Abstract: A method of charging fibrous webs with nonaqueous polar liquids. A web 20 that contains nonconductive fibers is wetted with a nonaqueous polar liquid 14. The web 20 is then substantially dried 22 to provide a fibrous electret web. The fibrous electret web can be used as a filter in a filtration face mask 40 that is adapted to cover the nose and mouth of the wearer. The present method has the advantage over known charging methods in that the nonaqueous liquid requires less energy for drying than is required for aqueous liquids. Additionally, many filter webs can be directly wetted with nonaqueous liquids, which cannot be easily wetted with aqueous liquids.

Abstract: A method for accelerating the release of a flammable blowing agent from an expanded foam is disclosed. According to the method, an expanded foam structure is perforated to form a first series of channels extending partially through its thickness from a first surface and a second series of channels extending partially through its thickness from a second surface opposite the first surface. The channels provide paths enabling the blowing agent to escape more rapidly from the interior of the expanded foam structure.

Abstract: Small particles of polymeric material are produced by expansion of a mixture of monomers and a propellant. The size and shape of the particles can be precisely tailored by materials selection and expansion conditions. Particles of 10 nanometers to 100 microns can be produced. If monomers exhibiting solid state reactivity are utilized, the particles thus formed can be polymerized at any time after formation. The particles produced by this method can be molecularly imprinted by incorporating a template into the particle prior to fully curing the particle, in a manner which allows selective extraction of the template from the cured particle after formation without deformation of the imprint site. A two step polymerization process allows the particles to be deposited on and adhered to a wide variety of substrates without additional agents.

Abstract: The allergens and extractable protein content of a latex device can be reduced by subjecting the un-cured latex device to a pre-cure leaching treatment with a solution containing a protease, followed by curing and a post-cure leaching treatment.

Abstract: A novel method of producing a porous product is provided, including the steps of: preparing a molded product by subjecting a molding material comprising a polymer component and a pore-forming agent dispersed in the polymer component, the pore-forming agent assuming a solid state at a room temperature, to molding at a temperature which causes the pore-forming agent to melt; and soaking the molded product with a solvent which dissolves the pore-forming agent but fails to dissolve the polymer component, to form pores.

Abstract: A polysaccharide sponge characterized by having: (i) an average pore size in the range between about 10 &mgr;m to about 300 &mgr;m; (ii) an average distance between the pores being the wall thickness of the pores in the range between about 5 &mgr;m to about 270 &mgr;m; and (iii) an E-modulus of elasticity being a measure of the rigidity of the sponge in the range of about 50 kPa to about 500 kPa.

Abstract: A system for producing blocks of open-cell, flexible polyurethane foam material and for conditioning each freshly-manufactured block to impart thereto optimal flexible foam properties. The system includes means to pour the flowable constituent of the foam material to be manufactured into a production station at the inlet of a conveyor, the constituents interacting to create on the conveyor a block of open-cell flexible foam material which is then wrapped in a plastic film casing that exposes the leading and trailing end of the block so that the encased block is open ended. The conveyor transports the wrapped block toward the rear end of a gate in a conditioning station having a port therein whose front end is coupled by an air duct to a suction fan.

Abstract: This invention discloses an apparatus and method for hydrating or washing ophthalmic devices, comprising the step of directing to an ophthalmic device having a higher concentration of impurities fluid which has previously been directed to ophthalmic device having a lower concentration of impurities.

Abstract: The invention relates to a method of removing water-insoluble binder from a porous article formed from pressed particulate material, such as tantalum powder. The invention provides a method capable of removing substantially all of the binder from the article for high purity applications, such as capacitor manufacture. The method comprises contacting the article with an aqueous solution of an agent which reacts with said binder to produce a water soluble derivative thereof whereby said binder derivative may be substantially dissolved in said solution. In a particular embodiment, the derivative is produced by hydrolysis of a fatty acid binder.

Abstract: A device useful for localized delivery of a therapeutic material is provided. The device includes a structure including a porous material; and a water-insoluble salt of a therapeutic material dispersed in the porous material. The water-insoluble salt is formed by contacting an aqueous solution of a therapeutic salt with a heavy metal water-soluble salt dispersed throughout a substantial portion of the porous material. The porous material can be made of a polymer other than fibrin with fibrin incorporated into the pores, which can be the only layer of polymeric material on the medical device (e.g., stent). A new method for preparing a porous polymer material on a medical device.

