Abstract: A sintered magnet of Fe-B-rare earth alloy having an axis of easy magnetization oriented at an angle to a major axis can be directly produced from the alloy material by (a) press molding the material in an applied magnetic field into a compact of the dimensions determined by taking into account factors of shrinkage expected in X, Y and Z directions, and (b) sintering the compact.

Abstract: A method of producing products from a mechanically alloyed, dispersion strengthened iron-base powder comprises consolidating the powder and working the consolidated body to the desired product shape. To obtain a desired grain size in the product, the process includes at least two stages of recrystallization annealing which may be effected after consolidation or alternatively at least one of the recrystallization anneals may be carried out while the material is still in powder form.

Abstract: Sputter targets and a process for producing sputter targets are provided, comprised of carbides and/or nitrides and/or borides of refractory metals. In a first step, a dense composite body is produced comprised of one or more carbides and/or nitrides and/or borides of the metals of Groups IV A-VI A of the periodic table and a metallic binding agent comprised of one or more metals of the iron group of the periodic table. This composite body in the form of a shaped blank is machined, if necessary, and the binding agent is removed by chemical or electrochemical treatment. The sputter target as so produced has excellent mechanical strength and high thermal shock resistance. Levels of contaminating elements and the residual metallic binding agent are extremely low, meeting the requirements typically placed on sputter targets.

Abstract: Superplastically formable aluminum alloys and composite materials are prepared from rapidly solidified, coarse aluminum powder of a precipitation hardenable alloy, processed to have a low oxide and contaminant content. The powder is mixed, together with reinforcement in the case of the composite material, and then consolidated and extruded at a high extrusion ratio to promote microstructural uniformity and to break up the surface oxide present on the particles. The extrusion is then thermomechanically processed to impart a recrystallized fine-grain aluminum microstructure which is suitable for use in superplastic forming. The unreinforced powder alloy exhibits uniform elongations of over 800 percent at a strain rate of 2.times.10.sup.-4 per second, and a composite having 0.10 volume fraction silicon carbide reinforcement exhibits uniform elongations of over 450 percent at the same strain rate.

Abstract: The disclosure relates to a method whereby complex shapes, not moldable in a single molding operation, are molded in plural parts, each part being of the same or different powdered metal composition or prealloy of the type disclosed. One or more of the parts preferably has bumps or dimples thereon for joining to another of the parts in the manner to be described. The other part can also have depressions for receiving the bumps to aid in alignment of the parts prior to processing.

Abstract: When a composite nitride obtained by nitriding a fine powder of an alloy comprising metallic silicon and a metal of the group IIIa of the Periodic Table is sintered, a highly homogeneous silicon nitride sintered body having a high strength can be obtained. This fine powder of the alloy and this composite nitride exert a function of promoting sintering of Si.sub.3 N.sub.4.

Abstract: A process for producing an aluminum alloy comprises: producing an aluminum alloy powder, consisting of (A) 10 to 36 wt % of Si, 1 to 12 wt % of Fe, 2 to 10 wt % of at least one of metal selected from the group consisting of Ni, Co, Cr and Mn, reminder of the alloy powder consisting of aluminum, or consisting of (B) 10 to 36 wt % of Si, 2 to 10 wt % of Ni, 2 to 10 wt % of at least one of metal selected from the group consisting of Fe, Co, Cr, and Mn, and remainder of the alloy powder consisting of aluminum; compressing a mass of the powder by either compacting the power or accumulating the powder in a can where in case of compacting the powders are so as to have its actual density ratio of 65% to 90%, and in case of the accumulation the powders are compressed so as to have its actual density ratio of not more than 90%; heating the thus compressed mass of powder in convection type heating furnace at a temperature of 250.degree. C. to 550.degree. C.

Abstract: An electrical contact material characterized by a pressed and sintered powder of silver composite with about 5 weight percent of graphite fibers.

Abstract: There is disclosed a process for forming a wear-resistant, sintered layer on a metallic substrate. The process comprises steps of adhesively attaching to a surface of metallic substrate an alloy particle sheet containing 94 to 99 weight % of ternary eutectic alloy particles and 6 to 1 weight % of acryl binder, heating in a non-oxidating atmosphere to a temperature of 150.degree. to 380.degree. C. and holding at the temperature for at least 5 minutes, and heating a sintering temperature of the alloy particles.

Abstract: A dispersion strengthened cobalt-chromium-molybdenum alloy produced by gas atomization containing a fine oxide dispersion, and characterized, after fabrication by gas atomization, thermomechanical processing and further high temperature exposure, by excellent corrosion resistance, high fatigue strength, high ductility and high temperature stability; a process for producing said alloy and prostheses formed from said alloy.

