Heat And Pressure Simultaneously To Effect Sintering Patents (Class 419/48)
  • Publication number: 20090071822
    Abstract: There are provided a sputtering target material for a soft-magnetic film layer with a high saturation magnetic flux density and high amorphous properties and a method for producing the sputtering target material. The target material is made of an alloy comprising one or more of Zr, Hf, Nb, Ta and B in an amount satisfying 5 at %?(Zr+Hf+Nb+Ta)+B/2?10 at % and having 7 at % or less of B; 0 to 5 at % in total of Al and Cr; and the balance being Co and Fe in an amount satisfying 0.20?Fe/(Fe+Co)?0.65 (at % ratio) with unavoidable impurities.
    Type: Application
    Filed: September 17, 2008
    Publication date: March 19, 2009
    Applicant: SANYO SPECIAL STEEL CO., LTD.
    Inventors: Toshiyuki Sawada, Akihiko Yanagitani
  • Patent number: 7501081
    Abstract: A nanostructured monolithic titanium boride (TiB) material and methods of forming such a material are disclosed and described. This material has a room-temperature four-point flexural strength about three times that of commercially available titanium diboride (TiB2). The achievement of nanostructured internal microstructural arrangement having a network of interconnected titanium monoboride whiskers affords a very high strength to this material above some of the best ceramic materials available in the market. The material contains a small amount of titanium and a densifier, but it is largely made of TiB phase with substantially no TiB2. The nanostructured monolithic titanium boride material can be formed by high temperature processing of a powder precursor having carefully selected weight and size distributions of titanium powder, titanium diboride powder, and densifier powder.
    Type: Grant
    Filed: January 25, 2007
    Date of Patent: March 10, 2009
    Assignee: University of Utah Research Foundation
    Inventor: K. S. Ravi Chandran
  • Publication number: 20090022616
    Abstract: Disclosed in this specification is a process for refurbishing a spent sputtering target. The process includes the step of applying sufficient heat and axial force to the filled sputtering target to hot press the filled sputtering target such that the powdered metal fuses with the un-sputtered metal, producing a refurbished target. The process may be used to refurbish precious metal targets, such as ruthenium targets.
    Type: Application
    Filed: July 15, 2008
    Publication date: January 22, 2009
    Inventors: Robert Acker, Adrish Ganguly, Matthew T. Willson
  • Patent number: 7467937
    Abstract: In one aspect of the present invention, a high-temperature, high-pressure press apparatus has a cartridge assembly adapted for connection to a unitary frame. An anvil is attached at a front end of a cylindrical body of the cartridge and a hydraulic chamber within the body is adapted to apply axial pressure to the anvil. A threaded end of the anvil is adapted for mating with a threaded inside diameter of a borehole disposed within a wall of the frame. A radial compression element disposed around an outer diameter of the body is adapted to limit radial expansion of the body proximate the hydraulic chamber. At least one mechanism is attached to the radial compression element; the at least one mechanism being adapted to preload the threaded connection between the cartridge assembly and the frame.
    Type: Grant
    Filed: November 29, 2007
    Date of Patent: December 23, 2008
    Inventors: David R. Hall, Ronald Crockett, Timothy C. Duke, Scott Dahlgren
  • Patent number: 7467936
    Abstract: A cartridge assembly for connection to a frame of a high temperature, high pressure press, having an anvil at a front end of a cylindrical body of the cartridge and a hydraulic chamber within the body adapted to apply axial pressure to the anvil. A radial compression element is disposed around an outer diameter of the body and is adapted to limit radial expansion of the body proximate the hydraulic chamber.
    Type: Grant
    Filed: March 27, 2007
    Date of Patent: December 23, 2008
    Inventors: David R. Hall, Ronald Crockett, Scott Dahigren, Timothy C. Duke
  • Patent number: 7459105
    Abstract: A nanostructured monolithic titanium boride (TiB) material and methods of forming such a material are disclosed and described. This material has a room-temperature four-point flexural strength about three times that of commercially available titanium diboride (TiB2). The achievement of nanostructured internal microstructural arrangement having a network of interconnected titanium monoboride whiskers affords a very high strength to this material above some of the best ceramic materials available in the market. The material contains a small amount of titanium, but it is largely made of TiB phase with substantially no TiB2. The nanostructured monolithic titanium boride material can be formed by high temperature processing of a powder precursor having carefully selected weight and size distributions of titanium and titanium diboride powders. Potential applications of this material can include wear resistant components such as die inserts for extrusion dies, nozzles, armor, electrodes for metal refining etc.
    Type: Grant
    Filed: July 7, 2005
    Date of Patent: December 2, 2008
    Assignee: University of Utah Research Foundation
    Inventor: K. S. Ravi Chandran
  • Patent number: 7410610
    Abstract: An article made of constituent elements is prepared by furnishing at least one nonmetallic precursor compound, wherein all of the nonmetallic precursor compounds collectively contain the constituent elements. The constituent elements include a titanium-base metallic composition, boron present at a level greater than its room-temperature solid solubility limit, and, optionally, a stable-oxide-forming additive element present at a level greater than its room-temperature solid solubility limit. The precursor compounds are chemically reduced to produce a material comprising a titanium-base metallic composition having titanium boride particles therein, without melting the titanium-base metallic composition. The titanium-base metallic composition having the titanium boride particles therein is consolidated without melting.
