Powder Pretreatment Patents (Class 419/62)
  • Publication number: 20100233014
    Abstract: A powder metallurgical combination is provided comprising an iron-based powder A comprising core particles of iron to which core particles nickel is diffusion alloyed and wherein said nickel diffusion alloyed to said core particles comprises 4-7% (preferably 4.5-6%) by weight of said iron-based powder A, and a powder B substantially consisting of particles of pure iron. Further a method is provided for preparing a powder metallurgical combination.
    Type: Application
    Filed: July 10, 2008
    Publication date: September 16, 2010
    Applicant: HOGANAS AB (PUBL)
    Inventor: Mats Larsson
  • Patent number: 7794649
    Abstract: The present invention is directed to a method of making heat cells that are suitable for incorporation into disposable heating wraps. The heat cells comprise an exothermic composition comprising an absorbent gelling material, wherein the absorbent gelling material provides for improved heat application in the relief of temporary or chronic body aches and pains.
    Type: Grant
    Filed: September 23, 2005
    Date of Patent: September 14, 2010
    Assignee: Wyeth LLC
    Inventors: Vincent York-Leung Wong, Clarence Anthony Turley
  • Publication number: 20100166593
    Abstract: A production method of an extrusion billet includes a step of preparing a plate or lump starting material comprising a magnesium alloy, a step of performing a plastic deformation process at a rolling reduction of 70% or more to the starting material at a temperature of 250° C. or lower to introduce a strain without generating dynamic recrystallization, a step of producing powder by granulating the material after the plastic deformation process, and a step of producing a powder billet by compressing the powder.
    Type: Application
    Filed: June 19, 2008
    Publication date: July 1, 2010
    Applicant: KURIMOTO, LTD.
    Inventors: Katsuyoshi Kondoh, Makoto Hotta, Jinsun Liao, Kantaro Kaneko, Norio Fujii, Hirohito Kametani, Akihiko Koshi
  • Publication number: 20100116471
    Abstract: A composite article (1; 10; 40) comprises a plurality of inclusions (5) of a magnetocalorically active material embedded in a matrix (4) of a magnetocalorically passive material. The inclusions (5) and the matrix (4) have a microstructure characteristic of a compacted powder.
    Type: Application
    Filed: December 27, 2007
    Publication date: May 13, 2010
    Inventors: Georg Werner Reppel, Matthias Katter
  • Publication number: 20100108503
    Abstract: In one example embodiment, a sputter target structure for depositing semiconducting chalcogenide films is described. The sputter target includes a target body comprising at least one chalcogenide alloy having a chalcogenide alloy purity of at least approximately 2N7, gaseous impurities less than 500 ppm for oxygen (O), nitrogen (N), and hydrogen (H) individually, and a carbon (C) impurity less than 500 ppm. In a particular embodiment, the chalcogens of the at least one chalcogenide alloy comprises at least 20 atomic percent of the target body composition, and the chalcogenide alloy has a density of at least 95% of the theoretical density for the chalcogenide alloy.
    Type: Application
    Filed: October 27, 2009
    Publication date: May 6, 2010
    Applicant: APPLIED QUANTUM TECHNOLOGY, LLC
    Inventors: Brian Josef Bartholomeusz, Michael Bartholomeusz
  • Publication number: 20100098574
    Abstract: Provided are methods comprising at least one metal powder with an extractable material and a composition comprising a polyol, a hydrophilic polymer, or both in order to form a mixture in which the metal powder and the extractable material assume respective positions. The composition functions as a homogenizing agent that allows the mixture to remain well-mixed for extended periods of time under ambient conditions. Also provided are green bodies and porous constructs, including implants, that are made in accordance with the disclosed methods. The green bodies and porous constructs have a substantially uniform porosity that is at least partially attributable to the ability of the composition to maintain the metal powder and the extractable material in their respective positions prior to sintering.
    Type: Application
    Filed: August 13, 2009
    Publication date: April 22, 2010
    Inventors: Hengda D. Liu, Bryan Smith, Richard King
  • Publication number: 20100034688
    Abstract: There is provided a method of manufacturing a permanent magnet having extremely high orientation by arranging such that the crystal fractures of alloy raw meal powder having more equal crystal orientational relationship are combined in magnetic field. In this invention, alloy raw meal powder is filled into a cavity and, while agitating the alloy raw meal powder inside the cavity, is oriented in the magnetic field. This oriented body is then compression molded in the magnetic field into a predetermined shape.
    Type: Application
    Filed: November 19, 2007
    Publication date: February 11, 2010
    Inventors: Hiroshi Nagata, Yoshinori Shingaki
  • Publication number: 20100009855
    Abstract: The present invention provides a process for joining oxide-superconducting tubes with a superconducting joint. The process involves the preparation of a partially preformed superconducting material, followed by cold isopressing of the powder of partially performed superconducting material into tube shape and further provided with grooves at both ends of the tubes with a subsequent deposition of a silver layer. The process further involves the lapping of one of the end faces of a pair of said tubes to be joined. These lapped end faces of both the tubes clubbed together on a common silver bush are coated with a paste of the same partially preformed superconducting material in organic formulation. Then these coated end faces are closed pressed together to form a joint. This joint portion and the end portions of the tubes are wrapped with a perforated silver foil followed by deposition of another layer of silver.