Abstract: A method of treating contact lenses made from polymerizable materials by providing supercritical fluids to the lenses.

Abstract: A method for dimensional stabilization treatment is disclosed which enables externally supplied high pressure steam to permeate well into interior of wood or wood composite, and which is thereby capable of constantly imparting high dimensional stability to the wood or wood composite. In the method, wood or wood composite W to be treated is held in a sealed space between two press platens 1a, 1b, and the sealed space is evacuated to establish reduced pressure therein, and thereupon, high pressure steam is supplied to the sealed space. The evacuation may be continued in parallel with the high pressure steam supply.

Abstract: A method of treating contact lenses made from polymerizable materials by providing supercritical fluids to the lenses.

Abstract: The present invention is a method for producing a nonwoven fabric from a water modifiable polyolefin-containing film. In order to produce the fabric where polyethylene is the minority constituent, a polymer blend is formed with the polyethylene as the dispersed phase and polyethylene oxide as the continuous phase. In another embodiment wherein the polyethylene is the majority constituent and the polyethylene oxide is the minority constituent of the film, a reactive blend created during processing exhibits an inverse phase morphology so that the polyethylene oxide becomes the continuous phase and the polyethylene becomes the dispersed phase. In either embodiment, the film is then treated with an aqueous solvent to remove the polyethylene oxide to produce the nonwoven, porous fabric. The resulting nonwoven, porous fabric has a silk-like hand and shine ideal for disposable personal hygiene articles, and is flushable through waste water disposal systems.

Abstract: Disclosed is a method of manufacturing a cellulose ester film, the method comprising the steps of dissolving a cellulose ester and a plasticizer in a solvent containing a cyclic diether solvent to obtain a cellulose ester solution, casting the solution on a support to form a cellulose ester film, separating the cellulose ester film from the support, and drying the separated film, wherein the water content of the solution is 0.06 to 15 weight %, and the residual solvent content in the film at the separation step is 50 to 450 weight %.

Abstract: An air filter comprising a laminate of a non-woven fabric made up of polyolefin fibers or polyester fibers or a composite of the non-woven fabrics and a PTFE porous film, wherein the amount of the total gases generated from the air filter is 20 .mu.g/g by the analysis of gas chromatography. The amount of the gases generated from the air filter is greatly reduced by heat-treating the non-woven fabric at a temperature of from 80 to 130.degree. C. for from 5 minutes to 20 minutes before or after laminating with the PTFE porous film.

Abstract: A method of manufacturing disposable, single-use lipstick samplers by means of a dipping process. In a preferred form, a reservoir containing molten lipstick wax material is provided, and a spindle which is disposed above the reservoir is advanceable toward and retractable away from the reservoir. A plastic cup-shaped form having an apertured tip is applied to the spindle, which is thereafter advanced so as to submerge the tip of the form into the molten liquid wax material. The spindle and coated form are then removed from the reservoir, and a vacuum is applied through the spindle to the aperture of the tip of the form, so as to draw lipstick wax material therefrom and into the interior of the spindle. The form is allowed to cool so as to solidify the wax, and thereafter is fitted with a cover, removed, and suitably packaged.

Abstract: The invention is concerned with a cellulose sponge which may be produced by mixing a solution of cellulose in an aqueous tertiary amine-oxide with a pore forming agent and a sponging agent and subsequently exposing it to conditions which cause a decomposition of the sponging agent and a foaming of the cellulose solution, whereafter the foamed cellulose is contacted with water to precipitate the cellulose.

Abstract: A process for production of a moulded ceramic and/or metallic body from a ductile material comprising one or more ceramic and/or metallic components, which material is fed into the pre-heated mould cavity (1) of a moulding tool. The moulded tool includes at least two mould parts (4, 5) of which at least one wholly or partly consists of a microporous material with communicating micropores. At least one mould cavity (1) comprising at least one mould surface (2, 3) exhibiting closed micropores is arranged in the microporous mould part (4, 5) or in a microporous section (6) thereof. The microporous mould part (4, 5) or the microporous section (6) thereof is pre-heated by supply of warm fluid, such as a heated gas. Said part (4, 5) or section (6) is after terminated moulding cooled by supply of cold fluid, such as a condensed gas. the invention includes in a further aspect a moulded body produced according to the process.

