Abstract: A method is described for the total phosphine detection in cereal caryopses, comprising the steps of inserting a sample of cereal caryopses inside a container (1) equipped with hermetic closure (2); adding to the sample an aqueous solution of H2SO4 with a v/v concentration in the range of 5-20%, with obtainment of an aqueous dispersion, and hermetically closing the first container (1); subjecting the aqueous dispersion contained in the first container (1) to the action of microwaves for a time not greater than 3 minutes; drawing a predetermined volume of gas overlying the aqueous dispersion and detecting the phosphine possibly present by means of colorimetric and/or spectrophotometric methods, preferably by bringing it into contact with a predetermined volume of an aqueous solution of AgNO3 of known molarity, inside a second container (3) with hermetic closure and visually analysing the obtained color and/or spectrophotometrically measuring the absorbance at 400 nm of the aqueous solution.

Abstract: The present invention provides a hydrogen peroxide indicator and a peracetic acid indicator that include a substrate on which is disposed an indicator composition that includes at least one of a select group of colorants and a transition metal salt. As a result of exposure to hydrogen peroxide and/or peracetic acid, the colorants change color, and even become colorless, thereby providing an indication of the presence of hydrogen peroxide and/or peracetic acid.

Abstract: A sensing element in which a dye that changes in the light absorption characteristic of the visible region upon reaction with ozone gas is deposited in the pores of a porous material is prepared. A change in dye before and after exposing the sensing element to a measurement environment for a predetermined time is measured. The ozone gas amount in measurement target air is measured on the basis of the change in dye.

Abstract: An encapsulated sorbent tube includes a sampling sorbent tube having an open end and containing a sorbent material therein enclosed within an independent encapsulation element that has a body portion and an end portion. The body portion of the encapsulation element has an inner diameter greater than the outer diameter of the sampling sorbent tube sufficient to accommodate the sampling sorbent tube therein. The end portion of the encapsulation element is formed and defined by the longitudinal length of the encapsulation element in excess of the sampling sorbent tube, and includes a proximal frangible element and a distal closure seal, each being independent of and separated from the sampling sorbent tube.

Abstract: A pH sensitive indicator device comprises a body including at least a portion of a translucent or transparent gas permeable material and an acid base colour change or halochromic material in or associated with the gas permeable material. The halochromic material can be received in a recess within the body of a gas permeable material or incorporated into the body of a gas permeable material. The gas permeable material can comprise a silicone elastomer.

Abstract: A method of making an optochemical sensor, the method comprising: providing a reflective substrate having a major surface; affixing a detection layer comprising at least one intrinsically microporous polymer to at least a portion of the major surface; depositing a substantially continuous semi-reflective metallic layer on at least a portion of the detection layer, the semi-reflective metallic layer comprising palladium and having a network of fine irregular cracks therein; and heating the detection layer and semi-reflective metallic layer in the presence of molecular oxygen at a temperature sufficient to cause the cracks to widen. Sensors prepared according to method are also disclosed.

Abstract: An apparatus for identifying suspected materials, includes: an upper portion and a lower portion; one or more cylinders for containing reactive material; one or more activation handles for releasing the contents of the cylinders, wherein one or more activation handle is slidable along a respective slot in an upper cover portion of the apparatus; one or more piston associated respectively with the cylinders, and with the activation handles, respectively; one or more fixed needle affixed to a frame, wherein a respective tip of the needles is pointed towards a respective bottom stopper of a cylinder, and; reaction chamber affixed below the frame, capable of receiving a flowable agent from the needles.

Abstract: New methods of operating surface reactors, and such reactors, particularly spinning disk reactors, require that a first reactant is fed to a reactor surface (20) and forms a thin radially outward moving film (60) thereon in a reaction passage (42) formed between the reaction surface (20) and a parallel, closely spaced (less than 1 mm) retaining surface (40). The passage thickness is precisely controllable and the surfaces (20, 40) move relative to one another so that strong shear is applied to the material between them. A second reactant is fed to the surface (20) as a second thin film (65) that as it enters the first film (60), preferably perpendicularly, it is immediately merged therewith along a correspondingly very narrow interaction line (66) by the shear at a rate such as to break up molecular clusters in the films, so that their molecules can aggressively and completely interact by forced interdiffusion.