    Type: Grant
    Filed: November 12, 2004
    Date of Patent: August 12, 2008
    Assignee: General Electric Company
    Inventors: Andrew Philip Woodfield, Eric Allen Ott, Clifford Earl Shamblen, Michael Francis Xavier Gigliotti, David Alan Utah, Alan Glen Turner
  • Patent number: 7407622
    Abstract: A method of manufacturing a fan blade (26) for a gas turbine engine by powder metallurgy comprises the steps of forming a container (52) and placing at least one metal insert (52) at a predetermined position within the container (52) and filling the container (52) with metal powder (60). The at least one metal insert (62) has a predetermined pattern of stop off material (68,70) on at least one surface of the metal insert (64,66). The container (52) is evacuated and then sealed. The container (52) is hot pressed to consolidate the metal powder (60) into a consolidated metal powder preform (72). The container (52) is removed from the consolidated metal powder preform (72). The consolidated metal powder preform (72) is heated and a fluid is supplied to the predetermined pattern of stop off material (68,70) to hot form at least a portion of the consolidated metal powder preform (72) to form the hollow metal fan blade (26).
    Type: Grant
    Filed: November 15, 2005
    Date of Patent: August 5, 2008
    Assignee: Rolls-Royce plc
    Inventors: Wayne E Voice, Junfa Mei
  • Patent number: 7387763
    Abstract: A sheet is prepared by mixing a mass of metallic powders with a temporary thermoplastic binder to form an injection-moldable mixture, thereafter injection molding the injection-moldable mixture to form a sheet precursor. The sheet precursor is consolidated to a relative density of substantially 100 percent to form the sheet, and thereafter heat treated. The final sheet is preferably a nickel-base superalloy having more than about 30 volume percent of gamma prime phase, or an intermetallic such as a titanium aluminide.
    Type: Grant
    Filed: August 19, 2005
    Date of Patent: June 17, 2008
    Assignee: General Electric Company
    Inventor: Thomas Joseph Kelly
  • Patent number: 7371271
    Abstract: An object of the present invention is to provide a composite soft magnetic sintered material that has high density, high mechanical strength and high relative magnetic permeability at high frequencies and, in order to achieve this object, the present invention provides a method of producing the composite soft magnetic sintered material, which comprises mixing a composite soft magnetic powder, that consists of iron powder, Fe—Si based soft magnetic iron alloy powder, Fe—Al based soft magnetic iron alloy powder, Fe—Si—Al based soft magnetic iron alloy powder, Fe—Cr based soft magnetic iron alloy powder or nickel-based soft magnetic alloy powder (hereinafter these powders are referred to as soft magnetic metal powder) of which particles arc coated with a ferrite layer which has a spinel structure, with 0.05 to 1.
    Type: Grant
    Filed: March 29, 2002
    Date of Patent: May 13, 2008
    Assignee: Mitsubishi Materials PMG Corporation
    Inventors: Kazunori Igarashi, Ryoji Nakayama, Koichiro Morimoto, Muneaki Watanabe
  • Patent number: 7364803
    Abstract: The present invention relates to a low cost technique for manufacturing dual helical gears, such as herringbone gears, from powder metals. The dual helical gears made by this technique are of high density (greater than 92% of theoretical density) and offer superior strength. The present invention more specifically discloses a forged metal herringbone gear which is comprised of a body and a plurality of teeth wherein the metal has a density of greater than 92% of theoretical and wherein the grain in the teeth is one range higher on the ASTM E 112 grain size chart than the grain in the body of the gear. The present invention also discloses a method for manufacturing a high density forged dual helical gear.
    Type: Grant
    Filed: June 21, 2005
    Date of Patent: April 29, 2008
    Assignee: Keystone Investment Corporation
    Inventor: Gary L. Anderson
  • Patent number: 7329381
    Abstract: A metallic article made of metallic constituent elements is fabricated from a mixture of nonmetallic precursor compounds of the metallic constituent elements. The mixture of nonmetallic precursor compounds is chemically reduced to produce an initial metallic material, without melting the initial metallic material. The initial metallic material is consolidated to produce a consolidated metallic article, without melting the initial metallic material and without melting the consolidated metallic article.
    Type: Grant
    Filed: June 14, 2002
    Date of Patent: February 12, 2008
    Assignee: General Electric Company
    Inventors: Andrew Philip Woodfield, Eric Allen Ott, Clifford Earl Shamblen
  • Patent number: 7311874
    Abstract: A method of fabricating a sputter target comprises: homogenously blending a plurality of powders including at least a first powder and a second powder. The first powder is comprised of chromium (Cr), cobalt (Co), ruthenium (Ru), nickel (Ni), or iron (Fe). The second powder is comprised of boron (B), carbon (C), a nitrogen (N)-containing material, a boride, a carbide, a nitride, a silicide, an oxygen (O)-containing material or an oxide. The second powder has a particle size of between 0.01 microns and 50 microns. The method further comprises: canning the blended plurality of powders to form a substantially non-segregated encapsulated powdered material mix; pressing the encapsulated powdered material mix to form a billet; and machining the billet to form a sputter target.