Abstract: A polishing pad for use in chemical-mechanical planarization (CMP) of semiconductor wafers includes a multiplicity of elongated microcolumns embedded in a matrix material body. The elongated microcolumns are oriented parallel to each other and extend from a planarizing surface used to planarize the semiconductor wafers. The elongated microcolumns are uniformly distributed throughout the polishing pad in order to impart uniform properties throughout the polishing pad. The polishing pad can also include elongated pores either coaxial width or interspersed between the elongated microcolumns to provide uniform porosity throughout the polishing pad.

Abstract: A powder injection molding composition or feedstock is made of 70% or more by weight of a powdered metal or ceramic and 30% or less by weight of a binder system. The binder system contains a sufficient amount of polypropylene or polyethylene to hold the so-called brown preform of the molded metal or ceramic powder together for the sintering step of the injection molding process and a sufficient amount of partially hydrolyzed cold water soluble polyvinyl alcohol, water and plasticizer to facilitate molding of the composition into the so-called green preform of the article to be manufactured. The debinding step of the injection molding process for transforming the green preform into the brown preform consists simply of immersing the green preform in water at ambient temperature to dissolve the polyvinyl alcohol. The binder system is nonhazardous, safe, harmless and fully degradable.

Abstract: A continuous process for heating a polybenzazole or polybenzothiazole filament, which includes the step of heating the filament to a temperature of at least 100.degree. C. but no greater than 290.degree. C. while applying a tension thereto of at least 3.5 grams per denier, which is carried out at a line speed of at least 100 m/minute; and there is no prior or subsequent heating of the fiber to any temperature greater than 300.degree. C. It has been discovered that placing tension on the filament while it is dried increases its tensile modulus without a significant decrease in its tensile strength.

Abstract: A method of and apparatus for molding and texturizing the upper surfaces of concrete products such as patio and paving stones following the steps of densifying and molding the concrete products and releasing them on pallets to a substantially horizontally traveling, longitudinally extending conveyor, then passing the concrete products continuously on the conveyor past an overhead force spraying station at a predesignated speed and directing a predetermined volumetric, overhead spray of liquid at a predetermined spray angle and pressure to progressively loosen some of the material and texturize the upper surfaces as the products move past the spraying station, and then before they have absorbed enough liquid to deleteriously affect their strength, either in the uncured or cured state, and, while they are continuing to travel along the conveyor, directing a flow of gas at the upper surfaces at a pressure to blow off the liquid and loosened material from the surfaces.

Abstract: A microporous membrane and method of manufacture is presented utilizing irradiation and thermal induction phase separation techniques. During manufacture, microsphereulites are created by irradiation of curable agents in a casted polyolefin film. The microsphereulites then serve as nucleating agents in a thermally-induced phase separation step, providing a microporous membrane with improved flow and mechanical properties.

Abstract: The bran has been less usable and have not been treated as industrial resources. The present invention is a method for producing a porous carbon material product and a hard porous carbon material product which have wide variety of functionalities utilizing such bran which is burned and carbonized stably. The method according to the present invention comprises of the steps of kneading bran with a thermosetting resin and an adequate amount of a solution including an adhesive paste or water, the bran is such as rice bran or wheat bran adjusted grain size; granulating the bran kneaded to predetermined grain size or less; molding the bran granulated in a metal mold by pressurizing and degassing to be a mold; burning and carbonizing the mold detached from the metal mold by heating to desired final burning temperature at a predetermined rate under inactive gas atmosphere or under vacuum; and cooling the mold from the final burning temperature to normal temperature at a predetermined rate.

Abstract: A sponge cloth of decrystallized cellulose modified by the acetyl group content, where the average degree of substitution is 0.2 to 1.5. The cloth does not contain any organic or inorganic sulfur compounds. The sponge cloth is produced by treating wood pulp with sodium hydroxide solution, then treating it with acetylating substances, drying and dissolving in an organic solvent with the addition of a pore-forming salt, fibers and optionally pigment dyes and foaming agents, spreading the mixture on a web and boiling in water with subsequent drying to form a finished cloth.