Abstract: A process for the production of a reinforced metal plate comprising forming a slurry of metal coated carbon fibers, binder fibers and metal powder, laying down a mat from said slurry, drying the resultant mat and then sintering said, is disclosed. The dried sintered mat may be made stronger by contacting the mat with a silicate before sintering.

Abstract: Methods and apparatus are disclosed for consolidating loose or pre-compressed particulate materials, such as metal powder or metal flakes, in press equipment utilizing a reusable canister means that is sealed in vacuum from the atmosphere and heated prior to consolidation in the press equipment at elevated pressures and temperatures, thereby improving utilization of the press equipment.

Abstract: The method of consolidating a metallic, metallic and ceramic, or ceramic body in any of initially powdered, sintered, fibrous, sponge, or other form capable of compaction, includes the steps:(a) providing a bed of flowable particles within a contained zone, said particulate primarily including flowable and resiliently compressible carbonaceous particles,(b) positioning said body in said bed,(c) and effecting pressurization of said bed to cause pressure transmission via said particles to said body, thereby to compact the body into desired shaped, increasing its density,(d) said body and bed being at elevated temperatures prior to said pressurization step.

Abstract: A system for automatically consolidating a plurality of metallic or ceramic (or mixtures thereof) powder preforms is disclosed. The system comprises an assembly container wherein a consolidation container is filled with hot consolidation particles for facilitating the consolidation, and a hot preform to be consolidated thereby. The atmosphere of the assembly container is maintained hot and inert or reducing during assembly of the consolidation charge. Further disclosed are means for automatically delivering the consolidation containers, consolidation particles and preforms to the assembly container. The system includes means for conveying the consolidation containers to a press for consolidation, for separating the containers from the consolidation particles and consolidated preform after pressing, and for recycling the consolidation particles and consolidation containers.

Abstract: Powder metallurgy products of high tensile strength are formed in a pore-free state by a novel process which entirely avoids the use of canisters. An open-pore specimen is purged with depurative gas, backfilled with a reactive gas and, while still immersed in the reactive gas, compressed isostatically to an extent necessary to close the pores. The specimen may then be compressed to full density without the need for either high vacuum or a depurative or reactive gas atmosphere.

Abstract: A method of producing a cylindrical permanent magnet having a multipole surface anisotropy. The method comprises the steps of: preparing a metal mold cooperating with a lower punch in defining therein a cylindrical compacting cavity, the metal mold being provided in the inner peripheral surface thereof with field coils corresponding in number to the number of the magnetic poles of the magnet to be produced; charging the compacting cavity with a ferromagnetic powder having a magnetic anisotropy; energizing the field coils to impart a magnetic anisotropy to the ferromagnetic powder while compacting the powder between an upper punch and the lower punch to form a compact; demagnetizing the formed compact followed by a firing; and magnetizing the fired compact in the same direction as the anisotropy. The method is characterized in that the field coils produce pulse magnetic field the intensity of which is not smaller than 3.5.times.10.sup.

Abstract: A method of manufacturing a scandate dispenser cathode having a matrix at least the top layer of which at the surface consists substantially of tungsten (W) and scandium oxide (Sc.sub.2 O.sub.3) and with emitter material in or below said matrix. If said method comprises the following steps:(a) compressing a porous plug of tungsten powder(b) heating said plug in a non-reactive atmosphere and in contact with scandium to above the melting temperature of scandium,(c) cooling the plug in a hydrogen (H.sub.2) atmosphere(d) pulverizing the plug to fragments(e) heating said fragments to approximately 800.degree. C. and firing them at this temperature for a few to a few tens of minutes in a hydrogen atmosphere and slowly cooling in said hydrogen atmosphere(f) grinding the fragments to scandium hydride-tungsten powder (ScH.sub.2 /W)(g) compressing a matrix or a top layer on a matrix of pure tungsten from said ScH.sub.

Abstract: A canless method for hot working a nickel-base gas atomized alloy powder. The powder is blended with nickel powder, consolidated and sintered to a sufficient green strength. The surface of the resultant form is sealed to create an oxygen impervious layer so as to prevent oxidation therein. The sealed surface, in a sense, acts as a can. The form is then reheated and hot worked.

