Abstract: The present invention relates to a method of preparing a transparent moulding comprising a blend of a first thermoset polymeric material forming the matrix of said moulding, and of a second polymeric material dispersed within said first material, said method comprising at least the following stages: i) preparation of a liquid polymerizable mixture by dissolving said second polymeric material in a thermosetting polymerizable composition that is a precursor of said first thermoset polymeric material, ii) filling of a mould with the liquid polymerizable mixture obtained in stage i), iii) cooling of the liquid polymerizable mixture in the mould to a temperature T less than or equal to 0° C., iv) initiation of the polymerization of said cooled liquid polymerizable mixture at a temperature T? less than or equal to 0° C.

Abstract: A novel method is disclosed for the preparation of a sintered porous body of a metallic or ceramic powder having a closed cell texture and a porosity as high as 95% or higher. The method comprises the steps of: preparing a foamable aqueous slurried composition containing a powder of the metallic or ceramic material, a blowing agent and a binder resin which is a water-soluble polymer capable of becoming gelled; subjecting the slurried composition to gelation of the binder resin; subjecting the gelled mass of the composition to foaming by gas-evolution from the blowing agent; and heating the thus gelled and foamed body of the composition to effect drying and sintering of the particles of the metallic or ceramic powder.

Abstract: The present invention relates to an improved molding process and composition for lightweight synthetic fiber logs used in natural gas, propane and wood burning fireplaces. A method of manufacturing castable fireplace logs comprising the combination of inorganic fibers with a binder carrier mix to form logs of superior color and detail in a shortened production time frame.

Abstract: A method of manufacturing a sintered body is provided. A molding powder, a gel-forming material powder and a solvent are mixed at a temperature not higher than a dissolving point of the gel-forming material. A treatment of pulverizing agglomerates containing the molding powder, gel-forming material powder and solvent absorbed in the gel-forming material powder is carried out. The mixture is then heated to a temperature not lower than the dissolving point thereby forming a sol. The sol is then cooled to a temperature not higher than the gel point, thereby forming a molding material. The molding material is used for producing a sintering body.

Abstract: The present invention discloses a method for forming scaffolds. This invention provides various fixation agents for different polymers or applications, and a fixation process is performed at low temperature. Moreover, the method comprises a dissolution process, a temperature adjusting process, a freezing process and a fixation process, wherein the fixation process is selected from the group of a solid-liquid exchange process, a neutralization process and a gelation process.

Abstract: The present invention relates generally to a flexible plastic substrate, its manufacturing process and optical components for optical display applications. In so doing, cyclic olefin copolymer (COC) is placed between upper and lower heat-resistant sheets, then heated and pressurized by hot press to form a COC film. Next, the film is subjected to quenching treatment in ice water, and then heat treatment in vacuum drying oven after being placed between two flat plates. Finally, a COC plastic substrate with a high degree of optical penetration, low water permeability and low roughness is shaped, which can be efficiently applied to optical display thanks to its simple processing, lightweight, thin-profile and flexibility.

Abstract: A method of separating a poly(arylene ether) from a solvent includes treating a poly(arylene ether)-containing solution with a devolatilizing extruder to form an extruded composition, and cooling the extruded composition with a cooling device that does not immerse the extruded composition in water. The composition may be used to isolate a poly(arylene ether) from the solvent-containing reaction mixture in which it is prepared, or to remove solvent from a multi-component poly(arylene ether)-containing thermoplastic composition.

Abstract: A method for fabricating an aeration stone is disclosed, which abandoned activated sludge, red soil and an alkaline metal oxide are separately dried firstly and then cracked, and next the cracked abandoned activated sludge, red soil and alkaline metal oxide are separately sieved to obtain smaller grains thereof, and then the grains are separately ground into fine particles thereof and are mixed to be a mixture. Next, the mixture is molded into a green aeration stone. Next, the green aeration stone is fired at a high temperature and then cooled down to obtain a finished aeration stone. Therefore, the present invention recycles the abandoned sludge of wastewater treatment works to reduce the secondary pollution of abandoned sludge.