Abstract: A sampling device for analysis of a substance which is chosen from the group consisting of isocyanates, aminoisocyanates, amines, and isothiocyanates, and which is present in an air flow intended to pass through the sampling device is disclosed, as well as a method for the production of said sampling device, and a method for the analysis of said substance in the air flow.

Abstract: A Fabry-Perot cavity has a pair of partially transmissive, partially reflective, surfaces. A first of the surfaces is flexibly suspended adjacent and parallel to a second of the surfaces. A gap exists between the surfaces. A variable electrostatic potential permits this gap to be adjusted. A translucent chemical layer is disposed on the first surface. A photosensor is attached to the second surface. Light irradiates the photosensor through the chemical layer and the first and second surfaces wherein the light is also partially reflected between the surfaces. A sensing environment is provided wherein an agent undergoes a reaction with the chemical layer as well as an environment wherein the reaction does not occur. The output of the photosensor is measured to assess a change in spectrum and spectral intensity for each of the sensing environments. The gap between the surfaces as well as the light used are selected to provide an optimum photosensor output.

Abstract: An apparatus for measuring the concentration of a target substance includes a detection container, a pump, and an integral temperature indicator or integral temperature correction factor indicator. The detection container has or contains a detection material chemically reactive with the target substance to produce an observable indication upon exposure to the target substance and such that the concentration of the target substance detected is readable from the observable indication. The pump is engageable with the detection container and operable to draw a sample of a gaseous environment into the detection container, the drawn sample containing the target substance, such that the detection material is exposed to the target substance. The integral temperature correction factor indicator, is particularly adapted to illuminate or indicate the correction factor applicable to the concentration measurement at specific temperatures.

Abstract: The present invention provides ratiometric fluorescent pH sensors for non-invasive, continuous monitoring of pH in such applications as fermentation processes. The ratiometric fluorescent pH sensors comprise a fluorescent dye that exhibits a shift in excitation wavelength with a corresponding shift in pH in the local environment of said fluorescent dye. Ratiometric measurements of the emission intensities at dual excitation maxima correlate to pH. Also provided is a fluorescent dye 6-methacryloyl-8-hydroxy-1,3-pyrene disulfonic acid (MA-HPDS). Further provided are systems and methods to non-invasively and continuously monitor pH.

Abstract: There is disclosed a method of operating a calorimetric gas detector system that comprises a substrate (1) bearing a material (12) that can react with a target gas to produce a change in the wavelength of radiation absorbed or transmitted by the material (“colour-change material”). The method involves: a) applying onto a region (15) of the substrate that includes colour-change material a chemical of predetermined concentration that reacts directly or indirectly with the colour-change material to produce a change in the wavelength of the radiation absorbed or transmitted by the material; b) detecting the radiation absorbed or transmitted in said region (15) at a wavelength absorbed or transmitted by the reaction product of the colour change material with the chemical, and c) generating a signal in accordance with the amount of radiation detected at the second wavelength, said signal being dependent on the amount of colour-change material on the substrate.

Abstract: An apparatus, process, coating, and filter for the accurate measurement of total mercury concentration in flue gas. In a preferred aspect, the concentrations of both elemental and oxidized mercury are preserved by the apparatus for analysis. Accordingly, embodiments of the present apparatus and process can be used to determine regulatory compliance or for process control measurement.

Abstract: A sensing element in which a dye that changes in the light absorption characteristic of the visible region upon reaction with ozone gas is deposited in the pores of a porous material is prepared. A change in dye before and after exposing the sensing element to a measurement environment for a predetermined time is measured. The ozone gas amount in measurement target air is measured on the basis of the change in dye.

Abstract: The present disclosure relates to a carbon dioxide detector having a borosilicate substrate. It may also have a carbon dioxide responsive indicator solution disposed on the borosilicate substrate. The carbon dioxide detector may be part of a carbon dioxide detector system also including an air intake operably connected to the housing to allow air to reach the carbon dioxide detector. The carbon dioxide detector may include a borosilicate substrate and a carbon dioxide responsive indicator solution disposed on the borosilicate substrate. This detector may be part of a further system, such as a resuscitation system. The detector may be made by wetting a borosilicate substrate with a carbon dioxide responsive indicator solution and drying the indicator solution to immobilize it and form a dried carbon dioxide detector. It may be used to detect the concentration of carbon dioxide in an air sample by exposing the detector to the sample.