    Type: Grant
    Filed: December 19, 2003
    Date of Patent: December 25, 2007
    Assignee: Heraeus Inc.
    Inventor: Wenjun Zhang
  • Patent number: 7273584
    Abstract: An oxide dispersion strengthened martensitic steel excellent in high-temperature strength having residual ?-grains can be manufactured by a method comprising mixing either element powders or alloy powders and a Y2O3 powder; subjecting the resulting mixed powder to mechanical alloying treatment; solidifying the resulting alloyed powder by hot extrusion; and subjecting the resulting extruded solidified material to final heat treatment involving normalizing and tempering heat treatment to thereby manufacture an oxide dispersion strengthened martensitic steel in which Y2O3 particles are dispersed in the steel, wherein ?to ?transformation is not allowed to occur during the described hot extrusion and the proportion of residual ?-grains in which oxide particles are finely dispersed in high density is increased by controlling the mixture ratio of the powders for the mechanical alloying treatment.
    Type: Grant
    Filed: August 30, 2004
    Date of Patent: September 25, 2007
    Assignee: Japan Nuclear Cycle Development Institute
    Inventors: Satoshi Ohtsuka, Shigeharu Ukai, Takeji Kaito, Takeshi Narita, Masayuki Fujiwara
  • Patent number: 7241368
    Abstract: The present invention relates to a hafnium silicide target for forming a gate oxide film composed of HfSi0.05-0.37. Obtained is a hafnium silicide target superior in workability and embrittlement resistance, and suitable for forming a HfSiO film and HfSiON film that may be used as a high dielectric gate insulation film in substitute for a SiO2 film, and the manufacturing method thereof.
    Type: Grant
    Filed: June 5, 2002
    Date of Patent: July 10, 2007
    Assignee: Nippon Mining & Metals Co., Ltd.
    Inventors: Shuichi Irumata, Ryo Suzuki
  • Patent number: 7229588
    Abstract: A cobalt-chromium-boron-platinum sputtering target alloy having multiple phases. The alloy can include Cr, B, Ta, Nb, C, Mo, Ti, V, W, Zr, Zn, Cu, Hf, O, Si or N. The alloy is prepared by mixing Pt powder with a cobalt-chromium-boron master alloy, ball milling the powders and HIP'ing to densify the powder into the alloy.
    Type: Grant
    Filed: January 13, 2004
    Date of Patent: June 12, 2007
    Assignee: Heraeus, Inc.
    Inventors: Michael Sandlin, Bernd Kunkel, Willy Zhang, Phillip Corno
  • Patent number: 7223950
    Abstract: A microwave burning furnace including a housing constituted by a metal on which a microwave is to be irradiated, a metallic door provided in the housing, a burning chamber provided in the housing and surrounded by a material having a low microwave absorption characteristic and a high heat insulating property, and microwave generating means, wherein the burning chamber includes a heater element constituted by at least two types of heating materials having a heating material for a high temperature region which automatically generates a heat mainly in the high temperature region to have a burning temperature by an irradiation of a microwave and a heating material for a low temperature region which automatically generates a heat mainly in the low temperature region including an ordinary temperature.
    Type: Grant
    Filed: February 4, 2005
    Date of Patent: May 29, 2007
    Assignees: Matsushita Electric Industrial Co., Ltd., National Institute for Fusion Science
    Inventors: Eiji Nomura, Jun Nomura, Motoyasu Sato
  • Patent number: 7175802
    Abstract: Spent sputtering targets are refurbished by filling the depleted region of the target with new sputter material using a hot isostatic pressing or HIP'ing technique.
    Type: Grant
    Filed: September 16, 2002
    Date of Patent: February 13, 2007
    Assignee: Heraeus, Inc.
    Inventors: Michael Sandlin, Wenjun Zhang, Bernd Kunkel
  • Patent number: 7153468
    Abstract: A method includes combining a solid first material and a solid second material and melting at least a portion of the first material sufficient to coat the second material and any remaining first material. An approximately homogenous distribution of the second material can be formed throughout the liquid phase of the first material. The first material liquid phase can then be solidified to define a composite target blank exhibiting an approximately homogenous distribution of the solid second material in a matrix of the solidified first material. The first material can comprise SE and the second material can comprise Ge and/or Ag. The composite target blank can include at least about 50 vol % matrix. The first and second materials can be powdered metals. Accordingly, a physical vapor deposition target can include a matrix of a first material and an approximately homogenous distribution of particles of a second material throughout the first material matrix.
    Type: Grant
    Filed: August 16, 2001
    Date of Patent: December 26, 2006
    Assignee: Honeywell International Inc.