    Type: Application
    Filed: December 31, 2007
    Publication date: January 14, 2010
    Inventors: Shrikant Narayan Ekbote, Gursharan Kaur Padam, Narendra Kumar Arora, Mukul Sharma, Ramesh Sethi
  • Publication number: 20100003536
    Abstract: According to the present invention there is provided a metal matrix composite material and a method for the manufacture thereof, the material comprising an aluminium-based alloy matrix, the matrix comprising a microstructure composed of at least a first aluminium alloy phase and having a second phase of nanostructured quasicrystalline particles embedded therein and further including in said matrix fibrils of at least one other dissimilar material.
    Type: Application
    Filed: October 22, 2007
    Publication date: January 7, 2010
    Inventors: George David William Smith, Patrick Spencer Grant, Marina Lorena Galano, Fernando Enrique Audebert
  • Publication number: 20090320961
    Abstract: A magnet core is required to be particularly dense, made of alloys produced in a rapid solidification process and have a minimal coercitive field strength. To achieve these aims, a coarse-grain powder fraction is first produced from an amorphous strip of a soft magnetic alloy. In addition, at least one fine-grain powder fraction is produced from a nanocrystalline strip of a soft magnetic alloy. The particle fractions are then mixed to produce a multi-modal powder, wherein the particles of the coarse-grain particle fraction have an amorphous structure and the particles of the fine-grain powder fraction have a nanocrystalline structure. The multi-modal powder is then pressed to produce a magnet core.
    Type: Application
    Filed: July 11, 2007
    Publication date: December 31, 2009
    Applicant: VACUUMSHMELZE GMBH & CO.KG
    Inventor: Markus Brunner
  • Publication number: 20090317280
    Abstract: A method for manufacturing a metal-based ceramic composite target containing noble metal is provided, which includes firstly applying a ceramic powder uniformly onto a surface of a magnetic metal powder by using a wet powder mixing process, and drying it to obtain a ceramic-metal composite powder, and then uniformly mixing a noble metal powder with the ceramic-metal powder by using a dry powder mixing process, and finally making the ceramic-metal composite powder into a compact target by using a molding and compacting process. The manufacturing method of the present invention can uniformly mix the powders of the magnetic metal, the ceramic, and the noble metal, and reduce the loss of the noble metal powder in the production process of the target, so as to improve the quality of the target and decrease the production cost thereof.
    Type: Application
    Filed: September 26, 2008
    Publication date: December 24, 2009
    Applicant: CHINA STEEL CORPORATION
    Inventors: Jung-Chih Chen, Shu-Hua Yuchen, In-Ting Hong, Fu-Tzao Chen, Cheng-Tung Liu
  • Publication number: 20090292365
    Abstract: Provided are methods for processing a green body that includes compacted metal powder, comprising impacting the green body with a particulate material for a time and under conditions effective to displace a portion of the metal powder from the green body. The present methods can be used to prepare green bodies that have “roughened” surfaces and that can be used to make orthopedic implants displaying low movement relative to bone when installed in situ, which corresponds to higher stability upon implantation and decreases the time required for biological fixation of the implant. Also provided are implants comprising a metallic matrix, and methods comprising surgically installing an implant prepared from a “surface roughened” green body in accordance with the present invention.
    Type: Application
    Filed: May 21, 2009
    Publication date: November 26, 2009
    Applicant: DEPUY PRODUCTS, INC.
    Inventors: Bryan Smith, Jeffrey A. Rybolt, Derek Hengda Liu, Andrew James Martin
  • Publication number: 20090181179
    Abstract: A method for producing a composite metal powder according to one embodiment of the invention may comprise: Providing a supply of molybdenum metal powder; providing a supply of a sodium compound; combining the molybdenum metal powder and the sodium compound with a liquid to form a slurry; feeding the slurry into a stream of hot gas; and recovering the composite metal powder.
    Type: Application
    Filed: January 11, 2008
    Publication date: July 16, 2009
    Applicant: CLIMAX ENGINEERED MATERIALS, LLC
    Inventors: Naresh Goel, Carl Cox, Dave Honecker, Eric Smith, Chris Michaluk, Adam DeBoskey, Sunil Chandra Jha
  • Publication number: 20090123329
    Abstract: The invention relates to a metal matrix material based on shape-memory alloy powders, to the production method thereof and to the use of same. More specifically, the invention relates to a metal matrix material which is characterised in that it is based on particles of shape-memory alloy powder, having a base of copper at a concentration of between 45 vol.-% and 70 vol.-% in relation to the total volume of the material, said powder particles being supported by a metal matrix. The invention also relates to a method of producing the aforementioned material and to the use of same for absorbing vibrations, particularly acoustic and mechanical vibrations.