Abstract: The present disclosure relates to a carbon dioxide detector having a borosilicate substrate. It may also have a carbon dioxide responsive indicator solution disposed on the borosilicate substrate. The carbon dioxide detector may be part of a carbon dioxide detector system also including an air intake operably connected to the housing to allow air to reach the carbon dioxide detector. The carbon dioxide detector may include a borosilicate substrate and a carbon dioxide responsive indicator solution disposed on the borosilicate substrate. This detector may be part of a further system, such as a resuscitation system. The detector may be made by wetting a borosilicate substrate with a carbon dioxide responsive indicator solution and drying the indicator solution to immobilize it and form a dried carbon dioxide detector. It may be used to detect the concentration of carbon dioxide in an air sample by exposing the detector to the sample.

Abstract: An air/gas-driven tool with an integrated air/gas dryness indicator. The tool includes a housing that defines a cavity. An air/gas dryness detector is disposed in the cavity. An air/gas flow passage is situated to provide a stream of compressed air/gas to the dryness detector. A visual indicator is adapted to provide an indication of compressed air/gas dryness detected by the dryness detector. The tool can be constructed so that the air/gas dryness indicator is provided by way of a removable indicator cartridge containing a dryness-indicating material such as a color changing desiccant or moisture sensitive paper. The indicator cartridge can be sized and configured to be received in a cavity formed in a housing of the air/gas-driven tool, so as to be viewable through a view port formed in the tool. Alternatively, the indicator cartridge can be configured with its own view port and mounted on a surface of the tool while being partially received in the cavity.

Abstract: A method of determining bias in a measurement of a constituent concentration level in a sample gas is provided. The method comprises establishing a sample gas flow from an emission stream into a sample gas line of an emissions monitoring system. The method further comprises removing water from the sample gas flow and cooling the sample gas flow to a temperature below about 41° F. to produce a cooled, dried sample gas flow. The constituent concentration level is then determined for the cooled, dried sample gas flow. The method further comprises introducing a span gas having a known span gas constituent concentration level into the sample gas flow to form a combined sample and span gas flow, the span gas being introduced at a desired span gas flow rate. The method still further comprises removing water from the combined sample and span gas and cooling the combined sample and span gas to a temperature below about 41° F. to produce a cooled, dried, combined sample and span gas flow.

Abstract: A hand-held device detects the presence of a preselected substance in the breath. A deformable housing forms a test chamber for interacting an indicator reagent with the breath. An ampoule positioned inside the housing is ruptured by manual pressure through the walls of the housing. The contents of the ruptured ampoule are exposed to the breath introduced into the chamber. The presence of a substance in the breath causes the indicator reagent to undergo a visually ascertainable change. The ampoule is secured within the housing by a pair of filter plugs having inboard concavities to receive the rounded ends of the ampoule to center it within the housing, and plural detents prevent slippage of the filters. Additional embodiments lower the user's risk of being cut by glass shards, prevent reagent inhalation, enhance the visual aspects of the device, and physically indicate the presence of breath flowing through the device.

Abstract: A method for the quantitative determination of atmospheric hydroperoxyl radical comprising: (a) contacting a liquid phase atmospheric sample with a chemiluminescent compound which luminesces on contact with hydroperoxyl radical; (b) determining luminescence intensity from the liquid phase atmospheric sample; and (c) comparing said luminescence intensity from the liquid phase atmospheric sample to a standard luminescence intensity for hydroperoxyl radical. An apparatus for automating the method is also included.

Abstract: The present invention is a disposable sensor for use with a device that quantifies analytes in a gaseous sample. It comprises (i) a sensing element, (ii) a means for interfacing the disposable sensor with a gas analysis device, and (iii) a housing. When used with a device that can quantify the concentration of an analyte in a gas sample, the present invention facilitates the use of exhaled breath analysis as a clinical tool.

Abstract: A device for detecting sulfuryl fluoride, in which the gas specimen to be examined is subjected to pyrolysis with ensuing detection of a pyrolysis product, is to be improved for the sake of achieving a mobile, economical structure. To attain this object, in a preliminary tube (1) for pyrolysis, there is a chemical layer (5) of pyrophoric iron, and as an indicator system for the pyrolysis product, a test tube (2) for hydrogen fluoride is used.

