Alloying Occurs During Sintering Patents (Class 419/46)
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Patent number: 6506338Abstract: A pressureless sintering process for producing FeAl wherein the heating rate is controlled in a manner which minimizes expansion of a mixture of elemental powders of iron and aluminum. During the process, the heating rate is maintained below 1° C./min to minimize the volume expansion during the formation of the intermediate phase Fe2Al5. As a result of the process, the final density can be increased up to 95% of the theoretical density. The sequence of phases formed during the heating of Fe+Al mixture were identified by X-ray diffraction, optical microscopy, SEM and along with DSC data were correlated to the expansion and shrinkage behavior of the samples.Type: GrantFiled: April 14, 2000Date of Patent: January 14, 2003Assignee: Chrysalis Technologies IncorporatedInventors: Shalva Gedevanishvili, Seetharama C. Deevi
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Patent number: 6475262Abstract: The method comprises preparing an iron-based powder mixture, and compressing and sintering the mixture to form the component. Said mixture comprises a first powder which forms 40 to 60 wt % of the mixture and which is an atomised pre-alloy comprising nickel, cobalt and iron, a second powder which forms 30 to 50 wt % of the mixture and essentially consists of iron, a third powder which essentially consists of ferromolybdenum, a fourth powder which essentially consists of graphite, and optionally a fifth powder which consists essentially of ferrotungsten. The component has a composition comprising 5 to 11 wt % of nickel, 5 to 11 wt % of cobalt, 5 to 8 wt % molybdenum, up to 1 wt % tungsten, 0.25 to 0.9 wt % carbon, and a balance which essentially consists of iron.Type: GrantFiled: September 23, 1999Date of Patent: November 5, 2002Assignee: Federal-Mogul Sintered Products LimitedInventors: Paritosh Maulik, Stephen Mcarthur
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Patent number: 6458317Abstract: A plating material mainly consisting of nickel-titanium is hot pressed onto a surface.Type: GrantFiled: February 12, 2001Date of Patent: October 1, 2002Assignee: Valtion Teknillinen TutkimuskeskusInventors: Jari Koskinen, Eero Haimi
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Publication number: 20020114723Abstract: Dental restorations are fabricated using metal powder. Preferably, the metal powder is a high fusing metal and preferably, the metal powder comprises a non-oxidizing metal. The metal powder is applied to a die and is covered with a covering material such as a refractory die material preferably in the form of a flowable paste. A second covering material may be sprinkled or dusted onto the paste. The model is then dried prior to firing. After drying, the model is sintered to provide a high strength metal restoration. After sintering, the outer shell can be broken off easily with one's hand to expose the sintered coping.Type: ApplicationFiled: July 24, 2001Publication date: August 22, 2002Inventors: Arun Prasad, Gregg Daskalon
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Publication number: 20020068004Abstract: The present invention relates to a method of controlling the microstructures of Cu—Cr-based contact materials for vacuum interrupters, in which a heat-resistant element is added to the Cu—Cr-based contact materials to obtain an excellent current interrupting characteristic and voltage withstanding capability, and contact materials manufactured thereby. The method of controlling the microstructures of Cu—Cr-based contact materials includes the steps of mixing a copper powder used as a matrix material, a chromium powder improving an electrical characteristic of the contact material and a heat-resistant element powder making the chromium particles in the matrix material fine to thereby obtain mixed powder, and subjecting the mixed powder to one treatment selected from sintering, infiltration and hot pressing to thereby obtain a sintered product.Type: ApplicationFiled: April 10, 2001Publication date: June 6, 2002Inventors: Jung Mann Doh, Jong Ku Park, Mi Jin Kim
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Publication number: 20020064475Abstract: A valve seat made of an Fe-based sintered alloy excellent in wear resistance and having a reduced counterpart valve attack property is disclosed, which comprises a base comprising 15-40% by weight of Cu, 0.3-12% by weight of Ni and 0.0005-3.0% by weight of C, and further comprising 0.1-10% by weight of Co and 0.1-10% by weight of Cr when necessary, with the balance being Fe and inevitable impurities, the base having a structure which comprises an Fe-based alloy phase 1 composed of Fe as a main component combined by a Cu-based alloy phase 2 composed of Cu as a main component, wherein hard particles phase 3 having MHV of 500-1700 is dispersed in the base. The Fe-based alloy phase 1 is an Fe alloy phase which comprises Ni, Cu and C with Fe having more than 50% by weight, while the Cu-based alloy phase 2 is a Cu alloy phase which comprises Ni, Fe and C with Cu having more than 50% by weight.Type: ApplicationFiled: November 15, 2001Publication date: May 30, 2002Applicant: Mitsubishi Materials CorporationInventors: Kinya Kawase, Koichiro Morimoto