Abstract: The present invention relates to a method of making a fibrous electret material which includes the steps of (1) forming a fibrous web of nonconductive thermoplastic fibers from a blend of nonconductive thermoplastic resin and an additive which is (a) a thermally stable organic compound or oligomer containing at least one perfluorinated moiety or (b) a thermally stable organic triazine compound or oligomer containing at least one nitrogen atom in addition to those in the triazine group or (c) a combination thereof; (2) impinging jets of water or a stream of water droplets onto the web at a pressure sufficient to provide the web with filtration enhancing electret charge; and (3) drying the web.

Abstract: A sponge of decrystallized cellulose modified by an acetyl group content, where the average degree of substitution is 0.2 to 1.5. No organic or inorganic sulfur compounds are present in the sponge. The sponge is produced by treating pulp with sodium hydroxide solution, then treating it with acetylating substances, drying and dissolving in an organic solvent with the addition of a pore-forming salt, fibers and optionally pigment dyes, pressing the mixture into a perforated mold whose receiving volume corresponds to the dimensions of the sponge to be produced, then placing the mold with its contents in boiling water, and removing the sponge thus formed in the mold.

Abstract: A process is provided for the production of a porous retainer for use in a rolling bearing for holding rolling elements. The process comprises the following steps:(1) blending a polyimide resin, which serves as a porous matrix material for the porous retainer, with another heat-resistant resin which has a forming temperature range close to the polyimide resin and, when treated with a solvent in the presence of the polyimide resin, is solely dissolved out;(2) forming the resulting resin blend into a retainer of a desired shape; and(3) treating the thus-formed retainer with the solvent, whereby the another heat-resistant resin is solely dissolved out.

Abstract: A synthetic resin tube comprises an internal layer which is made of non-rigid synthetic resin and has a substantially smooth inner circumferential surface, and an external layer which is formed by winding a strip made of rigid synthetic resin around an outer circumferential surface of the internal layer overlapping winds of the strip and connecting the external layer with the internal layer, a cross section of the strip being S-shaped. When the external layer is formed, adjacent winds of the strip are connected temporarily and capable of being disconnected. After the external layer is formed, flexibility can be given to an optional length of the tube by removing the temporary connection among the winds of the strip.

Abstract: A method of drying a green particulate article includes the steps of:a. Providing a green article which includes a particulate material and a pore phase material, the pore phase material including a solvent; andb. contacting the green article with a liquid desiccant for a period of time sufficient to remove at least a portion of the solvent from the green article, the pore phase material acting as a semipermeable barrier to allow the solvent to be sorbed into the liquid desiccant, the pore phase material substantially preventing the liquid desiccant from entering the pores.

Abstract: A water solvent extraction degreasing method capable of reducing degreasing time without consideration of abrupt decomposition/vaporization and swelling caused by heat. An organic binder is removed from a molded product that is produced by a powder material mixed with the organic binder and this organic binder contains at least one water-soluble organic compound and at least one water-insoluble thermoplastic resin. The degreasing step of this method includes a water solvent extraction step for extracting the water-soluble organic compound from the organic binder contained in the molded product, using water as a solvent.

Abstract: Process for the preparation of polyether-amide solutions, steam-sterilizable dialysis membranes obtainable using the polyether-amide solutions, and a process for the production of these membranes.Polycondensation of one or more dicarboxylic acid derivatives of the formula I ##STR1## with one or more aromatic diamines of the formula II ##STR2## and, if appropriate, m-phenylenediamine, in aprotic polar solvents is known.As a result of passing ammonia, in an amount sufficient to neutralize the HCl formed, into the polymer solution obtained after the end of the polycondensation and filtering off the ammonium chloride formed, it is possible to prepare neutral, salt-free and particularly storage-stable polyether-amide solutions which can be further processed to membranes without isolation of the polymer. The resulting membranes are steam-sterilizable, chemically and thermally stable and show efficiency data in the region of that of good high-flux dialysis membranes.

Abstract: Multiphase ceramic materials for use in electronic applications such as patch antennas and multilayered ceramic devices may be fabricated by providing a novel combination of a glassy precursor material with operable amounts of a high purity cordierite material. The combined materials are sintered at appropriate temperatures, so that a non-glassy celsian type phase is formed. The materials of the instant invention, fabricated according to the method disclosed herein, demonstrate low dielectric constant (K) and low electrical loss (high Q) characteristics.