    Inventors: Vasanth Mohan, Jianxing Li, Timothy A. Scott
  • Patent number: 7144547
    Abstract: In a target for cathode discharging arc ion plating containing Al and Cr as an essential ingredient according to the invention, the thickness of the Al and Cr compound layer formed between Cr particles and Al contained in a target is 30 ?m or less. Alternatively, the total for the peak intensities of Al—Cr compound observed between diffraction angles between 10 to 80° by X-ray diffractiometry according to ?=2? method is 10% or less relative to the total for the peak intensities of Al, Cr and the Al—Cr compound. Further, the relative density of the target is 92% or more. The target is capable of forming hard films of high quality while preventing not uniform movement of arc spots and suppressing formation of macro particles.
    Type: Grant
    Filed: March 26, 2003
    Date of Patent: December 5, 2006
    Assignee: Kabushiki Kaisha Kobe Seiko Sho (Kobe Steel, Ltd.)
    Inventors: Kenji Yamamoto, Toshiki Sato, Yasuo Nakane, Hidekazu Morimoto, Yoichiro Yoneda
  • Patent number: 7108830
    Abstract: A method of production of large Ingots of neutron attenuating composites using a vacuum-bellows system allows for large cross-sectional shapes to be extruded and rolled. This method uses a vacuum-bellows technology which allows the manufacturing of large 8–16 inch diameter ingots (50–450 lbs. each). A variety of primary metal matrix materials can be used in this technology. High specific strength and stiffness can be achieved because the technology allows for final densities of 99% and higher. The vacuum-bellows technology allows metals and ceramics to blend and mesh together at compression pressures of 800 tons with elevated temperatures. The controlled compression movement allows for any oxide layer, on the metal, to be broken up and consolidated with the chosen ceramic particulate. One application is to blend boron-rich ceramics and high purity (99.5–99.99%) aluminum particulates together and produce a large ingot using this vacuum-bellows technology.
    Type: Grant
    Filed: September 9, 2002
    Date of Patent: September 19, 2006
    Assignee: Talon Composites
    Inventor: Robin A. Carden
  • Patent number: 7097807
    Abstract: Objects comprising Al-7.5 Mg particulate having pressure consolidated nanocrystalline coating material are formed. Oxides of the coating material, in particulate form, may become dispersed in the pressure consolidated, thereby increasing its strength.
    Type: Grant
    Filed: April 3, 2003
    Date of Patent: August 29, 2006
    Assignee: Ceracon, Inc.
    Inventors: Henry S. Meeks, III, Marc S. Fleming
  • Patent number: 7077883
    Abstract: The present invention relates to a pre-alloyed powder and its use as a bond powder in the manufacture of powder metallurgy parts and of diamond tools in particular. A pre-alloyed powder is disclosed, based on the iron-copper dual phase system, additionally containing Co, Ni, Mo, W, oxides or carbides as reinforcing elements in the iron phase, and Sn in the copper phase.
    Type: Grant
    Filed: September 28, 2004
    Date of Patent: July 18, 2006
    Assignee: Umicore
    Inventors: Bert-Jan Kamphuis, Janneck Peersman
  • Patent number: 7074247
    Abstract: There is provided a method of making a composite abrasive compact which comprises an abrasive compact bonded to a substrate. The abrasive compact will generally be a diamond compact and the substrate will generally be a cemented carbide substrate. The composite abrasive compact is made under known conditions of elevated temperature and pressure suitable for producing abrasive compacts. The method is characterised by the mass of abrasive particles from which the abrasive compact is made. This mass has three regions which are: (i) an inner region, adjacent the surface of the substrate on which the mass is provided, containing particles having at least four different average particle sizes; (ii) an outer region containing particles having at least three different average particle sizes; and (iii) an intermediate region between the first and second regions.
    Type: Grant
    Filed: October 15, 2001
    Date of Patent: July 11, 2006
    Inventors: Klaus Tank, Moosa Mahomed Adia, Roy Derrick Achilles, Paul Machael Daniel
  • Patent number: 7037464
    Abstract: In an oxide dispersion strengthened martensitic steel which comprises, by % by weight, 0.05 to 0.25% C, 8.0 to 12.0% Cr, 0.1 to 4.0% W, 0.1 to 1.0% Ti, 0.1 to 0.5% Y2O3 with the balance being Fe and unavoidable impurities and in which Y2O3 particles are dispersed in the steel, by adjusting the Ti content within the range of 0.1 to 1.0% so that an excess oxygen content Ex.O in steel satisfies [0.22×Ti (% by weight)<Ex.O (% by weight)<0.46×Ti (% by weight)], the oxide particles are finely dispersed and highly densified to thereby obtain an oxide dispersion strengthened martensitic steel excellent in high-temperature strength. It is also possible to reduce the amount of oxygen contamination in steel during the mechanical alloying of raw material powders to provide Ex.O within a predetermined range, by carrying out the mechanical alloying in an Ar atmosphere having a super purity of not less than 99.
    Type: Grant
    Filed: August 7, 2003
    Date of Patent: May 2, 2006
    Assignee: Japan Nuclear Cycle Development Institute
    Inventors: Satoshi Ohtsuka, Shigeharu Ukai, Takeji Kaito, Takeshi Narita, Masayuki Fujiwara
  • Patent number: 7037466
    Abstract: After recycled titanium alloy chips are crushed and cleaned, they are pressed into cylindrically briquettes with a relative density of 0.6, and placed into capsules. The capsules are heated and placed into a preheated pressing rig. The pressing rig repetitively applies axial force to the capsule, resulting in a relative density of at least 0.95. The product billets are used for consumable electrodes, secondary casting alloys, forgings, extruded semi-finished products and the like.