    Type: Application
    Filed: August 30, 2006
    Publication date: May 14, 2009
    Applicant: Universidad Del Pais Vasco Euskal Herriko Unibertsitatea
    Inventors: Jose Maria San Juan Nunez, Maria Luisa No Sanchez
  • Publication number: 20090107837
    Abstract: A method of recycling ruthenium (Ru) and Ru-based alloys comprises steps of: providing a solid body of Ru or a Ru-based alloy; segmenting the body to form a particulate material; removing contaminants, including Fe, from the particulate material; reducing the sizes of the particulate material to form a powder material; removing contaminants, including Fe, from the powder material; reducing oxygen content of the powder material to below a predetermined level to form a purified powder material; and removing particles greater than a predetermined size from the purified powder material. The purified powder material may be utilized for forming deposition sources, e.g., sputtering targets.
    Type: Application
    Filed: October 29, 2007
    Publication date: April 30, 2009
    Applicant: HERAEUS INC.
    Inventors: Wuwen Yi, William Heckman, Bernd Kunkel, Carl Derrington, Patrick Griffin
  • Publication number: 20090092517
    Abstract: A copper alloy extruded material is provided by extruding a copper alloy powder solidified billet and old grain boundaries remain in it.
    Type: Application
    Filed: July 25, 2006
    Publication date: April 9, 2009
    Inventors: Yoshiharu Kosaka, Masanori Okuyama, Akimichi Kojima, Katsuyoshi Kondoh
  • Patent number: 7442338
    Abstract: The present invention develops a manufacture method, via conventional liquid metallurgy, of finished and semi-finished metallic parts as casting, ingot, blooms and slabs in alloys base Fe, base Ni and base Co, microstructurally reinforced with complex molybdenum and titanium carbide particles, by means of their previous elaboration and latter addition to the molten alloy in the melting furnace. Then, when the alloy solidifies, they are inserted and distributed within the grains of the base metallic matrix, enhancing their mechanical properties and behavior at room as well as at high temperatures.
    Type: Grant
    Filed: May 13, 2004
    Date of Patent: October 28, 2008
    Assignee: Fundacion Inasmet
    Inventors: Ignacio Erauskin Lopetegui, Manuel Gutierrez Stampa, Inigo Agote Beloki, Manuel Orbegozo Ibarguren
  • Publication number: 20080199720
    Abstract: Porous metal foam structures and methods of making the same are described. Preferred methods include the steps of combining a liquid-extractable, pore-forming agent with a metal powder in the presence of a liquid in which the pore-forming agent is soluble, thereby forming a mixture, compacting the mixture to form a green body, and dissolving the pore-forming agent from the green body to produce a metal skeleton.
    Type: Application
    Filed: February 21, 2007
    Publication date: August 21, 2008
    Applicant: DePuy Products, Inc.
    Inventor: Hengda Liu
  • Publication number: 20080166255
    Abstract: A method of making Re and Re-based materials comprises steps of: providing a Re powder starting material or a Re powder starting material and at least one additional powder material; subjecting at least the Re powder to a first degassing treatment for reducing the oxygen content thereof; increasing the density of the degassed Re powder or a mixture of the degassed Re powder and the at least one additional powder material to form a green billet; subjecting the billet to a second degassing treatment to further reduce the oxygen content; and consolidating the billet to form a consolidated material with greater than about 95% of theoretical density and low oxygen content below about 200 ppm for Re and below about 500 ppm for Re-based materials formed from the mixture, excluding oxygen from non-metallic compounds and ceramics. Materials so produced are useful in the manufacture of deposition sources such as sputtering targets.
    Type: Application
    Filed: January 3, 2008
    Publication date: July 10, 2008
    Applicant: HERAEUS INC.
    Inventors: Fenglin YANG, Carl Derrington, Bernd Kunkel
  • Publication number: 20080102301
    Abstract: In a first embodiment the invention relates to a process for producing a dispersoid-strengthened material, comprising the steps of: (i) providing metal particles, wherein the metal is selected from platinum group metals, gold, silver, nickel and copper, as well as alloys thereof; (ii) mixing the metal particles with a precursor compound of the dispersoid and solvent; (iii) removing the solvent, so as to obtain metal particles provided with precursor compound; and (iv) compacting the metal particles provided with precursor compound in order to obtain the dispersoid-strengthened material, wherein the precursor compound is converted into the dispersoid during the compacting operation.