Abstract: A dope is cast onto a drum whose surface is cooled, so as to form a casting film. After the peeling of the casting film, a cleaning gas containing dry ice particles is applied to a periphery of the casting drum with use of a drum cleaning unit. Thus the dry ice particles collide to the periphery of the casting drum, and the colliding energy is effective of removing from the periphery an organic material adhered on the casting drum. The organic material mainly contains aliphatic acid, aliphatic acid ester and metal salt of aliphatic acid. Before the increase of the amount of the organic material, it is removed and therefore isn't transmitted onto the surface of the casting film. Thus a high quality film having no optical unevenness is produced without the decrease of the productivity.

Abstract: An aqueous solution of polyacrylic acid is placed in a mold, frozen, and freeze-dried to form a sponge-like polyacrylic acid structure. The sponge-like polyacrylic acid structure is compressed by the application of heat and pressure to reduce the thickness and increase the density of the sponge-like polyacrylic acid structure to form a densified polyacrylic acid structure. The densified polyacrylic acid structure is preconditioned by heating to form a wound dressing. The wound dressing can be applied to control severe, life-threatening bleeding from a wound at a wound site of a person.

Abstract: Methods of forming supple tissue dressing assemblies from hydrophilic polymer sponge structures, such as chitosan, by uniformly cooling the sponge structure and freezer from above freezing to below freezing. The supple tissue dressing assemblies are characterized by suppleness or multi-dimensional flexibility. The assemblies can be flexed, bent, folded, twisted, and even rolled upon itself before and during use, without creasing, cracking, fracturing, otherwise compromising the integrity and mechanical and/or therapeutic characteristics of the assemblies.

Abstract: Latex articles with geometrically defined surface structure providing enhanced grip characteristics in dry, wet or oily environment; and a method of making same comprising applying a polymeric coagulant coating to a smooth former surface, wherein the coating becomes tacky during drying, applying discrete coagulant particles of selected size, shape and distribution to the tacky coating to attach and protrude from the former surface with the polymeric coagulant coating, dipping the former into an aqueous latex emulsion, wherein the polymeric coagulant coating and the discrete coagulating particles destabilize the latex, thereby developing a latex layer, vulcanizing and stripping the latex article inside out, and dissolving the discrete coagulant particles in water or suitable solvents to reveal the geometrically designed texture with pre-selected size, shape and distribution of impressions providing improved dry, wet and oily surface grip by removal of a fluid boundary layer.

Abstract: The present invention relates to a process for fabricating molded structures having a radially organized pore structure. The molded structures are formed using a spinning-induced sedimentation technique such that sedimentation of a multi-component liquid suspension produces the internal geometry and porosity of the structure. The porous molded structures of the invention can be used in a number of applications including tissue and organ engineering, dialysis and phase separation membranes and water and liquid waste purification systems.

Abstract: A method of manufacturing a chemical-mechanical polishing (CMP) pad comprises the steps of (a) forming a layer of a polymer resin liquid solution (i.e., a polymer resin dissolved in a solvent); (b) inducing a phase separation in the layer of polymer solution to produce an interpenetrating polymeric network comprising a continuous polymer-rich phase interspersed with a continuous polymer-depleted phase in which the polymer-depleted phase constitutes about 20 to about 90 percent of the combined volume of the phases; (c) solidifying the continuous polymer-rich phase to form a porous polymer sheet; (d) removing at least a portion of the polymer-depleted phase from the porous polymer sheet; and (e) forming a CMP pad therefrom.

Abstract: A tire mold for molding a rubber or plastic article includes an aluminum tire mold having an internal mold cavity, at least one vent hole of a selected diameter extending from the mold cavity to the exterior of the mold. A metal vent plug is operatively disposed within the vent hole such that air may be released through the vent hole from the internal mold cavity to the exterior of the mold upon heating the entire mold during molding of the rubber or plastic article, but prevents any rubber or plastic from entering the vent hole during molding of the rubber article. This is done by heating the aluminum tire mold, then inserting a metal vent plug into each vent hole; then cooling the entire aluminum tire mold with the metal vent plug to room temperature; then freezing the aluminum tire mold to a temperature of at least about ?100° F. for at least one-half hour such that the aluminum tire mold deforms around each metal vent plug; and finally, removing the mold from the freezing conditions.