    Type: Grant
    Filed: September 29, 2003
    Date of Patent: May 2, 2006
    Inventors: Vladimir Leonidovich Girshov, Arnold Nikolayevich Treschevskiy, Victor Georgievich Kochkin, Alexey Alexandrovich Abramov, Natalja Semenovna Sidenko
  • Patent number: 6960319
    Abstract: Disclosed is a flow-softening tungsten alloy having the general formula: W100-pAiBjCkDe wherein W is tungsten; A is one or more elements selected from the group consisting of nickel, iron, chromium and cobalt; B is in or more elements selected from the group consisting of molybdenum, niobium and tantalum; C is one or more of the elements selected from the groups consisting of titanium and aluminum; D is one or more elements selected from the group consisting of boron, carbon, and silicon; i is from about 5 to about 8 weight percent; j is from 0 to about 4 weight percent; k is from about 0.1 to about 4 weight percent; 1 is from 0 to about 0.1 weight percent; and p is greater than or equal to about 7 weight percent and less than or equal to about 20 weight percent. In this alloy p is approximately equal to the sum of i, j, k and 1. A method of preparing this alloy and a kinetic energy penetrator manufactured from it are also disclosed.
    Type: Grant
    Filed: October 27, 1995
    Date of Patent: November 1, 2005
    Assignee: The United States of America as represented by the Secretary of the Army
    Inventor: Deepak Kapoor
  • Patent number: 6946096
    Abstract: A method for making aerospace face seal rotors reinforced by rhenium metal, alloy, or composite in combination with silicon carbide or other ceramic. The resulting rotor also is disclosed. Ceramic grains, preferably silicon carbide (SiC), are mixed with powdered metallic (PM) binder that may be based on a refractory metal, preferably rhenium. The mixture is applied to a rotor substrate. The combined ceramic-metal powder mixture is heated to sintering temperature under pressure to enable fusion of the ceramic in the resulting metal-based substrate. A load may then be applied under an elevated temperature. The resulting coated rotor can exhibit high hot hardness, increased durability and/or high hot wear resistance, as well as high thermal conductivity.
    Type: Grant
    Filed: May 15, 2003
    Date of Patent: September 20, 2005
    Assignee: Honeywell International, Inc.
    Inventors: William L. Giesler, Robbie J. Adams
  • Patent number: 6939508
    Abstract: A method for manufacturing a net-shaped bimetallic part that includes the steps of: providing a tool that defines a cavity and a tooling surface; depositing a layer of an environmental metal material onto the tooling surface; filling the cavity in the tool with a powdered metal material; and simultaneously heating the tool and subjecting the tool to a pressurized gas to consolidate the powdered metal material and diffusion bond the environmental metal material to the consolidated powdered metal material to form a bimetallic part.
    Type: Grant
    Filed: October 24, 2002
    Date of Patent: September 6, 2005
    Assignee: The Boeing Company
    Inventors: Clifford C. Bampton, Victor Samarov
  • Patent number: 6921510
    Abstract: An article has a metallic matrix made of its constituent elements with a dispersoid distributed therein. The article is prepared by furnishing at least one nonmetallic matrix precursor compound. All of the nonmetallic matrix precursor compounds collectively include the constituent elements of the metallic matrix in their respective constituent-element proportions. A mixture of an initial metallic material and the dispersoid is produced. The matrix precursor compounds are chemically reduced to produce the initial metallic material, without melting the initial metallic material, and the dispersoid is distributed in the initial metallic material. The mixture of the initial metallic material and the dispersoid is consolidated to produce a consolidated article having the dispersoid distributed in the metallic matrix comprising the initial metallic material. The initial metallic material, the dispersoid, and the consolidated article are not melted during the consolidation.
    Type: Grant
    Filed: January 22, 2003
    Date of Patent: July 26, 2005
    Assignee: General Electric Company
    Inventors: Eric Allen Ott, Andrew Philip Woodfield, Clifford Earl Shamblen, Michael Francis Xavier Gigliotti
  • Patent number: 6852273
    Abstract: (a) The metal matrix composite is suitable for the manufacture of flat or shaped titanium aluminide, zirconium aluminide, or niobium aluminide articles and layered metal composites having improved mechanical properties such as lightweight plates and sheets for aircraft and automotive applications, thin cross-section vanes and airfoils, heat-sinking lightweight electronic substrates, bulletproof structures for vests, partition walls and doors, as well as sporting goods such as helmets, golf clubs, sole plates, crown plates, etc. The composite material consists of a metal (e.g., Ti, Zr, or Nb-based alloy) matrix at least partially intercalated with a three-dimensional skeletal metal aluminide structure, whereby ductility of the matrix metal is higher than that of the metal aluminide skeleton. The method for manufacturing includes the following steps: (a) providing an aluminum skeleton structure having open porosity of 50-95 vol.
    Type: Grant
    Filed: January 29, 2003
    Date of Patent: February 8, 2005
    Assignee: ADMA Products, Inc.
