIALS CO., LTD.Inventors: Jin Woo Han, Eui Soo Kim, Seung Won Park, Insung Sohn, You Min Shin -
SPUTTERING TARGET AND ORGANIC LIGHT-EMITTING DISPLAY DEVICE INCLUDING BLACK MATRIX DEPOSITED THEREBY
Publication number: 20140048783Abstract: A sputtering target that can form a black matrix having high-resistance and low-reflection characteristics and an organic light-emitting display device including the black matrix deposited thereby. The sputtering target that is used in a sputtering process for depositing a black matrix contains one selected from the group consisting of Mo—Si—O, W—Si—O and Mo—W—Si—O, the content of the Mo or W being at least 0.5 times the content of the Si.Type: ApplicationFiled: August 8, 2013Publication date: February 20, 2014Applicant: Samsung Corning Precision Materials Co., Ltd.Inventors: Jin Woo Han, Eui Soo Kim, Seung Won Park, JooSok Kim, Insung Sohn -
Patent number: 8652399Abstract: A sputtering target for producing a metallic glass membrane characterized in comprising a structure obtained by sintering atomized powder having a composition of a ternary compound system or greater with at least one or more metal elements selected from Pd, Zr, Fe, Co, Cu and Ni as its main component (component of greatest atomic %), and being an average grain size of 50 ?m or less. The prepared metallic glass membrane can be used as a substitute for conventional high-cost bulk metallic glass obtained by quenching of molten metal. This sputtering target for producing the metallic glass membrane is also free from problems such as defects in the metallic glass membrane and unevenness of composition, has a uniform structure, can be produced efficiently and at low cost, and does not generate many nodules or particles. Further provided is a method for manufacturing such a sputtering target for forming the metallic glass membrane.Type: GrantFiled: August 11, 2010Date of Patent: February 18, 2014Assignees: JX Nippon Mining & Metals Corporation, Tohoku UniversityInventors: Atsushi Nakamura, Masataka Yahagi, Akihisa Inoue, Hisamichi Kimura, Shin-ichi Yamaura
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Patent number: 8652306Abstract: To provide a method for manufacturing a mask blank capable of manufacturing a high quality mask blank that suppresses generation of defects in a thin film for forming a mask pattern with high yields, a method for manufacturing a transfer mask that manufactures the thin film of the mask blank by patterning, and a sputtering target used for manufacturing the mask blank. By using the sputtering target containing silicon and having a hardness of 900 HV or more in Vickers' hardness, the thin film for forming the mask pattern on a substrate is formed by sputtering, and the high quality mask blank that suppresses generating of defects is manufactured, and further the transfer mask is manufactured by patterning the thin film.Type: GrantFiled: August 19, 2003Date of Patent: February 18, 2014Assignee: Hoya CorporationInventor: Masaru Mitsui