Abstract: A wear resistant hydrogel for use as a prosthetic implant, such as for cartilage, is made by forming a solution of polyvinyl alcohol in a solvent of DMSO/water. The solution is placed in a mold and is gelated by cycling the mold in a freeze-thaw cycle at a temperature at or below 4° C. for a period of 2 to 24 hours. The hydrogel so formed is washed in a saline solution, including potassium carbonate. The hydrogel is then dehydrated to 20 to 70% water content and thereafter irradiated with Gamma radiation. The surface of the hydrogel is then cross-linked using a boric acid solution preferably between 2.5 and 5% for about 1 minute. The hydrogel is then rinsed and sterilized.

Abstract: A solution casting process for producing cellulose triacetate (TAC) film is provided. Bead of dope, which includes cellulose triacetate and solvent, is cast on to a rotating supporting drum, to form self-supporting cast film. The self-supporting cast film is stripped from the supporting drum. The self-supporting cast film is dried while the self-supporting cast film being stripped is fed by feed rollers, to form the cellulose triacetate film. A surface temperature of the feed rollers is set equal to or lower than 0° C. The self-supporting cast film upon being stripped has modulus of longitudinal elasticity equal to or more than 450,000 Pa.

Abstract: Cellulose triacetate film is produced by a solution casting process. Dope, which includes cellulose triacetate and mixed solvent with methyl acetate, is cast on a rotary drum in a form of bead by use of a flow casting die, to form gel film. When a self-supporting characteristic of the gel film becomes higher than one limit value, the gel film is stripped from the rotary drum by use of a stripping roller, to obtain the cellulose triacetate film. During the casting step, a surface of the rotary drum is cooled at ?10° C. or lower.

Abstract: A process for preparing artificial bone is described which comprises: (i) preparing a mixture of a finely divided bio-compatible ceramic powder, an organic binder and a pore-forming agent in an inert liquid to form a body and causing at least some of the pore-forming agent to align along a common axis; (ii) optionally shaping the resulting body; (iii) allowing the pore-forming agent to form a porous structure in the body; (iv) heating the shaped body to a temperature sufficient to fix the porous structure and; (v) further heating the body to eliminate residues of organic binder and pore-forming agent and to fuse it.

Abstract: Processes for the preparation of adherent polyvinylidene fluoride, hexafluoropropylene coatings on objects and for the direct production of open celled foams from a polymer latex without a need for any blowing agent.

Abstract: A method and apparatus for removing a polymeric contact lens from a mold comprising lowering the temperature of the contact lens with a cryogenic material, such as liquid nitrogen, to a temperature and for a time sufficient for the lens to release from the mold without the application of external forces.

Abstract: In a cellulose acylate solution, cellulose acylate is dissolved in an essentially non-chlorinated solvent. The essentially non-chlorinated solvent is a mixture of a ketone having a solubility parameter of 19 to 21 and an ester having a solubility parameter of 19 to 21. The solution further contains a releasing agent.

Abstract: This invention is concerned with a method for producing water-insoluble polysaccharides. A method for making the water-insoluble bio-compatible gel includes activating the hydroxyl-containing polysaccharides with the activating agent to form activated polysaccharides, and cross-linking the activated polysaccharides, under moderate conditions producing different shapes of the water-insoluble bio-compatible gel. The water-insoluble bio-compatible gels, films, porosities, powders, sheets, fibers and spheres of this invention may be applied to various medical and cosmetic uses.

Abstract: The invention provides biopolymer sponge tubes closed at one end for use in surgery. The preferred biopolymer iscollagen. The biopolymer sponge tubes are prepared by forming an aqueous dispersion of the biopolymer, introducing the dispersion into tube-shaped moulds, freezing the dispersion in the moulds to form a shaped, aqueous dispersion, followed by freeze-drying the frozen aqueous dispersion. The tubes are fitted over endoscopic surgical staplers to provide improved sealing of stapled tissues, especially for air-tight sealing in lung resections.