    Type: Application
    Filed: August 24, 2005
    Publication date: May 1, 2008
    Applicant: UMICORE AG & CO. KG
    Inventors: Michael Oechsle, Stefan Zeuner
  • Patent number: 7261759
    Abstract: A powder metal mixture comprises a lubricant powder conventionally used to produce powder metal parts in combination with a modified lubricant. A lubricant conventionally used to compact and sinter a chosen powder metal mixture is modified by adding to it starch particles smaller than the average metal particle, and optionally, micronized cellulose fibers in so small an amount that the modified lubricant is present in an amount less than 2% by weight of the mixture. The Hall apparent density and the Hall flow rate of a powder metal mixture made with the modified lubricant of starch or (starch+fibers) remains within the ranges deemed desirable for production of compacted powder metal parts. Using the modified lubricant in lieu of the conventional lubricant increases green strength of a part made by compacting the mixture and improves dimensional conformance.
    Type: Grant
    Filed: January 14, 2004
    Date of Patent: August 28, 2007
    Assignee: React-NTI, LLC
    Inventors: Bruce Anthony Tavares, Bart Jerome Nelson
  • Patent number: 7258812
    Abstract: A compound magnetic material having high heat resistance is provided. A fabrication method of a compound magnetic material includes the step of preparing mixed powder including an organic resin and compound magnetic particles. The long-period heat resistance temperature of the organic resin is at least 200° C. The containing ratio of the organic resin to the compound magnetic particles exceeds 0 mass % and not more than 0.2 mass %. The compound magnetic particle includes a metal magnetic particles, and a coat layer containing metal oxide, directly bound to the surface of the metal magnetic particle. The fabrication method of a compound magnetic material includes the steps of forming a compact by introducing mixed powder into a die having a lubricant applied to its surface and conducting warm-compacting, and applying heat treatment to the compact.
    Type: Grant
    Filed: October 28, 2002
    Date of Patent: August 21, 2007
    Assignees: Sumitomo Electric Sintered Alloy, Ltd., DENSO CORPORATION
    Inventors: Yoshiyuki Shimada, Hitoshi Oyama, Takao Nishioka
  • Patent number: 7160502
    Abstract: The present invention relates to a method for readily producing an anode for rechargeable batteries having conflicting properties in good balance, including the corrosion resistance and the activities such as the initial activity and the high rate discharge performance, and having excellent recyclability. The method includes the steps of mixing and molding anode materials containing an electrically conductive material and at least two kinds of AB5 type hydrogen storage alloys, wherein said alloys have substantially single phase structures and the same composition, wherein each of the alloys have an average crystal long axis diameter of 30 to 350 ?m, and wherein the alloys have different ratios (D1/D2) of the average crystal long axis diameter (D1) to the average short axis diameter (D2).
    Type: Grant
    Filed: April 9, 2002
    Date of Patent: January 9, 2007
    Assignee: Santoku Corporation
    Inventors: Kiyofumi Takamaru, Hideaki Ikeda, Koji Tatsumi
  • Publication number: 20040258552
    Abstract: A compound magnetic material having high heat resistance is provided. A fabrication method of a compound magnetic material includes the step of preparing mixed powder including an organic resin and compound magnetic particles. The long-period heat resistance temperature of the organic resin is at least 200° C. The containing ratio of the organic resin to the compound magnetic particles exceeds 0 mass % and not more than 0.2 mass %. The compound magnetic particle includes a metal magnetic particles, and a coat layer containing metal oxide, directly bound to the surface of the metal magnetic particle. The fabrication method of a compound magnetic material includes the steps of forming a compact by introducing mixed powder into a die having a lubricant applied to its surface and conducting warm-compacting, and applying heat treatment to the compact.
    Type: Application
    Filed: March 17, 2004
    Publication date: December 23, 2004
    Inventors: Yoshiyuki Shimada, Hitoshi Oyama, Takao Nishioka
  • Patent number: 6451251
    Abstract: Disclosed is a method for manufacturing a billet using aqueous salt solutions. The method for manufacturing a billet using aqueous salt solutions, comprising the following steps of: infiltrating aqueous salt solutions into metal powders or cut metal wires by adding the solutions to metal powders or cut metal wires filled in a cylindrical container, to obtain a mixture of aqueous salt solutions infiltrated into the metal powders or metal wires; evaporating water in aqueous salt solutions by heating said container containing the mixture, to obtain a dried mixture; and separating said dried mixture of metal powders or metal wires and salts from the container, to obtain a billet.
    Type: Grant
    Filed: June 12, 2001
    Date of Patent: September 17, 2002
    Assignee: Future Metal Co., Ltd.
    Inventors: Dong Yik Kim, Sung Kyun Kim
  • Patent number: 6248150
    Abstract: A method of producing a high-density article is presented comprising selecting one or more primary tungsten-containing constituents with densities greater than 10.0 g/cc and one or more secondary constituents with densities less than 10.0 g/cc, co-milling the mixture of constituents in a high-energy mill to obtain mechanical alloying effects, then processing the resulting powder product by conventional powder metallurgy to produce an article with bulk density greater than 9.0 g/cc.