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Patent number: 6348080Abstract: The present invention concerns a method of preparing a sintered product having a tensile strength 750 MPa comprising the steps of compacting a water-atomised, annealed iron-based powder comprising, by weight %, Cr 2.5-3.5, Mo 0.3-0.7, Mn 0.09-0.3, O <0.2, C<0.01 the balance being iron and, an amount of not more than 1%, inevitable impurities, at a pressure of at least 600 MPa and subjecting the compacted body to sintering at a temperature of at most 1220° C. The invention also concerns the annealed powder used in the method as well as the sintered products.Type: GrantFiled: July 18, 2000Date of Patent: February 19, 2002Assignee: Höganäs ABInventors: Johan Arvidsson, Ola Eriksson
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Publication number: 20020004141Abstract: The magnet has hard magnetic grains (K), with the hard magnetic grains (K) separated from one another in a surface layer of the magnet by a first phase (P1), while the hard magnetic grains (K) in the remaining part of the magnet are separated from one another through a nonmagnetic second phase (P2). The first phase (P1) is more corrosion resistant than the second phase (P2), so that the surface layer serves as corrosion protection. The first phase (P1) has, in addition to elements of which the second phase (P2) consists, at least one further element.Type: ApplicationFiled: May 18, 2001Publication date: January 10, 2002Inventors: Peter Schrey, Wilhelm Fernengel, Lothar Zapf
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Patent number: 6287433Abstract: An insoluble anode for sulfate electrolytes composed of, generally, from 1 to 99 wt % titanium or titanium alloy and the remainder lead or lead alloy, comprising a titanium-lead active layer, or a titanium-lead active layer covering and a core being made from titanium or lead. The anode is produced by infiltration of porous titanium with lead, either by consolidation of the mixture of titanium and lead powders. The anode formed of the active layer, or of the active layer covering and a sheet core is fabricated in the shape of a plate. The anode formed of the active layer covering and a rod or tube core is fabricated in the shape of a lattice. Advantageously, the titanium-lead active layer is dispersion-strengthened by zirconium carbide or titanium carbide particles, and it's surface is released of a portion of lead.Type: GrantFiled: May 15, 2000Date of Patent: September 11, 2001Inventor: Alla Sapozhnikova
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Patent number: 6284191Abstract: A powder metallurgical process of preparing iron aluminide useful as electrical resistance heating elements having improved room temperature ductility, electrical resistivity, cyclic fatigue resistance, high temperature oxidation resistance, low and high temperature strength, and/or resistance to high temperature sagging. The iron aluminide has an entirely ferritic microstructure which is free of austenite and can include, in weight %, 20 to 32% Al, and optional additions such as ≦1% Cr, ≧0.05% Zr or ZrO2 stringers extending perpendicular to an exposed surface of the heating element, ≦2% Ti, ≦2% Mo, ≦1% Zr, ≦1% C, ≦0.1% B, ≦30% oxide dispersoid and/or electrically insulating or electrically conductive covalent ceramic particles, ≦1% rare earth metal, ≦1% oxygen, and/or ≦3% Cu.Type: GrantFiled: September 20, 1999Date of Patent: September 4, 2001Assignee: Chrysalis Technologies IncorporatedInventors: Seetharama C. Deevi, A. Clifton Lilly, Jr., Vinod K. Sikka, Mohammed R. Hajaligol
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Patent number: 6280684Abstract: A sputtering target for fabricating a recording layer of a phase-change type optical recording medium contains a compound or mixture including as constituent elements Ag, In, Te and Sb with the respective atomic percent (atom. %) of &agr;, &bgr;, &ggr; and &dgr; thereof being in the relationship of 2≦&agr;≦30, 3≦&bgr;≦30, 10≦&ggr;≦50, 15≦&dgr;≦83 and &agr;+&bgr;+&ggr;+&dgr;=100, and a method of producing the above sputtering target is provided. A phase-change type optical recording medium includes a recording layer containing as constituent elements Ag, In, Te and Sb with the respective atomic percent of &agr;, &bgr;, &ggr; and &dgr; thereof being in the relationship of 0<&agr;≦30, 0<&bgr;≦30, 10≦&ggr;≦50, 10≦&dgr;≦80, and &agr;+&bgr;+&ggr;+&dgr;=100, and is capable of recording and erasing information by utilizing the phase changes of a recording material in the recording layer.Type: GrantFiled: January 19, 2000Date of Patent: August 28, 2001Assignee: Ricoh Company, Ltd.Inventors: Katsuyuki Yamada, Hiroko Iwasaki, Yukio Ide, Makoto Harigaya, Yoshiyuki Kageyama, Hiroshi Deguchi, Masaetsu Takahashi, Yoshitaka Hayashi
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Patent number: 6251339Abstract: The invention is directed to a method of forming parts having complex geometries made by coating ferrous based powders with a metallurgical coating, pressing the powder to make the parts, and using a low temperature heating step to diffuse the coating into the ferrous based powders.Type: GrantFiled: September 28, 1999Date of Patent: June 26, 2001Assignee: Materials Innovation, Inc.Inventors: Glenn L. Beane, David S. Lashmore, Lev Deresh
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Patent number: 6248291Abstract: A process for producing sputtering targets, which comprises molding a mixture of a powder of a high-melting substance having a melting point of 900° C. or above with a powder of a low-melting metal having a melting point of 700° C. or below at a temperature below the melting point of the low-melting metal under heat and pressure.Type: GrantFiled: December 12, 1997Date of Patent: June 19, 2001Assignee: Asahi Glass Company Ltd.Inventors: Susumu Nakagama, Masao Higeta, Atsushi Hayashi