Abstract: The present invention provides a hydrogen peroxide indicator and a peracetic acid indicator that include a substrate on which is disposed an indicator composition that includes at least one of a select group of colorants and a transition metal salt. As a result of exposure to hydrogen peroxide and/or peracetic acid, the colorants change color, and even become colorless, thereby providing an indication of the presence of hydrogen peroxide and/or peracetic acid.

Abstract: The invention disclosed herein relates generally to mailpieces and more particularly, a hazardous material detector for detecting hazardous material in a mail stream. The present invention is directed, in general to detector for collecting sample (s) of hazardous materials from a mail processing device. The mailpiece generally comprises an envelope comprising a front side and a back side; holes formed in at least one of the front side or the back side of the envelope; a hazardous material test strip for detecting the presence of hazardous material in contact with the test strip; whereby when hazardous materials are detected by the hazardous material test strip a physical change occurs to the hazardous material test strip and the physical change can be viewed through at least one hole formed in the at least one of the front side or the back side of the envelope. The detector helps to quickly determine whether hazardous materials are present in the mail stream.

Abstract: A metal co-ordinated complex in a medium, e.g. a palladium-fluorophore, may be used to detect food spoilage products by the release of a detectable component by preferential binding of the metal to, for example, sulphur compounds or amines. It can be easy to detect food spoilage in sealed packs.

Abstract: Water-based chemical indicator inks for ethylene oxide sterilization processes and methods for its use. The chemical indicator ink contains at least one pH indicator dye selected from the group consisting of Bromocresol green, Bromophenol blue, Methyl red, Ethyl orange, and combinations thereof. The pH indicator dye undergoes an irreversible color change when exposed to ethylene oxide vapor in the presence of low-temperature steam, but when exposed to other sterilization processes either does not undergo a color change or undergoes a color change that is different than is obtained when exposed to ethylene oxide.

Abstract: An apparatus for measuring the concentration of formaldehyde in an exhaust stream from turbines, internal combustion engines and the like, which apparatus includes a portable housing having a sample gas inlet through which a sample gas for analysis is introduced into the portable housing and an analysis system disposed in the portable housing suitable for analyzing the sample gas for the presence of formaldehyde in the sample gas.

Abstract: An integral multilayer analytical element for analysis of ammonia or ammonia-producing substance is provided, which comprises a thin liquid blocking layer having a comparative facility with a thicker liquid blocking layer and is stably fabricated on a common production line employed for different type of slides. In the integral multilayer analytical element for analysis of ammonia or ammonia-producing substance comprising a transparent support, an indicator layer containing an indicator which produces a detectable change by gaseous ammonia, a liquid blocking layer permitting a gaseous ammonia to pass through, a reagent layer containing an alkaline buffering agent and optionally a reagent capable of reacting with said ammonia-producing substance to produce ammonia, and a spreading layer, adhesively laminated in this order, the improvement which comprises that said liquid blocking layer is composed of at least two porous membranes.

Abstract: A food quality indicator device an indicator compound provided on a substrate. The indicator compound changes color due to the presence of volatile compounds, such as volatile bases, in spoiled food, even when the food is frozen. Alternatively, the indicator compound detects the presence of an unwanted amine-producing biological agent, such as bacteria or fungi. The indicator compound is typically contained within a polymeric matrix disposed on the substrate. Examples of suitable indicator compounds include halogenated azo dyes, sulfonated xanthene dyes, and sulfonated hydroxy-functional triphenylmethane dyes.

Abstract: Disclosed is an exhalation gaseous component gauge including, in a palm-sized casing having exhalation taking-in and taking-out slots made on its front and rear sides, a semiconductor gas sensor so placed that the air flowing from one's mouth may pass the sensor, a CPU responsive to the signal from the sensor for determining the quantity of the exhalation gaseous components, and a display for showing the so determined result. The palm-sized casing is so sized and configured as to permit one to have a look at the display while holding the gauge in hand to direct the air from the mouth to the exhalation taking-in slot. Also, disclosed is a cellular phone equipped with an exhalation gaseous component gauge.