    Type: Grant
    Filed: July 20, 1999
    Date of Patent: June 19, 2001
    Inventor: Darryl Dean Amick
  • Patent number: 6238614
    Abstract: The present invention provides a method, which infiltrates super-heated material between preheated powder particles and therefore minimizes heat deformation and increases measurement accuracy. A rapid prototyping apparatus in accordance with the present invention comprises powder material spreading means 10, dispensing infiltration material means 20, laser beam scanning means 30, and control means. The powder material spreading means spread out powders 61 on the surface of platform 52 uniformly while moving along the X axis. The powders are the main material of desired products. The dispensing infiltration material means dispense infiltration materials 63 while moving along three axes and the super-heated infiltration materials 64 by laser beam 43 are infiltrated between the powders selectively. The laser beam scanning means preheat the powders by laser beam 42 within the melting point of the powders and super-heat the infiltration material by laser beam 43.
    Type: Grant
    Filed: August 13, 1999
    Date of Patent: May 29, 2001
    Assignee: Korea Advanced Institute Science and Technology
    Inventors: Dong Yol Yang, Hyon Kee Sohn
  • Patent number: 6136061
    Abstract: The present invention provides for nanostructured metal compacts exhibiting a preferred grain orientation formed from nanosize metal particles, preferably having anisometric morphology. The compact may comprise a single-phase metal powder, that is, a metal powder comprised of a single element, or may be an alloy, or the metal powder may be admixed with another component thereby resulting in a compact exhibiting heterogenous properties. The metal particles are fabricated or compacted, as by a powder metallurgical process, utlizing a relatively high pressure sufficient to form a compact, object, body, article, product or the like, with desired integrity and desity. The particles tend to become oriented with their largest dimension perpendicular to the direction of the applied force. Compaction occurs at about ambient temperature, but may be at subambient or elevated temperatures provided this temperature variation is not deleterious to the grain structure of the compact.
    Type: Grant
    Filed: December 1, 1995
    Date of Patent: October 24, 2000
    Inventor: Charles P. Gibson
  • Patent number: 6074453
    Abstract: A method of making hydrogen storage powder resistant to fracture in service involves forming a melt having the appropriate composition for the hydrogen storage material, such, for example, LaNi.sub.5 and other AB.sub.5 type materials and AB.sub.5+x materials, where x is from about -2.5 to about +2.5, including x=0, and the melt is gas atomized under conditions of melt temperature and atomizing gas pressure to form generally spherical powder particles. The hydrogen storage powder exhibits improved chemcial homogeneity as a result of rapid solidfication from the melt and small particle size that is more resistant to microcracking during hydrogen absorption/desorption cycling. A hydrogen storage component, such as an electrode for a battery or electrochemical fuel cell, made from the gas atomized hydrogen storage material is resistant to hydrogen degradation upon hydrogen absorption/desorption that occurs for example, during charging/discharging of a battery.
    Type: Grant
    Filed: October 28, 1997
    Date of Patent: June 13, 2000
    Assignees: Iowa State University Research Foundation, Inc., California Institute of Technology
    Inventors: Iver E. Anderson, Timothy W. Ellis, Vitalij K. Pecharsky, Jason Ting, Robert Terpstra, Robert C. Bowman, Charles K. Witham, Brent T. Fultz, Ratnakumar V. Bugga
  • Patent number: 6042781
    Abstract: A process for consolidating powder, particulates, foils or sheets of metal coated composites, elemental metallic or metallic alloy or intermetallic compounds into net shapes having increased green strength at or near ambient temperature comprises treating the material with an aqueous activation solution. The aqueous activation solution is selected from dilute acids, reducing agents, molten salt electrolytes and mixtures thereof. Pressure is used to consolidate the treated powders, particulates, foils or sheets into a net shape at or near ambient temperature.
    Type: Grant
    Filed: December 10, 1996
    Date of Patent: March 28, 2000
    Assignee: Materials Innovation, Inc.
    Inventors: David S. Lashmore, Glenn L. Beane, Lev Deresh
  • Patent number: 5628047
    Abstract: A method of manufacturing a radially oriented magnet comprises disposing magnetic particles in a mold comprised of an insulating material, applying a pulsed magnetic field to the magnetic particles using a pair of pulse coils to impart a radial direction of magnetization to the magnetic particles, and press-forming the magnetic particles. The effective amount of magnetic flux which is applied to the magnetic particles can be effectively increased by introducing a pair of conducting rings between the pair of pulse coils for generating an eddy current effect between the pair of pulse coils to control the magnetic flux of the pulsed magnetic field. Such a method enables the manufacture of a downsized radially oriented magnet having a high degree of orientation.
    Type: Grant
    Filed: March 10, 1994
    Date of Patent: May 6, 1997
    Assignee: Seiko Instruments Inc.