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Patent number: 6214080Abstract: A powdered metal blend mixture for making a powdered metal part especially a valve seat insert. The mixture includes 15 to 30 wt. % of a valve steel powder, 0 to 10 wt. % nickel, 0 to 5 wt. % copper, 5 to 15 wt. % of a ferro-alloy powder, 0 to 15 wt. % of a tool steel powder, 0.5 to 5 wt. % of a solid lubricant, 0.5 to 2 wt. % graphite, 0.3 to 1.0% of a temporary lubricant, and the balance being substantially a low alloy steel powder containing 0.6 to 2.0 wt. % molybdenum, 0 to 5 wt. % nickel, and 0 to 3.0 wt. % copper. The present invention provides improved high temperature wear and corrosion resistance over prior art materials as well as improved machinability. The blend of the present invention provides a relatively high density material that allows for a single press and sinter technique.Type: GrantFiled: September 27, 1999Date of Patent: April 10, 2001Assignee: Eaton CorporationInventors: Sundaram L. Narasimhan, Heron Rodrigues, Yushu Wang
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Patent number: 6168755Abstract: Disclosed is a high nitrogen stainless steel alloy and alloy powder comprising chromium (Cr), molybdenum (Mo), manganese (Mn), nickel (Ni), nitrogen (N) and iron (Fe). The composition of the stainless steel alloy and powder comprises between about 27 and about 30% by weight Cr, between about 1.5 and about 4.0% by weight Mo, Mn present and is present in an amount up to 15% by weight, at least about 8% by weight Ni, and about 0.8 to about 0.97% by weight N with the balance being iron. It has been discovered that forming an alloy of this chemistry using nitrogen gas atomization process, followed by a consolidation process, the alloy is less likely to form detrimental ferrite, stable nitride and sigma (&sgr;) phases, without the need for further processing, such as solution treating and quenching. This allows for the formation of stainless steel articles having a thicker cross-section with reduced processing cost.Type: GrantFiled: May 27, 1999Date of Patent: January 2, 2001Assignee: The United States of America as represented by the Secretary of CommerceInventors: Francis S. Biancaniello, Stephen D. Ridder, Rodney D. Jiggetts
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Patent number: 6045601Abstract: A high density, non-magnetic alloy is described along with a process for manufacturing it. The preferred composition for the alloy is approximately 95% by weight of tungsten and 5% of austenitic stainless steel. The process for manufacturing the alloy begins with blending tungsten and stainless steel powders which are then mixed with an organic binder to form a feedstock. The latter is then molded into the form of compacted items, such as a hard drive counterweight balance, and then sintered in either vacuum or a hydrogen atmosphere. The tungsten heavy alloys of the present invention can be easily manufactured in large volume economically in many intricate shapes with excellent control of weight and dimensions.Type: GrantFiled: September 9, 1999Date of Patent: April 4, 2000Assignee: Advanced Materials Technologies, Pte, Ltd.Inventor: Lye King Tan
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Patent number: 5980812Abstract: Solid objects are formed in an imagewise layering process in which components of a dispersion are homogenized to form an alloy. Imagewise exposure of the layers to radiation to form an alloy permits separation of the exposed, homogenized regions from non-exposed, non-homogenized regions. As each layer is formed and imagewise homogenized, contiguous layer regions are bonded together to form a homogenized, three-dimensional object which may be separated from surrounding dispersion.Type: GrantFiled: April 30, 1997Date of Patent: November 9, 1999Inventor: John A. Lawton
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Patent number: 5963771Abstract: In the present invention, nickel and phosphorous are simultaneously plated onto the surface of iron powder, mixed iron and nickel powder, or iron-nickel pre-alloyed powder, to form iron-nickel-phosphorous ternary alloy powders with very uniform distribution of phosphorous, with concentrations ranging between 2.0 and 6.0 wt%. When mixed with an appropriate amount of organic binder, these powders may be used as raw materials for injection molding. Intricate parts thus formed can be sintered at relatively low temperatures to attain high sintered density, large grain size, and isotropic shrinkage. The sintered microstructure thus obtained is characterized by spheroidal grains embedded in continuous intergranular insulating phosphide phase. The magnetic properties of the resulting material are substantially improved as compared to those of powder processed products.Type: GrantFiled: September 29, 1997Date of Patent: October 5, 1999Inventors: Tien-Yin Chan, Shun-Tian Lin
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Patent number: 5930583Abstract: This invention relates to a method for forming a titanium alloy by powder metallurgy, which comprises the processes of mixing uniformly a powder of titanium or an alloy thereof with a low-melting point metal or alloy powder, injecting the mixture into a press forming die, then press forming them under heating to a temperature near and over the melting point of the low-melting point metal, or to a temperature between the liquidus and the solidus of the low-melting point alloy, or to a temperature near and over the liquidus to obtain the targeted compact, and holding this compact in the pressurized state to cause the molten low-melting point metal or alloy to infiltrate the powder grain boundary of the titanium or alloy thereof, and then sintering the compact thus obtained in an inert atmosphere or a vacuum to diffuse the titanium or alloy thereof and the low-melting point metal or alloy into each other and to make alloys of them.Type: GrantFiled: August 25, 1997Date of Patent: July 27, 1999Assignee: Japan as represented by Director General of Agency of Industrial Science and TechnologyInventors: Kazuo Yasue, Gongli Yu