Abstract: The present invention relates to a method for preparing an injectable composition of microparticles for the sustained release of a biologically active agent. The microparticles include a biocompatible polymer and a biologically active agent. The invention provides an improved process for the preparation of microparticles, wherein the physical characteristics of the microparticles, for example, the morphology, density and size, are independent of the process used to prepare the initially formed polymer/drug matrix. The method includes the steps of (a) providing a polymer/biologically active agent matrix; (b) compressing the polymer/biologically active agent matrix, thereby forming a compressed matrix; and (c) fragmenting the compressed matrix, thereby forming an injectable microparticle composition. The polymer/drug matrix can be provided by any suitable method.

Abstract: An assembly and method for forming a frozen confection portion of a frozen confection type food product, the assembly comprising a mold assembly provided with a mold cavity of a selected configuration ad formed by a flexible inert casing, a pump for moving confection into the mold cavity and casing to fill the mold cavity and casing, sealing means for sealing the ends of the casing to provide a link of confection, a cutter device for separating the link from adjoining links, freezing devices for receiving and further freezing the link, and apparatus for opening the casing of the link and permitting the frozen confection to exit out of the casing in the selected configuration.

Abstract: A process for producing a low-profile, high-strength dilatation catheter balloon is disclosed. The process comprises forming a tubular extrudate and quenching said extrudate in a cryogenic fluid. The quenched extrudate has morphology of a largely disordered material. The crystallinity in the extrudate is no more than 15%. The crystallinity of the extrudate is measured using X-ray crystallography or DSC. The extrudate is further processed in a mold in which the extrudate is longitudinally and radially stretched. The stretched extrudate is finally attached as a balloon to the distal end of a catheter.

Abstract: The invention relates to a method for the solvent-free preparation of a homogenisate, especially for implants or microparticles, wherein

Abstract: A method of removing substantially all of the volatile component in a green, volatile-containing ceramic article is disclosed. The method comprises freezing the ceramic article; and then subjecting the frozen article to a vacuum for a sufficient time to freeze-dry the article. Frequently, the article is heated while being freeze-dried. Use of this method efficiently reduces the propensity for any warpage of the article. The article is often formed from a ceramic slurry in a gel-casting process. A method for fabricating a ceramic core used in investment casting is also described.

Abstract: A microporous membrane is produced by cooling a solution comprising a vinylidene fluoride homopolymer or copolymer having a weight average molecular weight of 1×105 or more and a solvent therefor, to form a two-phase gel, said microporous membrane comprising a polymer phase comprising said vinylidene fluoride homopolymer or copolymer, and intercommunicating voids which have an average pore size measured by the half-dry method of 0.005 to 5 &mgr;m and range from one side of the membrane to the other side, and said microporous membrane having as its internal structure a percolation structure in which the polymer phase forms an isotropic network structure by three-dimensional branching in arbitrary directions, the voids are formed by surrounding by said polymer phase of the network structure and intercommunicate with one another, and the ratio of the maximum pore size measured by the bubble point method to the average pore size measured by the half-dry method is 2.0 or less.

Abstract: Disclosed is a thermoplastic polyurethane for slash molding, excellent in moldability, capable of providing a skin material having a uniform thickness, and capable of allowing a minute laser processing or the like to be vehicleried out thereon. Also, the present invention discloses a skin material comprising the thermoplastic polyurethane. The thermoplastic polyurethane of the present invention is prepared in a form of a powdery resin by mixing and then condensing an amount of 15-60 parts by weight of one or more isocyanate compounds; an amount of 30-70 parts by weight of an ether-containing polyester polyol; and an amount of 5-40 parts by weight of one or more chain extenders.

Abstract: A solution casting process for producing cellulose triacetate (TAC) film is provided. Bead of dope, which includes cellulose triacetate and solvent, is cast on to a rotating supporting drum, to form self-supporting cast film. The self-supporting cast film is stripped from the supporting drum. The self-supporting cast film is dried while the self-supporting cast film being stripped is fed by feed rollers, to form the cellulose triacetate film. A surface temperature of the feed rollers is set equal to or lower than 0° C. The self-supporting cast film upon being stripped has modulus of longitudinal elasticity equal to or more than 450,000 Pa.