    Inventor: Hidetoshi Hiroyoshi
  • Patent number: 5561832
    Abstract: A tool steel powder added with a vanadium carbide powder by a milling process, and a method for manufacturing parts therewith are disclosed. Particularly, a method for adding a vanadium carbide (VC) powder to a tool steel powder by a ball milling or an attrition milling, and a method for manufacturing a part by using the milled tool steel powder are disclosed. The method for manufacturing a vanadium carbide added tool steel powder and for manufacturing parts using the powder, includes the steps of: mixing a tool steel powder with vanadium carbide powder in an amount of 5.about.15 wt %; ball-milling the mixture powder under wet atmosphere; carrying out an annealing in a vacuum; carrying out a cold die compaction or cold isostatic pressing to near net dimension and carrying out a vacuum sintering and then a hot isotropic pressing without canning.
    Type: Grant
    Filed: June 29, 1995
    Date of Patent: October 1, 1996
    Assignee: Korea Institute of Machinery & Metals
    Inventors: Chung Hyung-Sik, Bae Jong-Su, Kim Young-Jin
  • Patent number: 5538684
    Abstract: The present invention provides lubricant compositions for the powder metallurgical field. The lubricant compositions contain a solid phase lubricant such as graphite, molybdenum disulfide, and polytetrafluoroethylene in combination with a liquid phase lubricant that is a binder for the solid phase lubricant. The binder can be chosen from various classes of compounds including polyethylene glycols, polyethylene glycol esters, partial esters of C.sub.3-6 polyhydric alcohols, polyvinyl esters, and polyvinyl pyrrolidones. The binder is solubilized in an organic solvent.
    Type: Grant
    Filed: June 6, 1995
    Date of Patent: July 23, 1996
    Assignee: Hoeganaes Corporation
    Inventors: Sydney Luk, Ann Lawrence
  • Patent number: 5529747
    Abstract: A formable composite magnetic flux concentrator material is composed of about 65% to 90% ferromagnetic material, such as iron powder, and about 35% to 10% binder, the binder being a mixture of an epoxy and one or more catalysts. The concentrator material is provided in a formable state as a putty-like body which can be worked into any desired shape dictated by the configuration of the induction heating coil used in a particular application. In one form, the density of the concentrator material is increased by application of vibration, compression and vacuum to de-air the material and to reduce voids therein. In another form, the iron powder comprises spherical-shaped particles and non-spherical shaped powders chosen in a ratio to maximize the density of material available.
    Type: Grant
    Filed: December 7, 1994
    Date of Patent: June 25, 1996
    Assignee: Learflux, Inc.
    Inventor: Thomas J. Learman
  • Patent number: 5505903
    Abstract: In the manufacture of cold-moulded briquettes from iron-containing waste metallurgical material mixed with a binder, in order to obtain high-strength briquettes and almost complete reducibility, magnetite waste metallurgical material such as scale (1) is mixed with haematite fine material (5) to form a layer (10) of haematite line materials (5) enveloping the individual magnetite particles (9), after which the binder is added to the mixture (FIG. 1).
    Type: Grant
    Filed: June 21, 1994
    Date of Patent: April 9, 1996
    Assignee: Voest-Alpine Industrieanlagenbau GmbH
    Inventors: Gunter Schrey, Gero Tessmer, Karl Katzensteiner, Klaus Kopper
  • Patent number: 5468446
    Abstract: The pelletisation or granulation of a material or mixture of materials the or at least one of which is reactive in a liquid to produce a gas is improved by treating the reactive material prior to final compaction to form a coating thereon of a substance which is less soluble in the liquid than the reactive material. The preferred reactive material is calcium hydride and the preferred coating is calcium carbonate with or without calcium hydroxide.
    Type: Grant
    Filed: February 28, 1994
    Date of Patent: November 21, 1995
    Assignees: British Aerospace PLC, BAeSEMA Ltd.
    Inventors: Peter C. Morgan, Alan D. Hart, Philip D. Morgans
  • Patent number: 5458847
    Abstract: A electroless plating method of an Ni--Al intermetallic compound includes steps of a) providing a reducing solution containing a reducing agent and reducing nickel ions, b) adding a proper amount of aluminum powder to the reducing solution, and c) permitting the reducing agent to reduce the reducing nickel ions to be deposited on the aluminum powder. Such electroless plating method permits the Ni--Al compound to be produced inexpensively/efficiently/fastly.
    Type: Grant
    Filed: September 22, 1993
    Date of Patent: October 17, 1995
    Assignee: National Science Council
    Inventor: Chen-Ti Hu
  • Patent number: 5447682
    Abstract: According to the method of making a magnetic coating material, 100 parts by weight of a magnetic metal powder, 1 to 10 parts by weight of fatty acid, 1 to 5 parts by weight of a dispersing agent, and a solvent are combined in the absence of a binding agent, wherein the solvent is present in sufficient amount to yield an admixture having a solids concentration of the magnetic metal powder in the range from 65 to 70 percent. The admixture is kneaded using a pressure kneader. The kneaded admixture is then blended with a binding agent to provide the magnetic coating material.