    Inventors: Eugene Ivanov, Vladimir S. Moxson
  • Patent number: 6849102
    Abstract: A discontinuously reinforced metal composite, having a metal matrix and a plurality of intermetallic particles comprising at least two different metals, the intermetallic particles having a size ranging from 1 ?m to about 10 ?m and being dispersed within the metal matrix in an amount of at least 20% by volume, wherein the intermetallic particles are particles having at least one same metal as the metal in the metal matrix.
    Type: Grant
    Filed: June 13, 2003
    Date of Patent: February 1, 2005
    Assignee: Touchstone Research Laboratory, Ltd.
    Inventors: Gollapudi S. Murty, Brian E. Joseph
  • Patent number: 6827755
    Abstract: A high-strength and high-toughness ferritic steel having a tensile strength of not less than 1,000 MPA and a Charpy impact value of not less than 1 MJ/m2 is provided. A ferritic steel comprising, by weight, not more than 1% Si, not more than 1.25% Mn, 8 to 30% Cr, not more than 0.2% C, not more than 0.2% N, not more than 0.4% O, a total amount of not more than 12% of at least one compound-forming element selected from the group of Ti, Zr, Hf, V and Nb in amounts of not more than 3% Ti, not more than 6% Zr, not more than 10% Hf, not more than 1.0% V and not more than 2.0% Nb, also containing where necessary not more than 0.3% Mo, not more than 4% W and not more than 1.6% Ni, and the balance consisting of Fe and unavoidable impurities, and having an average crystal grain size of not more than 1 &mgr;m, can be obtained by a method comprising encapsulating a steel powder produced by mechanical alloying, and subjecting the encapsulated steel powder to plastic deformation.
    Type: Grant
    Filed: July 2, 2002
    Date of Patent: December 7, 2004
    Assignee: Hitachi, Ltd.
    Inventors: Masami Taguchi, Ryo Ishibashi, Yasuhisa Aono, Hidehiko Sumitomo, Hiroki Masumoto, Masakuni Fujikura
  • Patent number: 6814775
    Abstract: A sintered cubic boron nitride (cBN) compact for use in a tool is composed of between about 60 and 80 vol-% cBN having a volumetric mean particle size of between about 3 to 6 &mgr;m and between about 40 and 20 vol-% of a ceramic binder phase. The ceramic binder is composed of between about 20 and 60 vol-% of one or more of a carbide, nitride, or boride of a Group IVB or VIB metal, and between about 40 and 80 vol-% of one or more of carbides, nitrides, borides, or oxides of aluminum. The cBN compact additionally contains between about 3 and 15 wt-% tungsten. The cBN compacts are especially useful in machining iron and like chemically reactive parts, especially where such parts are powder metal parts.
    Type: Grant
    Filed: May 14, 2003
    Date of Patent: November 9, 2004
    Assignee: Diamond Innovations, Inc.
    Inventors: Robert Dean Scurlock, Stephen Lee Dole
  • Patent number: 6811745
    Abstract: A method to produce annular-shaped, metal-clad cermet components directly produces the form and avoids multiple fabrication steps such as rolling and welding. The method includes the steps of: providing an annular hollow form with inner and outer side walls; filling the form with a particulate mixture of ceramic and metal; closing, evacuating, and hermetically sealing the form; heating the form to an appropriate temperature; and applying force to consolidate the particulate mixture into solid cermet.
    Type: Grant
    Filed: January 16, 2003
    Date of Patent: November 2, 2004
    Assignee: UT-Battelle, LLC
    Inventors: Charles W. Forsberg, Vinod K. Sikka
  • Publication number: 20040208774
    Abstract: The present invention relates to a method of manufacturing sputtering targets doped with non-metal components including borides, carbides, nitrides or oxides. A powder process is utilized whereby alloyed powders, which contain non-metal elements of B/C/N/O and non-metal containing phases of less than ten microns in microstructure, are blended, canned and subjected to press consolidation. The sputtering targets of the present invention avoid spitting problems during sputtering of the target material on a substrate.
    Type: Application
    Filed: December 19, 2003
    Publication date: October 21, 2004
    Inventor: Wenjun Zhang
  • Publication number: 20040188249
    Abstract: A cobalt-chromium-boron-platinum sputtering target alloy having multiple phases. The alloy can include Cr, B, Ta, Nb, C, Mo, Ti, V, W, Zr, Zn, Cu, Hf, O, Si or N. The alloy is prepared by mixing Pt powder with a cobalt-chromium-boron master alloy, ball milling the powders and HIP'ing to densify the powder into the alloy.
    Type: Application
    Filed: January 13, 2004
    Publication date: September 30, 2004
    Applicant: HERAEUS, INC.