Abstract: Apparatus and method for detecting presence of an analyte in ambient air. The apparatus comprising a valve for admitting ambient air, a line for conveying the air to a sensing element, a housing for isolating the environment around the sensing element, an inlet port for flowing the air tho the sensing element in a turbulent flow in a direction substantially perpendicularly to the sensing element, an outlet port for conveying the air from the sensing element, and a pump in communication with the outlet port for providing suction for drawing the air to the sensing element. The method includes the steps of drawing in ambient air that may contain an analyte, projecting the air at a sensing element in a turbulent flow by flowing the air at the sensing element, the sensing element having on its surface a chemoselective material that selectively interacts with the analyte, and detecting the interaction of the analyte with the sensing element.

Abstract: An acid test kit uses an indicator paper in a transparent tube which is easily and temporarily inserted in a Schrader-valve at a compressor suction inlet of a refrigeration system. The simplicity, yet sufficient accuracy, of the kit permits several different ways of holding the paper in the tube through a friction fit. One way is to sandwich the paper between a tapered holder which is folded to provide a nose for actuating the Schrader valve. Another way is to provide the paper on or over a cylindrical member. A method for using the test kit including allowing vapor refrigerant from the system to pass through the tube to the atmosphere.

Abstract: A smoke sensor and a carbon monoxide sensor are integrated into a common detector housing. The smoke sensor is coupled to a smoke detector control integrated circuit which generates a binary output signal indicative of the presence of smoke. This signal is coupled to a programmed microprocessor in the detector housing. The carbon monoxide sensor is also coupled to the microprocessor. Outputs from the two sensors are processed substantially independently. In the presence of smoke, the smoke alarm is generated by the microprocessor. In the presence of sufficient levels of carbon monoxide, in the absence of smoke, a carbon monoxide alarm will be generated.

Abstract: Method and apparatus for determining in a person's exhalation air the concentration of a specific substance in the blood by measuring the concentration of said substance and the concentration of water vapor in the exhalation air and utilizing a known relationship between these concentrations. When the method is applied the exhalation air is exhaled freely in a defined air volume having a predetermined composition, and said concentrations are measured in this air volume. The apparatus for working the method comprises a device (16) which defines a space for receiving the exhalation air, which has two mutually opposite openings through which the space communicates with the surrounding air, and means (18, 22, 23) for selective quantitative detection of said substance in the air in the defined space.

Abstract: The present invention provides an apparatus and method of reducing noise associated with biomolecular measurement systems. Sensor detection system noise characteristics in the presence of other sensor detection systems are determined and advantageously used to determine an arrangement of the individual sensor cells. The sensor cells are arranged on a substrate such that the system noise is determinable and can thus be filtered from the measurement signal.

Abstract: The present invention provides a hydrogen peroxide indicator that includes a substrate on which is disposed an indicator composition that includes at least one of a select group of colorants. As a result of contact with hydrogen peroxide, the colorants change color, and even become colorless, thereby providing an indication of the presence of hydrogen peroxide.

Abstract: A gas indicator, which can be used over a broad range of gas concentration from a low concentration gas to a high concentration gas, includes a substrate sheet and plural change-color layers formed from a gas sensor ink on said substrate. The plural change-color layers are formed parallel to each other in a stripe pattern. The gas sensor ink contains an anthraquinone dye having at least one of a primary amino group or a secondary amino group.

Abstract: The invention relates to a novel sensor wherein the micro titer plates or supports are fitted with wells receiving the specimens to ascertain oxygen content. The wells contain luminescent or fluorescent dyes (for instance platinum, palladium or ruthenium complexes with phenathroline, porphyrin or pyridine ligands) which are imbedded in the particles of a gas-permeable but water-impermeable matrix. The matrix is a polystyrene derivative or a polystyrene copolymer. The particles in turn are dispersed in a second, water-permeable matrix consisting of a hydrophilic polymer such as polyhydroxy methacrylate, polyvinyl alcohol or polyvinyl pyrrolidone.

Abstract: The rate of carbon dioxide release from a grain sample can be measured by placing the grain sample in a sealed container, and positioning a pH responsive color-change material in the container so that carbon dioxide released from the grain sample chemically reacts with a buffer incorporated into the color-change material. Carbon dioxide measurements can be used to measure actual and potential spoilage of the grain associated with fungal attack.