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Patent number: 5926686Abstract: The present invention concerns low allow PM materials which after single pressing and sintering utilizing traditional powder metallurgy processes and equipment combine high mechanical strength and high density with maintained precision of tolerance. As base material is used an iron powder having at least one alloying element diffusion-bonded to the outer surfaces of unalloyed iron particle is provided.Type: GrantFiled: November 13, 1997Date of Patent: July 20, 1999Assignee: Hoganas ABInventors: Ulf Engstrom, Bjorn Johansson
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Patent number: 5918104Abstract: Powder metallurgy production of Ta10W alloy affording properties comparable to melt derived Ta10W, but at higher yields and lower costs, is enabled by blending component powders of minus 325 mesh and sintering at 2,400.degree. C. in three sinter steps and utilizing a slow ramp up in the first sinter step and cold isostatic pressing prior to the first sinter step and isostatic press densification in conjunction with at least the first sinter step.Type: GrantFiled: December 24, 1997Date of Patent: June 29, 1999Assignee: H.C. Starck, Inc.Inventors: Robert W. Balliett, Trung Luong
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Patent number: 5876481Abstract: A steel powder consisting of a combination of purified steel and prealloyed manganese, chromium, molybdenum and nickel. The steel powder is used in the production of metal parts using powder metallurgy. The addition of the prealloyed elements results in a metal part having greater strength and hardness with a low oxygen content and good compressibility.Type: GrantFiled: June 14, 1996Date of Patent: March 2, 1999Assignee: Quebec Metal Powders LimitedInventors: Fran.cedilla.ois Chagnon, Yves Trudel
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Patent number: 5872322Abstract: A method of making a structural iron-based article comprising: (a) blending a compressible base iron powder (max. particle size of 100 microns) a graphite powder to provide carbon in mixture, and a single master alloy powder (average particle size of 10 microns) meltable within the range of 900.degree.-1200.degree. C. (1690.degree.-2220 .degree.F.) to form a mixture, the master alloy powder being present in an amount of 1-5% by weight of the mixture and consisting of (i) hardenability enhancing alloying ingredients selected from Mn, Mo, Ni, Cr, Cu and Fe, with Fe being present only if Cr or Mo is selected and (ii) wetting agents selected from the group of B, Y, Si and rare earth misch metal, the master alloy being devoid of carbon and being proportioned to provide a desired amount of hardenability in the base powder; (b) compacting the mixture to a green density 7.1-7.4 g/cm.sup.Type: GrantFiled: February 3, 1997Date of Patent: February 16, 1999Assignee: Ford Global Technologies, Inc.Inventors: Stanislaw Mocarski, Charles Oliver Mchugh, Russell A. Chernenkoff, David Alan Yeager
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Patent number: 5848349Abstract: The present invention relates to modifying the properties of a metal matrix composite body by a post formation process treatment and/or a substantially contiguous modification treatment. The post formation process treatment may be applicable to a variety of metal matrix composite bodies produced by various techniques, and is particularly applicable to modifying the properties of a metal matrix composite body produced by a spontaneous infiltration technique. The substantially contiguous modification process may also be used primarily in conjunction with metal matrix composite bodies produced according to a spontaneous infiltration technique. Particularly, at least a portion of the matrix metal of the metal matrix composite body and/or the filler material of the metal matrix composite body is modified or altered during and/or after the formation process.Type: GrantFiled: February 3, 1995Date of Patent: December 8, 1998Assignee: Lanxide Technology Company, LPInventors: Marc Stevens Newkirk, Andrew Willard Urquhart, Michael Kevork Aghajanian, Mark Gordon Mortenson, Vilupanur Alwar Ravi, Alan Scott Nagelberg
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Patent number: 5822674Abstract: A material for electric contacts based on silver-tin oxide is obtained by mixing a powder of silver or an alloy mainly containing silver with a powder consisting mainly of tin oxide and 0.01 to 10 wt. % (in relation to the quantity of tin oxide) of an additive consisting of one or more compounds containing silver, oxygen and a metal from sub-groups II to VI of the periodic system and/or antimony, bismuth, germanium, indium and gallium, compacting the mixture and sintering it. The tin oxide may be replaced by zinc oxide.Type: GrantFiled: May 18, 1995Date of Patent: October 13, 1998Assignee: Doduco GmbH + Co. Dr. Eugen DurrwachterInventors: Volker Behrens, Thomas Honig