Abstract: A method for cutting a honeycomb core which has a plurality of hollow tubular cells, wherein the method includes the steps of: filling or coating a hollow tubular cell of the honeycomb core with a resin composition that is in a gel state at an ordinary temperature; cooling the resin composition to a solid state; cutting the hollow tubular cell together with the resin composition in the solid state; allowing to stand or heating the resin composition to a gel state; and removing the resin composition in the gel state from the hollow tubular cell.

Abstract: The invention relates to a process for machining a flexible foam. The flexible foam is treated to temporarily harden the foam. The hardened foam is machined. The foam is then returned to its original flexible state.

Abstract: Cellulose triacetate film is produced by a solution casting process. Dope, which includes cellulose triacetate and mixed solvent with methyl acetate, is cast on a rotary drum in a form of bead by use of a flow casting die, to form gel film. When a self-supporting characteristic of the gel film becomes higher than one limit value, the gel film is stripped from the rotary drum by use of a stripping roller, to obtain the cellulose triacetate film. During the casting step, a surface of the rotary drum is cooled at −10° C. or lower.

Abstract: According to the invention a body may be produced in plastic, in particular by means of rotational casting method, by using a suspension or paste with plastic particles, comprising at least partly a thermoplastic elastomer, in particular SEBS, SBS or TPU. Said invention presents the advantage of no danger to health.

Abstract: A method for manufacturing pellets of hot-melt ink which solidifies with a cooling rate-dependent shrinkage, comprising the steps of filling molten ink into a mold formed by two mold dies, allowing the ink to cool down and to solidify in the mold, and opening the mold and removing the ink pellet therefrom, wherein in the cooling step, the ink is shock-cooled with a cooling rate that results in a shrinkage sufficient to cause the solidifying ink to separate from at least one of the mold dies.

Abstract: A method of making phosphorescent fiber having phosphorescent particles composed, by weight, of 55-62.5% of strontium oxide, 35-42.5% of aluminum oxide, 1-9% of dysprosium oxide and 0.5-1.5% of europium oxide encapsulated with a wall material. The encapsulated particles are mixed and pelletized at a weight ratio of 15-25:85-75 with polymer capable of fiber formation to give a master batch, which is then compounded at a weight ratio of 30-70:70-30 with a polymer mixture, in combination with a softener and a dispersing agent. Polymer mixture consists of two polymers. One is the same polymer used to produce a master batch, the other is a polymer in the same chemical structure but different in physical properties such as melt index and tenacity. The compounded chip is melt-spun at 190-290° C. through a melt extruder. The fibers with the encapsulated phosphorescent particles exhibit such excellent physical properties as to be applicable to various textile products and show a high degree of luminescence.

Abstract: A method and apparatus for manufacturing a wire or cord for welding floor coverings, such as linoleum or artificial fiber floor covering. The wire or cord forms a fixed joint via thermal processes between separation edges of adjacent sections of floor coverings provided with colors and patterns such that minimal difference is apparent between the floor covering and the cord or wire. A mixture of colored granules is subjected to a process of mixing, heating, and cooling adapted to form solid sheets that are cut to form the cord or wire.

Abstract: The present invention is directed to methods of making biodegradable films and biodegradable precursor films having enhanced breathability and ductility. The method includes blending a water soluble polymer and a biodegradable polymer to form a blended polymer mixture. The biodegradable polymer is preferably a biodegradable aliphatic polyester, and the water-soluble polymer is preferably polyethylene oxide and/or polyethylene glycol. The blended polymer mixture is formed into a precursor film. The precursor film is further processed to form a breathable biodegradable film.