Abstract: A method and apparatus for building three-dimensional objects having an internal structure, wherein the structure is discontinuous and is composed from a plurality of patterns and bridging patterns formed on a plurality of levels, wherein a bridging level and pattern reside between previous and subsequent levels from which the bridging pattern obtains at least a portion of its pattern. A portion of the bridging pattern is obtained from the pattern on the previous level and a portion of the bridging pattern is obtained from the pattern on the subsequent level.

Abstract: A low-cost thermal decomposition degreasing method capable of drastically reducing the time required for a degreasing process which involves heating, vaporization and thermal decomposition, while assuring the shape retention property of an injection molded product during degreasing. The degreasing process comprises: (i) a first step wherein a molded product placed under a reduced pressure less than or equal to atmospheric pressure is heated at a temperature lower than the melting point of a thermoplastic binder so that the thermoplastic binder partially evaporates by 5 wt % or more, and then the molded product is further heated at a temperature lower than higher one of the melting points of a more volatile organic compound and a thermoplastic resin whereby the thermoplastic binder further evaporates by 10 wt % or more, and wherein the final temperature is set to 200.degree. C.

Abstract: A silicon nitride ceramic porous body having excellent acid and alkali resistance, mechanical strength, and durability can be employed as a filter or a catalytic carrier. The silicon nitride porous body contains a plurality of silicon nitride crystal grains with pores formed in grain boundary parts thereof, or includes a body part and a pore part wherein the body part is formed by a plurality of silicon nitride crystal grains and the pore part forms a three-dimensional network structure. The body part is formed by at least 90 vol. % of silicon nitride crystal grains, which are directly bonded to each other. In order to prepare the finished ceramic porous body, a porous body compact which is mainly composed of silicon nitride, is brought into contact with an acid and/or an alkali so that a component other than silicon nitride is partially or entirely dissolved and removed from the compact.

Abstract: An efficient method of producing a microporous polyolefin membrane having improved tensile strength and pierce strength is provided, in which a solution having dissolved therein 5% by weight to 50% by weight of a polyolefin whose weight-average molecular weight is in the range of 5.times.10.sup.5 to 2.5.times.10.sup.6 and whose weight-average molecular weight to number-average molecular weight ratio is less than 10, is extruded and rapidly cooled to obtain a gel-like product which is then stretched and has remaining solvent removed therefrom.

Abstract: The present invention relates to mat-shaped composites having porosities above 60% and densities below 0.6 g/cm.sup.3, comprising an aerogel and fibers dispersed therein, the aerogel having cracks and the aerogel fragments enclosed by the cracks, whose average volume is 0.001 mm.sup.3 to 1 cm.sup.3, being held together by the fibers. The present invention further relates to processes for producing the composites of the invention and to their use.

Abstract: A method of manufacturing disposable, single-use lipstick samplers by means of a dipping process. In a preferred form, a reservoir containing molten lipstick wax material is provided, and a spindle which is disposed above the reservoir is advanceable toward and retractable away from the reservoir. A plastic cup-shaped form having an apertured tip is applied to the spindle, which is thereafter advanced so as to submerge the tip of the form into the molten liquid wax material. The spindle and coated form are then removed from the reservoir, and gas pressure applied through the spindle to the aperture of the tip of the form, so as to blow off excess lipstick wax material therefrom. The form is allowed to cool so as to solidify the wax, and thereafter is fitted with a cover, removed, and suitably packaged.

Abstract: Plasticizer extraction from polymer membranes such as battery separators and the like, by exposure to a solvent-water combination. The water or steam is supplied to form an additional interface in a bulk solvent, and to agitate the solvent and control the temperature, as well. At the extractor exit, as well as the inlet, a water elbow is furnished in such a manner as to prevent solvent vapor contact with the atmosphere, and to keep the extractor body under some excessive pressure.