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Patent number: 5802437Abstract: Metallic shaped bodies are produced from an injection-molding composition comprising at least one carbonyl metal powder and at least one element powder of metals from the group Cr, Mn, V, Si, Ti or of other metals which are at least as oxidation-sensitive by shaping, removing the binder and sintering. In place of an element powder, it is also possible to use an alloy powder comprising the corresponding metals.Type: GrantFiled: September 28, 1995Date of Patent: September 1, 1998Assignee: BASF AktiengesellschaftInventors: Hans Wohlfromm, Dieter Weinand, Martin Blomacher, Manfred Schwarz, Eva-Maria Langer
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Patent number: 5744734Abstract: A method for fabricating articles of high-temperature aluminum alloys having a compressional strength of at least 20 kg/mm.sup.2 at temperatures of 300.degree. C. or greater, is disclosed. The method comprises the steps of: (a) forming a porous preform from particles of a first aluminum alloy via cold-pressing, the preform having the shape and dimension of the aluminum alloy article to be fabricated; (b) squeeze-casting a molten second aluminum alloy into void spaces of the porous preform to form an aluminum composite containing the first aluminum alloy, which serves as a reinforcement phase, dispersed in the second aluminum alloy, which serves as a matrix phase; (c) wherein the molten second aluminum alloy is cast at such temperatures so as to cause a surface of the first aluminum alloy particles to melt and thereby form a strong bonding with the second aluminum alloy.Type: GrantFiled: October 31, 1995Date of Patent: April 28, 1998Assignee: Industrial Technology Research InstituteInventors: Chih-Chao Yang, Edward Chang
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Patent number: 5734959Abstract: The invention is directed to a method of forming an implant having a porous surface using an organic binder compound to enhance the bonding between the porous surface layer and implant. Preferably, the binder is formed from a water-soluble protein that carbonizes during the sintering process to alloy with the metal of the porous surface layer. The porous surface layer may be in the form of beads or of fiber metal and can be preformed to fit with an implant or formed over the surface of the implant.Type: GrantFiled: October 12, 1995Date of Patent: March 31, 1998Assignee: Zimmer, Inc.Inventors: Steve Krebs, Clarence Panchison, H. Ravindranath Shetty
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Patent number: 5733427Abstract: A sputtering target formed of a refractory metallic silicide having a composition MSi.sub.x including a mixture composition of an MSi.sub.2 phase in the form of particles (M: at least one refractory metal selected from a group consisting of W, Mo, Ti, Zr, Hf, Ni and Ta), and an Si phase provided as a matrix phase. Interface layers having a predetermined thickness are formed at the interfaces between the MSi.sub.2 phase and the Si phase. The value X in the composition formula MSi.sub.x is set to a range of 2.0 to 4.0, and the thickness of the interface layers formed between the MSi.sub.2 phase and the Si phase, the dispersion of the composition, the density ratio of the target, the electrical resistivity of the Si phase and the surface roughness are set to predetermined values. An uniform high-quality thin film in which a composition distribution is uniform can be manufactured stably by using this target.Type: GrantFiled: March 30, 1995Date of Patent: March 31, 1998Assignee: Kabushiki Kaisha ToshibaInventors: Michio Satou, Takashi Yamanobe, Mitsuo Kawai, Tatsuzo Kawaguchi, Kazuhiko Mitsuhashi, Toshiaki Mizutani
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Patent number: 5703304Abstract: The invention concerns an iron-based powder for powder-metallurgically producing components by powder compacting and sintering. The powder which essentially consists of 0.7-2.0% of Mo, 0.2-2.5% by weight of Cr and 0-3.0% by weight of Cu, 0.05-0.25% by weight of Mn and 0.3-1.0% by weight of C, wherein Fe, Mo and Mn are present as a prealloyed, water atomised FeMoMn base powder, Cr is present as FeCr, Cu is present as a metal or partially prealloyed powder and C is present as a graphite, exhibits very interesting properties. The invention also includes a method for preparing sintered components from this iron powder.Type: GrantFiled: February 6, 1997Date of Patent: December 30, 1997Assignee: Hoganas ABInventors: Caroline Lindberg, Per Engdahl
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Patent number: 5701575Abstract: An article essentially consisting of one or more of Ti--Al intermetallic compounds is fabricated so as to have a volume ratio of voids no more than 3.5%, by preparing a mixture of materials selected from a group consisting of Ti, Ti alloys, Al, Al alloys, and Ti--Al compounds, having a composition suitable for forming a desired Ti--Al intermetallic compound, and heating said mixture so that said mixture may be sintered. Typically, the temperature and pressure for the heating or sintering process is appropriately selected so that the desired porosity may be obtained. The mechanical strength of an article according to the present invention is not only improved but is highly predictable, or, in other word, highly reliable. The fabrication costs can be reduced because the fabrication process involves only relatively low temperatures when pressing and heating the work at the same time.Type: GrantFiled: January 11, 1996Date of Patent: December 23, 1997Assignee: NHK Spring Co., Ltd.Inventors: Kohei Taguchi, Michihiko Ayada, Hideo Shingu