    Type: Grant
    Filed: June 24, 1993
    Date of Patent: September 5, 1995
    Assignee: Minnesota Mining and Manufacturing Company
    Inventor: Yusuki Saito
  • Patent number: 5407633
    Abstract: Method of manufacturing a dispenser cathode, in which method tungsten and a scandium-containing material are mechanically alloyed and the product thus formed is pressed into a cathode body. The cathode body is further provided with a barium-containing component. In the mechanical alloying process the tungsten is highly deformed and the scandium-containing material is mixed with the tungsten so as to be very finely distributed therein, so that an improved dispensation of scandium and hence an improved recovery after ion bombardment of the final cathode is attained.
    Type: Grant
    Filed: March 15, 1994
    Date of Patent: April 18, 1995
    Assignee: U.S. Philips Corporation
    Inventors: Jan Hasker, Robert H. Kane, Paul D. Goodell, Jacobus A. J. M. Deckers
  • Patent number: 5342575
    Abstract: Billets are produced from powdery alloys by a process which comprises densely packing in a can a powdery metal or alloy easy of plastic working and a powdery alloy difficult of plastic working in that order, sealing hermetically the can and thereafter degassing the same; or a process which comprises densely packing a powdery alloy difficult of plastic working in a can and, then, densely packing a powdery metal or powdery alloy easy of plastic working in the can to make the powdery metal or alloy into a lid of the can, wherein the powdery alloy easy of plastic working is coarse powder, while the powdery alloy difficult of plastic working is fine powder, and the powdery alloy is a rapidly solidified powdery alloy comprising an Al-base, Mg-base, Ni-base, Ti-base or Fe-base alloy.
    Type: Grant
    Filed: July 20, 1993
    Date of Patent: August 30, 1994
    Assignee: Yoshida Kogyo K.K.
    Inventor: Yoshitaka Nagai
  • Patent number: 5306462
    Abstract: A method of making a tantalum capacitor of improved specific capacitance (and volumetric efficiency) is described. Short tantalum fibers are precipitated out of a carrier liquid to form a felt, or tumbled to form fiber containing particles, and in either case subsequently bonded so as to form a felt or particles containing the fibers in random orientation in substantially non-aligned array. These particles or felt are heated to bond the fibers together, purify and (optionally) cylindricalize them. The felt or particles can be processed in conventional fashion thereafter to form the capacitor. Cylindricalized fibers and pellets of increased surface area are also described.
    Type: Grant
    Filed: July 31, 1992
    Date of Patent: April 26, 1994
    Assignee: Cabot Corporation
    Inventor: James A. Fife
  • Patent number: 5080859
    Abstract: A process for hardening sponge refractory metal and making it more susceptible to crushing by the addition of oxygen and/or nitrogen gas to either the reduction stage of the production of the metal from a tetrachloride thereof with magnesium, or to the treatment of a regulus of such metal following vacuum distillation thereof.
    Type: Grant
    Filed: June 1, 1990
    Date of Patent: January 14, 1992
    Assignee: Westinghouse Electric Corp.
    Inventors: Hani A. M. Abodishish, Randall W. Wahlquist
  • Patent number: 5059387
    Abstract: Shaped parts are formed from a powder having the desired chemistry of the finished part by mixing the powder with a thermosetting condensation resin that acts as a binder. The resin may be partially catalyzed, or additives or surfactants added to improve rheology, mixing properties, or processing time. Upon heating, the inherently low viscosity mixture will solidify without pressure being applied to it. A rigid form is produced which is capable of being ejected from a mold. Pre-sintered shapes or parts are made by injection molding, by using semi-permanent tooling, or by prototyping. Binder removal is accomplished by thermal means and without a separate debinding step, despite the known heat resistance of thermosetting resins. Removal is due to the film forming characteristic of the binder leaving open the part's pores, by providing oxidizing conditions within the part's pores as the part is heated, and by insuring that the evolving resin vapor diffuses through the pores by heating the part in a vacuum.
    Type: Grant
    Filed: June 2, 1989
    Date of Patent: October 22, 1991
    Assignee: Megamet Industries
    Inventor: Gregory M. Brasel
  • Patent number: 5033939
    Abstract: Shaped parts are formed from a powder having the desired chemistry of the finished part by mixing the powder with a thermosetting condensation resin that acts as a binder. The resin may be partially catalyzed, or additives or surfactants added to improve rheology, mixing properties, or processing time. Upon heating, the inherently low viscosity mixture will solidify without pressure being applied to it. A rigid form is produced which is capable of being ejected from a mold. Pre-sintered shapes or parts are made by injection molding, by using semi-permanent tooling, or by prototyping. Binder removal is accomplished by thermal means and without a separate debinding step, despite the known heat resistance of thermosetting resins. Removal is due to the film forming characteristic of the binder leaving open the part's pores, by providing oxidizing conditions within the part's pores as the part is heated, and by insuring that the evolving resin vapor diffuses through the pores by heating the part in a vacuum.