Abstract: The present invention provides a process and apparatus for preserving the potency of a tableted heat sensitive ingredient. The process includes the steps of forming the ingredient into a tablet and cooling the tablet for a sufficient time and at a sufficiently low temperature to decrease the heat degradation of the ingredient. The process may be carried out in any number of tablet cooling apparatus, including a conduit forming a passageway for receiving tablets from the tablet press. A coolant inlet is connected to the conduit for supplying coolant into the passageway and into contact with the tablets.

Abstract: The present invention provides a biomedical, biocompatible, polymeric foam scaffold suitable for use in the repair and regeneration of tissue and which contains located therein a network of, branched channels that are effective to encourage and facilitate vascularization and tissue growth within the scaffold and to methods for making such biomedical scaffolds.

Abstract: A process for preparing artificial bone is described which comprises: (i) preparing a mixture of a finely divided bio-compatible ceramic powder, an organic binder and a pore-forming agent in an inert liquid to form a body and causing at least some of the pore-forming agent to align along a common axis; (ii) optionally shaping the resulting body; (iii) allowing the pore-forming agent to form a porous structure in the body; (iv) heating the shaped body to a temperature sufficient to fix the porous structure and; (v) further heating the body to eliminate residues of organic binder and pore-forming agent and to fuse it.

Abstract: The invention provides pellets of a saponified ethylene-vinyl acetate copolymer which are excellent in feedability, cause little fluctuation of extruder torque or discharge during molding, and yield shaped articles with high dimensional accuracy such as the high accuracy of form and thickness. The pellets of the invention are such that the differential curve representing the magnitude of change in the cumulative pore volume curve generated by measuring the fractional volume of surface pores by the mercury intrusion method has no peak within the pore diameter range of 1×102˜1×104 Å.

Abstract: Described herein are polypeptide fibers, such as silk fibers, produced by regeneration and methods for making the fibers.

Abstract: A method for making a prototype mold includes step 1: to prepare thermoplastic liquid by mixing hollow particles and resin; step 2: to crush used prototype molds into 5 mm to 10 mm particles; step 3: to mix the crushed particles in step 2 with the thermoplastic liquid; step 4: to eliminate bubbles in the mixture of the thermoplastic liquid and the crushed particles; step 5: to pour the mixture of the thermoplastic liquid and the crushed particles in a mold to make a product; step 6: to heat the product in step 5 at 60 to 200 degrees Celsius for 0.5 to 120 hours; step 7: to heat the product in step 6 at 60 to 80 degrees Celsius for 8 to 12 hours to obtain a stable crystal structure; step 8: to take the product from the mold, and step 9: to trim the product.

Abstract: Processes for the preparation of adherent polyvinylidene fluoride, hexafluoropropylene coatings on objects and for the direct production of open celled foams from a polymer latex without a need for any blowing agent.

Abstract: It is an object of the present invention to overcome the problem of fibrillation which is a drawback found in solvent-spun regenerated cellulosic fibers and to thereby provide high-quality regenerated cellulosic fibers. The regenerated cellulosic fibers are produced by the use of a spinning dope of cellulose dissolved in a solvent containing N-methylmorpholine N-oxide under the conditions that the average degree of polymerization of cellulose contained in the spinning dope is held to 400 or lower and 5% to 30% by weight of the cellulose is adjusted to a degree of polymerization of 500 or higher. Thus a pseudo-liquid-crystalline phenomenon can be allowed to occur in the stretched filaments during spinning, so that the resulting regenerated cellulosic fibers have improved resistance to fibrillation as well as improved dyeability and feeling.

Abstract: A surface reforming method for a plastic molded product of this invention is characterized by comprising a step (a) for immersing a plastic molded product into supercritical carbon dioxide or subcritical carbon dioxide under a temperature lower than the glass transition temperature of said plastic, and a step (b) for vaporizing carbon dioxide adhered to the surface of the plastic molded product under a temperature lower than the glass transition temperature of said plastic. A plastic molded product may be composed of a polymer having a polar group.

Abstract: A machine and a method to manufacture soap bars. The machine and method involve a die assembly (10) having a pair of die blocks (11, 12) which support co-operating dies (13, 14). Liquid nitrogen is delivered to the two dies (13, 14) via a throttling passage (18) to cool the soap material being formed.