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Patent number: 5682590Abstract: A titanium-based carbonitride grade for finishing and semi-finishing turning operations with excellent properties is obtained starting from a titanium-based carbonitride grade used for milling operations. The carbon content of a conventional titanium-based carbonitride grade used for milling operations is optimized in such a way that it is close to the point where .eta.-phase or other substoichiometric phases are formed. The improved titanium-based carbonitride is also provided with a thin wear resistant Ti-containing coating deposited preferably by PVD technique.Type: GrantFiled: January 23, 1996Date of Patent: October 28, 1997Assignee: Sandvik ABInventor: Gerold Weinl
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Patent number: 5682588Abstract: The present invention relates to a method for producing, without quench-hardening process, a ferrous sintered alloy having satisfactory strength which is equal to that of the conventional ferrous sintered quenched material, and the method comprises the steps of: preparing a powder mixture by adding, in weight ratios, 1 to 2% of copper powder, 1 to 3% of Ni powder, and graphite to a ferrous alloy powder consisting of 3 to 5% of Ni, 0.4 to 0.7% of Mo, and the remainder Fe, the quantity of said graphite being determined such that the C-content after sintering is 0.2 to 0.7%; compacting said powder mixture in a tool to form a green compact; sintering said green compact in a non-oxidizing atmosphere at a temperature in the range of 1130.degree. to 1230.degree. C.; and cooling the sintered product in the sintering furnace at a rate of 5.degree. C./min. to 20.degree. C./min.Type: GrantFiled: September 23, 1996Date of Patent: October 28, 1997Assignees: Hitachi Powdered Metals Co., Ltd., Hitachi Koki Co., Ltd.Inventors: Tadayuki Tsutsui, Kei Ishii, Hideo Shikata, Sumihisa Kotani
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Patent number: 5659876Abstract: A method for producing a washer having a boss comprises the following steps in the sequence set forth: (a) sprinkling powder of a bearing alloy onto a backing metal made of an iron-based alloy to form a composite material; (b) sintering the composite material to obtain a bimetal material so as to accomplish a primary sintering; (c) fabricating the bimetal material into a shape of the washer having the boss; and (d) simultaneously accomplishing a secondary sintering and carburizing of the washer having the boss. By virtue of simultaneously conducting the secondary sintering and the carburizing for the washer, the number of steps in producing method (particularly, during a heat treatment) is reduced thereby improving the productivity of the washer having the boss while reducing thermal energy required for the heat treatment.Type: GrantFiled: October 19, 1995Date of Patent: August 19, 1997Assignee: Jatco CorporationInventor: Muneo Mizuta
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Patent number: 5628044Abstract: High purity iron-zinc intermetallic calibration standards are produced using a slow diffusion technique. The alloys are pure to greater than 99.5 wt % and are homogenous to greater than 98%. The alloys can be used to calibrate instrumentation used to monitor and measure galvanneal and galvanized coatings. The alloy calibration standards for each of the iron-zinc phases allows instrumentation correction factors to be determined for iron-zinc coating analysis.Type: GrantFiled: June 2, 1995Date of Patent: May 6, 1997Assignee: Old Dominion UniversityInventors: Desmond C. Cook, Richard G. Grant, Patricia S. Cook
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Patent number: 5613184Abstract: An aluminium alloy made by a powder metallurgy route and a method for its production are described. The method comprises the steps of producing a first powder of a near-eutectic aluminium-silicon based alloy; producing a second powder of a hypereutectic aluminium-silicon based alloy; mixing desired proportions of the two powders together; compacting the powder mixture and sintering the compacted powder.Type: GrantFiled: November 30, 1995Date of Patent: March 18, 1997Assignees: The Aluminium Powder Company Limited, Brico Engineering LimitedInventors: Charles G. Purnell, Paul Smith, Mohammad S. Mahmoud
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Patent number: 5594930Abstract: A brazeable aluminum material is composed of an aluminum core and a brazing agent layer consisting of a brazing agent thermally sprayed onto covering a surface of the core. A number of unmolten minute particles of the brazing agent are present in the brazing agent layer, which contains at least an aluminum-silicon alloy and/or a mixture of aluminum and silicon. Characteristic features of a method of producing the brazeable aluminum material are the steps of: preparing a powder composed of minute particles; and thermally spraying the powder onto the aluminum core in such a state that only a surface of each minute particle is molten, with a pith of the particle remaining unmolten. The powder is an Al-Si alloy and/or a mixture of Al powder and Si powder.Type: GrantFiled: October 27, 1993Date of Patent: January 14, 1997Assignee: Showa Aluminum CorporationInventors: Takashi Terada, Masahiro Kojima, Taizo Morita, Katsuyuki Arakawa, Ichiro Iwai, Masakazu Furuta
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Patent number: 5590383Abstract: A porous membrane produced by preparing a slurry made from at least one micropyretic substance and at least one liquid carrier. The slurry is dried into a green form having a desired geometric configuration. Combustion of the green form produces the porous membrane.Type: GrantFiled: August 29, 1994Date of Patent: December 31, 1996Assignee: Micropyretics Heaters International, Inc.Inventors: Jainagesh A. Sekhar, James J. Liu, Naiping Zhu