    Inventors: Michael Sandlin, Bernd Kunkel, Willy Zhang, Phillip Corno
  • Publication number: 20040182700
    Abstract: It is an object of the present invention to provide a silicon monoxide sinter having a uniform texture, good machinability, and splash resistance, which are all required of a silicon monoxide vapor deposition material, or a silicon monoxide sinter having a diameter of at least 100 mm and the shape required of a sputtering target material, and to obtain both of these sinters stably and with good productivity. A silicon monoxide sinter with a bulk density of at least 1.68 g/cm3 can be obtained by sintering under hot pressing conditions comprising a pressing pressure of at least 15 MPa and a temperature of 1200 to 1350° C., and by using a press die which comprises an inner die divided into a plurality of segments and integrated in an integrated outer die with a gap therebetween, and a cushioning material disposed in this gap, it is possible to obtain a silicon monoxide sinter whose diameter is at least 100 mm and whose bulk density is at least 2.
    Type: Application
    Filed: July 17, 2003
    Publication date: September 23, 2004
    Inventors: Yoshitake Natsume, Takashi Onishi, Tadashi Ogasawara, Munetoshi Watanabe, Toshiharu Iwase
  • Patent number: 6767505
    Abstract: A gas operated part forming die apparatus has compact high tonnage presses which are operated by high pressure gas generated within chambers and controlled to operate high pressure pistons and dies for compressing particulate material into dense formed parts. Combustion chambers are filled with pressurized mixtures of combustible gases and diluents. Elongated chambers have insulating walls and spaced electrodes. Some contain liquid or particulate ablatable materials or ablatable liners. Others extend fuzes between the electrodes and are filled with pressurized gases. Gas is removed from the particulate material. Die cavities may be precompressed during filing of chambers with pressurized gas. Igniting the combustible gases or creating arcs between the electrodes produces rapidly expanding high pressure resultant gases for driving pistons and movable dies and rapidly compressing die cavities. Pressures in the chambers are contained, or pistons are restrained until releasing and driving the pistons.
    Type: Grant
    Filed: July 12, 2001
    Date of Patent: July 27, 2004
    Assignee: Utron Inc.
    Inventors: F. Douglas Witherspoon, Dennis W. Massey, T. Arul Mozhi, David L. Kruczynski, John M. Ryan
  • Patent number: 6744025
    Abstract: The invention relates to an apparatus for hot-pressing a planar product in a process using microwave heating. The apparatus comprises a constant-volume, box-like microwave resonant cavity divided into two opposed subcavities by an elongated gap suitable for passing therethrough the product (1) to be heated. The product is guided through the gap by conveyor belts (2, 2′) of microwave-transparent material. The subcavities are delineated from the conveyor passageway gap by parallel walls of microwave-transparent material, each one of them sealed so as to form a wall of its own subcavity. At least one of the subcavities is pressurized, whereby the sealed wall of the pressurized subcavity is designed to yield under the pressure applied into the subcavity in a direction perpendicular to the product (1) to be pressed.
    Type: Grant
    Filed: February 10, 2003
    Date of Patent: June 1, 2004
    Assignee: Raute Oyj
    Inventor: Jaakko Vilo
  • Patent number: 6729003
    Abstract: A process of producing a ceramic electronic component comprises external electrodes having first electrode layers containing at least a noble metal, cuprous oxide, and glass ingredient electrically connected to internal electrodes comprising a noble metal. As the ceramic electronic components, for example, a multi-layer ceramic capacitor, multi-layer varistor, multi-layer dielectric resonator, multi-layer piezoelectric element, etc. may be mentioned.
    Type: Grant
    Filed: November 8, 2001
    Date of Patent: May 4, 2004
    Assignee: TDK Corporation
    Inventors: Hideki Yokoyama, Takaya Ishigaki, Akira Sasaki, Shintarou Kon, Tetuji Maruno
  • Publication number: 20040071582
    Abstract: To manufacture a flange for a compressor with a relief groove by using powder metallurgy in order to prevent deformation of the compressor in operation, powder material for the flange is charged into a mold; an ablative member having a melting point lower than that of the powder material is positioned at a place where a relief groove is to be formed; the flange is formed by compressing the powder material and the ablative member; and the formed flange is sintered at a temperature between the melting points of the power material and the ablative member so as to melt and remove the ablative member.
    Type: Application
    Filed: September 11, 2003
    Publication date: April 15, 2004
    Inventor: Jong-Kwan Park
  • Publication number: 20040067155
    Abstract: The present invention relates generally to metallic chips recycling, particularly, titanium alloys metal chips, and more particularly to said chips to form billets that can then be used for producing consumable electrodes for obtaining secondary casting alloys, in blacksmith's work for obtaining forgings, extruded semi-finished products and the like.
    Type: Application
    Filed: September 29, 2003
    Publication date: April 8, 2004
    Inventors: Vladimir Leonidovich Girshov, Arnold Nikolayevich Treschevskiy, Victor Georgievich Kochkin, Alexey Alexandrovich Abramov, Natalja Semenovna Sidenko
  • Patent number: 6716389
    Abstract: A process for producing sintered pellets made from blends of refractory metal and refractory metal nitride powders were found to have a higher fraction of intra-agglomerate pores than those made from the refractory metal or refractory metal nitride alone resulting in improved capacitor grade powders, anodes and finished capacitors therefrom. The pellet porosity and total intrusion volume maximizes when the mixture is in the 50-75 W/W % refractory metal nitride range. The total pellet pore surface area was found to be relatively independent of refractory metal nitride concentration above 50%. A substrate consisting of a 50/50 or 25/75 W/W % refractory metal/refractory metal nitride powder mixture should produce solid capacitors with higher capacitance recovery and lower ESR.