Abstract: A polymer bonded sheet product suitable for use as an electrode in a non-aqueous battery system. A porous electrode sheet is impregnated with a solid polymer electrolyte, so as to diffuse into the pores of the electrode. The composite is allowed to cool, and the electrolyte is entrapped in the porous electrode. The sheet products composed have the solid polymer electrolyte composition diffused into the active electrode material by melt-application of the solid polymer electrolyte composition into the porous electrode material sheet. The solid polymer electrolyte is maintained at a temperature that allows for rapid diffusion into the pores of the electrode. The composite electrolyte-electrode sheets are formed on current collectors and can be coated with solid polymer electrolyte prior to battery assembly. The interface between the solid polymer electrolyte composite electrodes and the solid polymer electrolyte coating has low resistance.

Abstract: A method for preparing optical quality, thin films of polymers and co-polymers, as well as blends of such polymers or co-polymers with flexible polymers and co-polymers which comprises(a) preparing a solution of the polymer or co-polymer or blend in a suitable solvent;(b) forming a film from the solution;(c) cooling the thus-formed film to a temperature below the freezing point of the solvent; and(d) dissolving the solvent out of said film at a temperature below the melting point of the solvent.This method can be employed to prepare films of high optical clarity for electro-optical device applications. Because of their thermal stability, mechanical strength and chemical resistance, films prepared according to this method can also be used as filters and separation membranes.

Abstract: A process comprising contacting PCR polyolefin chips containing volatile impurities with a heated gas at a superficial velocity sufficient to substantially reduce the volatile impurities. This process is found to cause the chips (i) to be essentially free of odors and (ii) subject to resin composition and prior use, to meet FDA regulations for direct food contact.

Abstract: The present invention relates to a high-strength porous film or sheet consisting essentially of a high-molecular-weight polyethylene resin having a viscosity-average molecular weight of not less than 300,000, wherein the said film has a thickness of 5 to 50 .mu.m, an air permeability of 200 to 1,000 sec/100 cc, a porosity of 10 to 50% and a pin puncture strength of not less than 600 gf/25 .mu.m, and a process for producing the said film.

Abstract: A method for producing biosorbents for adsorption of PCB's in which at least one proteinaceous material is contacted with a molar excess of at least one PCB congener mixture, forming a protein/PCB congener mixture. The protein/PCB congener mixture is dried after which the PCB congeners are extracted from the dried protein/PCB congener mixture forming a biosorbent in the form of an imprinted protein.

Abstract: The present invention relates to a method for eliminating surface irregulties on the wraparound window of a torpedo nose array. The method broadly comprises the steps of preheating an oven to a temperature in the range of from about room temperature to about 160.degree. F., placing the nose array with the surface irregularities in the preheated oven, applying a vacuum at a pressure of up to about 10 mm of mercury, and maintaining the object in the oven under the conditions of temperature and pressure for a time sufficient to cause polymerization at the surface of the object and removal of gas bubbles, waves and blisters from the surface of the nose array. The method further comprises introducing an anhydrous gas such as nitrogen into the oven during the vacuum applying step.

Abstract: The present invention is directed to a method of making a foamable film of at least one thermoplastic resin with at least one liquid blowing agent incorporated therein, said method comprising forming the thermoplastic resin and a liquid swelling agent for the thermoplastic resin into a layer, contacting the said layer with the liquid blowing agent and replacing at least part of the swelling agent in the resin by the liquid blowing agent.

Abstract: A method for forming parts from inorganic particulate materials is diclosed. The method utilizes a two-component binder composition which is removable at a faster rate than conventional binder compositions, thereby reducing the formation of voids and cracks that occur during binder removal. No toxic materials are required and the method does not rely on solvents. The method may be used with ceramics, metals, and cermets.

Abstract: A method for preparing a medical device having the steps: (1) treating an ionically crosslinked hydrogel to strip a substantial amount of the ionic crosslinks while retaining the hydrogel in a desired shape; and (2) ionically re-crosslinking the treated hydrogel of step (1) while retaining the hydrogel in the desired shape. In an exemplary embodiment, a ureteral stent is made by mounting a length of extruded calcium or barium alginate tubing onto a shaping jig and performing secondary shaping to form coil-shaped ends by soaking the mounted robing in a stirred potassium chloride bath, and then soaking it in a calcium chloride bath. The ends readily return after elastic deformation to their coil shapes, with the stent having a permanent memory imposed by the secondary shaping.