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Patent number: 5579533Abstract: A soldering tip comprising 50-95 weight percent uncoated copper particles and 5-50 weight percent iron particles is prepared by a method in which the particles are compacted, sintered and shaped into a soldering tip. The soldering tips are durable, resistant to pitting by molten solder, and thermally conductive.Type: GrantFiled: August 17, 1995Date of Patent: November 26, 1996Assignees: Donald Fegley, Emily I. WellerInventor: Carl E. Weller
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Patent number: 5568653Abstract: According to the invention there now is provided a method of producing a sintered titanium based carbonitride alloy with 3-25 weight-% binder phase with extremely good properties at semifinishing operations at turning. The method relates to the use of a raw material consisting of a complex cubic carbonitride comprising the main part of the metals from groups IV and V of the periodic system and carbon and nitrogen to be found in the finished alloy whereby said alloy has the composition0.85.ltoreq.X.sub.IV .ltoreq.0.990.58.ltoreq.X.sub.C .ltoreq.0.69where X.sub.IV is the molar ratio of the group IV elements of the alloy and X.sub.C is the molar ratio of carbon.Type: GrantFiled: May 11, 1995Date of Patent: October 22, 1996Assignee: Sandvik ABInventors: Gerold Weinl, Rolf Oskarsson
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Patent number: 5561831Abstract: According to the invention there now is provided a method of producing a sintered titanium based carbonitride alloy with 3-25 weight-% binder phase with extremely good properties at fine to medium coarse milling. The method relates to the use of a raw material consisting of a complex cubic carbonitride comprising the main part of the metals from groups IV and V of the periodic system and carbon and nitrogen to be found in the finished alloy whereby said alloy has the composition0.89.ltoreq.X.sub.IV .ltoreq.0.970.52.ltoreq.X.sub.C .ltoreq.0.61where X.sub.IV is the molar ratio of the group IV elements of the alloy and X.sub.C is the molar ratio of carbon.Type: GrantFiled: May 11, 1995Date of Patent: October 1, 1996Assignee: Sandvik ABInventors: Ake Ostlund, Rolf Oskarsson
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Patent number: 5554338Abstract: The invention relates to a method of preparing a composite sintered body having inner and outer portions fitted with each other. The method includes the steps of: (a) preparing an inner powder compact; (b) preparing an outer powder compact; (c) fitting the inner and outer powder compacts with each other so as to prepare a composite powder compact; and (d) sintering the composite powder compact so as to prepare the composite sintered body. The inner and outer powder compacts are respectively selected such that, during the step (d), the amount of growth of the inner powder compact becomes greater than that of the outer powder compact. Each of the inner and outer composite powder compacts is made of one member selected from the group consisting of a wax-type segregation prevention powder mixture and a metal-soap-type segregation prevention powder mixture. At least one of the inner and outer composite powder compacts is made of the wax-type segregation prevention powder.Type: GrantFiled: April 18, 1995Date of Patent: September 10, 1996Assignees: Nissan Motor Co., Ltd., Hitachi Powdered Metals Co., Ltd.Inventors: Hiroshi Sugihara, Hiroyuki Ishikawa, Tsutomu Uemura, Akira Fujiki, Hiromasa Imazato, Shinichi Umino
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Patent number: 5529745Abstract: By compacting in a magnetic field a mixture containing powder raw material A having a composition represented by (Tb.sub.x Dy.sub.1-x)T.sub.y wherein T is at least one metal of Fe, Co, and Ni and 0.30<x.ltoreq.x 0.50 and 1.70.ltoreq.y.ltoreq.2.00, powder raw material B having a composition represented by (Dy.sub.1-t Tb.sub.t).sub.z T.sub.1-z wherein 0.ltoreq.t.ltoreq.0.30 and 0.40.ltoreq.z.ltoreq.0.80 and optionally, powder raw material C consisting essentially of element T, and sintering the compact, there is prepared a magnetostrictive material having a composition represented by (Tb.sub.v Dy.sub.1-v)T.sub.w wherein 0.27.ltoreq.v<0.50 and 1.70.ltoreq.w.ltoreq.2.00, with grains oriented along [111] axis. The material having minimal crystalline magnetic anisotropy at room temperature and large magnetostrains is obtained at low cost by powder metallurgy.Type: GrantFiled: April 18, 1995Date of Patent: June 25, 1996Assignee: TDK CorporationInventors: Teruo Mori, Tomoko Nakamura
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Patent number: 5484490Abstract: A P-type thermoelectric material consists essentially of iron disilicide, metallic manganese and metallic aluminium dissolved in or alloyed with the iron disilicide, and silicon oxide and/or aluminum oxide present in the iron disilicide. The manganese is contained in an amount of from 1.67 to 4.1 atomic % with respect to a sum of atoms of iron and silicon constituting the iron disilicide, the metallic manganese and the metallic aluminum taken as 100 atomic %, and the metallic aluminum contained in an amount of from 1.33 to 3.33 atomic % with respect thereto, and a sum of the metallic manganese and the metallic aluminum in an amount of from 4.0 to 5.34 atomic % with respect thereto. The P-type thermoelectric material having such a composition produces a thermoelectromotive force equal to or greater than those of the conventional P-type thermoelectric materials comprised of iron disilicide, and it exhibits a mean resistivity equal to or smaller than that of the N-type thermoelectric material.Type: GrantFiled: February 23, 1994Date of Patent: January 16, 1996Assignees: Technova Inc., National Research Institute for MetalsInventors: Shigeki Tokita, Makoto Okabayashi, Takashi Amano, Isao Nishida