    Type: Grant
    Filed: October 25, 2002
    Date of Patent: April 6, 2004
    Assignee: H. C. Starck Inc
    Inventors: Terrance B. Tripp, Barbara L. Cox
  • Patent number: 6712871
    Abstract: A sintered alloy composition for automotive engine valve seats, and a method for producing the same, are described. An iron base sintered alloy composition comprising vanadium carbide particles, Fe—Co—Ni—Mo alloy particles, and Cr—W—Co—C alloy particles in which the composition is dispersed in a structure of sorbite is particularly suitable for use as materials of valve seats for automotive engines which requires excellent wear resistance, high-performance, high-rotation-speed, and low-fuel-consumption.
    Type: Grant
    Filed: August 29, 2002
    Date of Patent: March 30, 2004
    Assignee: Hyundai Motor Company
    Inventor: Jung Seok Oh
  • Publication number: 20040040837
    Abstract: A method of fabricating a glass containing target for sputter deposition of a glass onto a substrate. The method includes synthesizing a glass from pure chemical element materials and then forming the synthesized glass into a powder, which is then used to form a glass containing target. In accordance with one aspect of the invention, the glass containing target may be used for sputter deposition of a thin coating of glass on a substrate. In exemplary embodiments, the glass is a chalcogenide glass target useful in fabricating memory devices.
    Type: Application
    Filed: August 29, 2002
    Publication date: March 4, 2004
    Inventors: Allen McTeer, Jiutao Li, Terry L. Gilton
  • Patent number: 6676893
    Abstract: The presently claimed invention relates to a method of making a PcBN cutting tool insert. The method includes the following steps: mixing raw material powders, (e.g., cBN, hBN, TiC, TiN, Ti(C,N), WC, W, C, Co, Co2Al9, Al AlN, Al2O3) with a liquid (e.g., ethanol) and an agent (e.g., polyethylene glycol, PEG) to form a homogeneous slurry with the desired composition; forming spherical powder agglomerates, typically 100 &mgr;m in diameter, preferably by spray drying; pressing said agglomerates to form a body of desired dimensions and density using conventional tool pressing technology; removing the agent from the powder at a suitable temperature and atmosphere; raising the temperature to 1000-1350° C. in vacuum; solid state sintering the body at 1000-1350° C. in vacuum, for 1-90 minutes to form a body with 35-55 vol % porosity; optionally, adding 0.
    Type: Grant
    Filed: April 25, 2002
    Date of Patent: January 13, 2004
    Assignee: Sandvik AB
    Inventors: Ulf Rolander, Gerold Weinl
  • Patent number: 6676728
    Abstract: There is provided a method of making a high-melting metal powder which has high purity and excellent formability and, particularly, of a metal powder of spherical particles made of Ta, Ru, etc. having a higher melting point than iron. There is also provided a target of high-melting metal or its alloy, which is made by the sintering under pressure of these powders and which has high purity and a low oxygen concentration and shows high density and a fine and uniform structure. A powder metal material mainly composed of a high-melting metal material is introduced into a thermal plasma into which hydrogen gas has been introduced, thereby to accomplish refining and spheroidizing. Further, an obtained powder is pressed under pressure by hot isostatic pressing, etc.
    Type: Grant
    Filed: August 21, 2002
    Date of Patent: January 13, 2004
    Assignee: Hitachi Metals, Ltd.
    Inventors: Gang Han, Hideo Murata, Hideki Nakamura
  • Patent number: 6666901
    Abstract: Targets for the fabrication of quasicrystalline films are prepared from powders of the elemental constituents of the objective quasicrystalline material that have been pressed into a required target shape. The temperature of target fabrication is maintained sufficiently low that quasicrystalline alloy formation does not occur during target fabrication. Due to the high thermal shock resistance of each of the individual constituents and due to the dispersed form of the powders comprising the target, the target demonstrates very high resistance to thermal shock.
    Type: Grant
    Filed: November 8, 2001
    Date of Patent: December 23, 2003
    Assignee: Technology Assessment & Transfer, Inc.
    Inventor: Larry Lee Fehrenbacher
  • Patent number: 6652616
    Abstract: In accordance with the method according to the present invention, particles consisting of ferrotitanium, ferroniobium or ferrovanadium are dispersed and hot compacted in a metal matrix powder consisting of hardening steel or heat-resistant alloys. In so doing, titanium, niobium or vanadium carbide is obtained in situ by a solid-state reaction, i.e. without melting, from the carbon admixed or contained in the matrix powder and the ferroalloy particles. Carbon can also be absorbed from the gaseous phase and it may be substituted by nitrogen. This method permits a reasonably-priced introduction of hard particles into the composite material, the hard particles having a size that is necessary as a protection against scoring wear.
    Type: Grant
    Filed: May 28, 2002
    Date of Patent: November 25, 2003
    Assignee: Maschienfabrik Koppern GmbH & Co. KG
    Inventors: Hans Berns, Birgit Wewers