Abstract: An object is manufactured from a powdered material by isostatic pressing of a body, preformed from the powdered material, with a pressure medium, whereby the preformed body, in which at least the surface layer consists of a ceramic material in the form of a nitride, is surrounded by a casing which is rendered impenetrable to the pressure medium, before the isostatic pressing is carried out and the powder sintered. As the material in the casing there is used boron oxide or a glass containing boron oxide or a material forming glass while being heated, in which the content of boron oxide is sufficiently high for the glass--or the glass formed during heating--to be removable by water. The preformed body surrounded by the casing is subjected to a heat treatment for the formation of boron nitride on the surface of the preformed body, before the isostatic pressing is carried out. The casing is removed from the finished product by means of water or water vapor.

Abstract: A method for improving the handling characteristics of a flaked tantalum powder composition comprising heat treating the flaked powder component of the composition in order to pre-agglomerate the flaked component prior to mixing it with the granular tantalum powder component of the composition.

Abstract: A process for the production of agglomerated valve metal powder which comprises heating an admixture of a valve metal powder and a reducing agent in the presence of an inert gas or under high vacuum for a sufficient time and at a sufficiently elevated temperature that agglomeration of the valve metal powder occurs, and removing the reaction products of the reducing agent and the valve metal and any unreacted reducing agent from the agglomerated valve metal powder by subsequent reaction with an inorganic acid. The agglomerated powder can be sintered to prepare valve metal electrodes, e.g., anodes, which can also be prepared by direct sintering of the admixture of the metal powder and the reducing agent.

Abstract: A method of manufacturing molded articles of metal alloys, especially of nickel-base alloys, chromium-base alloys, titanium-base alloys, and dispersion-hardened alloys. A powder of the alloy, or a blend of powders of alloy constituents, is mixed with one or more plastics, selected from thermoplastics, duroplastics, and internal lubricants to form an injectionable granulate compound, the plastic content amounting to about 30% to 50% by volume. The compound is prepared by dissolving the plastic in a solvent which will not attack the base material of the alloy, and by blending it with the metal powder, after which the solvent is evaporated. The injectionable granulate compound is then injection molded to form a molded article. By heat treatment at 600.degree. C. or below in inert gas the plastic is eliminated from the molded article. The article is then sintered. To improve its strength, the article may subsequently be subjected to hot isostatic pressing.

Abstract: A porous body, for a solid electrolytic capacitor, is made from a combination of titanium and aluminum in order to reduce dependence upon tatalum, a material which is now in extremely short supply. First, the titanium hydride and aluminum are milled into an extremely fine micro-powder. Then, the powders are mixed with the aluminum content in the range of 45%-65%, compressed into the desired body shape, and given a three-step heat treatment. In the first step, the body is heated at a temperature of 400.degree. to 500.degree. C. for a dehydrogenation. In the second step, the dehydrogenated body is heated to an alloying temperature which is higher than 500.degree. C., but lower than the melting point of aluminum. In the third step, the alloyed body is heated to a temperature which is higher than the melting point of aluminum (about 1000.degree. C.).

Abstract: A particulate mass to be sintered is imbedded in a mold which comprises a porous mass of particulate refractory material enclosed within a flexible membrane. Six press units are provided for applying compressive pressures externally to the mold, together or in sequence, whereby to subject the sinterable mass to pressures in the respective directions, under the control of a preprogrammed control unit which receives clock pulses from a source and stimulates the respective press units. A flexible heating coil imbedded in the mold is supplied with alternating current from a source to inductively heat up the sinterable mass and the adjacent mold material, to enable sintering to occur. The sinterable mass may have been precompacted into a self-supporting so-called "green compact", or it may be supported in a self-supporting shell carried within and forming part of the mold. The mold preferably comprises three layers having characteristics chosen so as to assist in heating up the sinterable mass uniformly.

Abstract: A method and system whereby binder can be removed from a green body much more rapidly than in prior art systems without interfering with the integrity or aesthetics of the final part by providing a binder system having at least two components and preferably a mold release agent, the binder system having differing melting points. Each binder component can have parts with different melting temperature. When the temperature is raised to a point above the intermediate temperature at which the binder system flows, binder will proceed to exude to the surface of the green body wherefrom it can be removed.The binder is removed from the surface of the green body by blowing a non-saturated chemically inert atmosphere over the surface of the green body rapidly whereby the atmosphere at a region near the surface of the green body does not become saturated with the binder vapors.

Abstract: Cu/Al and Cu/Al/Ni memory alloys having improved mechanical properties are prepared by powder metallurgy from mixtures of pre-alloyed and/or pre-mixed powder ingredients. The mixture of powder ingredients is subjected successively to isostatic pressing, sintering in an inert atmospheric and subsequent multi-step hot working with intermediate annealing which serves to homogenize. Final annealing is carried out in the .beta.-phase solid solution temperature range and the annealed article is quenched in water.