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Patent number: 5466277Abstract: A sintered Al-alloy, which has a composition of 0.2 to 2.0% of Mg, 10.0 to 35.0% of Si, from 0.2 to 4.0% of Cu, and Al and unavoidable impurities in balance, is produced by using a mixture of the main powder (10.0-35.0% of Si, 0.2-2.0% of Cu, and Al and unavoidable impurities in balance) and at least one metal or mother-alloy powder selected from (a)-(i): (a) Mg powder; (b) Al--Mg powder; (c) Al--Cu powder; (d) Al--Mg--Si powder; (e) Al--Cu--Si powder; (f) Al--Mg--Cu powder; (g) Al--Mg--Cu--Si powder; (h) Mg--Cu powder; and, (i) Mg--Cu--Si powder.Type: GrantFiled: March 30, 1994Date of Patent: November 14, 1995Assignee: Showa Denko K.K.Inventors: Shin Miura, Youichi Hirose, Mitsuaki Sato
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Patent number: 5453243Abstract: A process for producing titanium aluminide weld rod comprising: attaching one end of a metal tube to a vacuum line; placing a means between said vacuum line and a junction of the metal tube to prevent powder from entering the vacuum line; inducing a vacuum within the tube; placing a mixture of titanium and aluminum powder in the tube and employing means to impact the powder in the tube to a filled tube; heating the tube in the vacuum at a temperature sufficient to initiate a high-temperature synthesis (SHS) reaction between the titanium and aluminum; and lowering the temperature to ambient temperature to obtain a intermetallic titanium aluminide alloy weld rod.Type: GrantFiled: August 17, 1994Date of Patent: September 26, 1995Assignee: The United States of America as represented by the Secretary of the InteriorInventors: Jeffrey S. Hansen, Paul C. Turner, Edward R. Argetsinger
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Patent number: 5433917Abstract: Process for producing novel fluxed PZT dielectric ceramic compositions having sintering temperatures below about 1000.degree., so as to be non-reactive with electrode layers when co-fired therewith. The PZT is sintered with an effective amount of an eutectic mixture of CuO and an oxide of an alkaline earth metal, preferably barium oxide and/or strontium oxide, to reduce the sintering temperature of the PZT composition below about 1000.degree. C. Dopant such as manganese oxide may be added to reduce the dielectric losses.Type: GrantFiled: September 16, 1993Date of Patent: July 18, 1995Assignee: The Penn State Research FoundationInventors: Ashvin Srivastava, Amar Bhalla, L. Eric Cross
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Patent number: 5429793Abstract: A process for producing metal oxide dispersion-strengthened anodes for use in fuel cells in which a metal alloy powder comprising at least one metal powder and at least one metal oxide forming phase is formed into a "green" cohesive structure. The "green" cohesive structure is heated in a sintering furnace resulting in simultaneous sintering and internal oxidizing of the oxide forming phase within the "green" cohesive structure, forming an oxide dispersion-strengthened structure. To promote simultaneous sintering of the "green" cohesive structure and internal oxidation of the oxide forming phase within the "green" cohesive structure, an oxidizing agent is disposed within the "green" cohesive structure or is applied to the exterior of the cohesive structure.Type: GrantFiled: May 17, 1994Date of Patent: July 4, 1995Assignee: Institute of Gas TechnologyInventors: Estela T. Ong, Nellie Burton-Gorman
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Patent number: 5427734Abstract: The object of the invention is to provide a manufacturing method of a complex shaped R--Fe--B type sintered anisotropic magnet improved the moldability of injection molding and preventing the reaction between R ingredients and binder and controlled the degradation of magnetic characteristics due to residual carbon and oxygen. Utilizing the R--Fe--B type alloy powder or the resin coated said alloy powder, and methylcellulose and/or agar and water, instead of the usual thermoplastic binder, it is mixed and injection molded. The molded body is dehydrated by the freeze vacuum dry method to control the reaction between R ingredients and of the R--Fe--B alloy powder and water; furthermore, by administering the de-binder treatment in the hydrogen atmosphere, and sintering it after the dehydrogen treatment, residual oxygen and carbon in the R--Fe--B sintered body is drastically reduced, improving the moldability during the injection molding to obtain a three dimensionally complex shape sintered magnet.Type: GrantFiled: June 24, 1993Date of Patent: June 27, 1995Assignee: Sumitomo Special Metals Co., Ltd.Inventors: Osamu Yamashita, Masahiro Asano, Tsunekazu Saigo
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Patent number: RE37875Abstract: Solid objects are formed in an imagewise layering process in which components of a dispersion are homogenized to form an alloy. Imagewise exposure of the layers to radiation to form an alloy permits separation of the exposed, homogenized regions from non-exposed, non-homogenized regions. As each layer is formed and imagewise homogenized, contiguous layer regions are bonded together to form a homogenized, three-dimensional object which may be separated from surrounding dispersion.Type: GrantFiled: November 13, 2000Date of Patent: October 15, 2002Inventor: John A. Lawton