    Type: Grant
    Filed: October 29, 1990
    Date of Patent: July 23, 1991
    Assignee: Megamet Industries
    Inventor: Gregory M. Brasel
  • Patent number: 4976917
    Abstract: Quench-solidifed Al-Si alloy powder which contains more than 12 wt % Si is preformed, and the preforming is compression-molded into an aluminum alloy part. The aluminum alloy part is repeatedly subjected to a heating-and-cooling cycle of heating the aluminum alloy part to a temperature between 440.degree. C. and 500.degree. C. and cooling it to a temperature not higher than 380.degree. C.
    Type: Grant
    Filed: May 2, 1990
    Date of Patent: December 11, 1990
    Assignee: Mazda Motor Corporation
    Inventor: Makoto Fujita
  • Patent number: 4933025
    Abstract: A method for treating rare earth permanent magnetic material is disclosed. The treatment includes soaking ribbon rare earth permanent magnetic material consisting essentially of grains of the tetragonal crystal phase RE.sub.2 TM.sub.14 B where RE is neodymium and/or praseodymium or mixtures thereof with other rare earth elements and TM is iron or mixtures of iron and cobalt, cobalt in a soaking solution of either distilled water or phosphoric acid and manganese phosphate solution, draining off the soaking solution, rinsing with distilled water while agitating to separate and remove fine powdered magnetic material, and washing and drying the remaining powder or ribbons. The treated material is taken to substantial dryness before the material is incorporated into a permanent magnet.
    Type: Grant
    Filed: October 2, 1989
    Date of Patent: June 12, 1990
    Assignee: General Motors Corporation
    Inventors: Erwin A. Alson, Thomas H. VanSteenkiste
  • Patent number: 4931252
    Abstract: A process for reducing disparities of mechanical properties in tungsten-nickel-iron alloys containing in % by weight 85 to 99% of tunsten, 1 to 10% of iron, the alloys being obtained from tungsten, nickel and iron powders which have the same or different grain diameter, shape and size distribution, which entails simultaneously adding an effective amount of each of cobalt and manganese powders to tungsten powder or to a mixture of tungsten, nickel and iron powders.
    Type: Grant
    Filed: May 27, 1988
    Date of Patent: June 5, 1990
    Assignee: Cime Bocuze
    Inventors: Laurent Brunisholz, Guy Nicolas
  • Patent number: 4909840
    Abstract: A process for the production of a secondary powder composition having a nanocrystalline structure and being comprised of binary or quasi-binary substances composed of at least one of the elements Y, Ti, Zr, Hf, Nb, Mo, Ta and W and at least one of the elements V, Cr, Mn, Fe, Co, Ni, Cu and Pd, optionally also containing further ingredients, such as Si, Ge, B and/or oxides, nitrides, borides, carbides, and their possible mixed crystals. The components are in powdered form and are mixed in elementary form or as pre-alloys and have particle sizes ranging from 2 to 250 .mu.m. The powder components are subjected to high mechanical forces in order to produce secondary powders having a nanocrystalline structure. The secondary powders obtained in this way can be processed into molded bodies according to known compression molding processes, but at a temperature below the recrystallization temperature.
    Type: Grant
    Filed: April 7, 1988
    Date of Patent: March 20, 1990
    Assignee: Fried. Krupp Gesellschaft mit beschrankter Haftung
    Inventor: Wolfgang Schlump
  • Patent number: 4832741
    Abstract: A green pressed article of high strength and of low relative density, formed from a heat-resistant aluminum alloy of the Al/Fe/X or Al/Cr/X type, where X is Ti, Ce, Zr, Hf, V, Nb, Cr, Mo or W, is produced by a powder-metallurgical process, wherein an alloy melt is atomized to form fine particles by means of an inert gas jet, with which 0.5 to 2% by volume of oxygen is admixed, and the powder produced in this manner is compacted. Nitrogen, argon or helium can be employed as inert gas. The green pressed article is preferably formed from a small proportion of coarser, non-spherical particles and a greater proportion of finer, spherical particles.
    Type: Grant
    Filed: May 6, 1988
    Date of Patent: May 23, 1989
    Assignee: BBC Brown Boveri AG
    Inventor: Malcolm J. Couper
  • Patent number: 4818482
    Abstract: A method for pickling and consolidating water atomized metallic powders to reduce surface oxides. The technique includes introducing the powder into an acid bath--preferably nitric acid and hydrofluoric acid, rinsing the powder, introducing the powder into an alkaline bath, rinsing the powder and then consolidating the powder into a workpiece. Alternatively, the powder can be additionally introduced into a second acid bath and/or placed into a finishing boric acid bath before consolidation.
    Type: Grant
    Filed: July 9, 1987
    Date of Patent: April 4, 1989
    Assignee: Inco Alloys International, Inc.
    Inventors: Jon M. Poole, Lindy J. Curtis