Abstract: There are provided a detector agent which is effectively discolored at a lower concentration for various halogen compounds and a method for detecting halogen compounds by use of said detector agent. A detector agent for halogen compounds, which contains curcumin or Bromocresol Green as a discoloring component, and said discoloring component is preferably supported on granular activated alumina.

Abstract: An apparatus for measuring the concentration of a target substance is provided. The apparatus includes a detection container, a pump, and an integral temperature indicator or integral temperature correction factor indicator. The detection container has or contains a detection material chemically reactive with the target substance to produce an observable indication upon exposure to the target substance and such that the concentration of the target substance detected is readable from the observable indication. The pump is engageable with the detection container and operable to draw a sample of a gaseous environment into the detection container, the drawn sample containing the target substance, such that the detection material is exposed to the target substance. As for the integral temperature correction factor indicator, it is particularly adapted to indicating the correction factor applicable to the concentration measurement at specific temperatures.

Abstract: Improved calorimetric analysis technology based on the analysis of reaction gas, is disclosed. In accordance with the inventive apparatus, a gas permeable medium bearing a suitable calorimetric reagent, is positioned so that gas exiting the apparatus passes through the gas permeable medium.

Abstract: An anodic double layer gasochromic sensor structure for optical detection of hydrogen in improved response time and with improved optical absorption real time constants, comprising: a glass substrate; a tungsten-doped nickel oxide layer coated on the glass substrate; and a palladium layer coated on the tungsten-doped nickel oxide layer.

Abstract: Disclosed herein are calorimetric sensor films comprising a reflective layer, polymeric detection layer, and semi-reflective layer. Also disclosed are devices comprising the colorimetric sensor films and methods of making the films and devices.

Abstract: A device for detecting gaseous and vaporous components of a gas mixture by means of channels 2, which are located next to each other on a support 201, are connected in parallel in terms of flow, and are exposed to the component to be detected along a flow axis 3. A scanning section 6 of a scanning device is provided which extends along one of the channels 2, for detecting the change in color of reaction zones in the channels 2. Multiple channel arrangements can also be analyzed in a simple manner with a scanning section evaluating individual channels. At least some of the channels 2 on the support 201 are directed such that an angle &agr; not equal to 0 is formed between the flow axis 3 and the scanning section 6, and the channels 2 are located in the covered area of the scanning section 6.

Abstract: A rapid method of determining the efficacy of a sterilization cycle, and an indicator adapted to perform such method, comprising subjecting to the sterilization cycle a source of active enzyme having activity which correlates with the viability of a microorganism commonly used to monitor sterilization, and incubating the enzyme source, following the completion of the sterilization cycle, with an effective amount of a substrate system capable of reacting with any residual active enzyme to produce a detectable enzyme-modified product.

Abstract: An optical sensor is provided for determining a physical and/or chemical parameter of a sample, having at least one optical transmitter and at least one optical receiver, and having a sensitive element which is arranged in a beam path between the transmitter and the receiver and is exposable to the sample, and which changes its absorption and/or its refractive index for electromagnetic radiation of a specific wavelength in response to a change in parameters of the sample, in particular, a gas-sensitive element, and possibly having an evaluation unit arranged downstream of the receiver. The transmitter and the receiver can be coupled to the sensitive element via at least one optical waveguide. Provision is made for the transmitter (12) and for the receiver (14) to be coupled to the sensitive element via at least one optical waveguide (26, 28).

Abstract: A membrane capable of sensing gaseous phase ammonia is provided. The membrane includes a hydrophobic membrane layer that has a microporous structure and a pH sensitive dye embedded within the microporous structure such that the membrane is capable of calorimetrically sensing a change in ammonia with a high degree of sensitivity and responsiveness as applied to, for example, a change in ammonia dissolved in a dialysis solution during dialysis therapy.

Abstract: A field-installable and removable moisture and/or acid test kit and method is used for a vapor compression system. A moisture and/or acid indicator is provided in the test kit which is installed at a single point location upstream or downstream of the system compressor in a region where the system working fluid is in a substantially vapor phase. The test kit can be connected to the system by a threaded connection or a quick disconnect fitting. The moisture/acid indicator in the test kit detects the presence of moisture and/or acid by a diffusion of moisture or acid to the indicator via diffusion. Some magnification is provided in the test kit because the lower transport rates from the vapor diffusion mechanism requires a smaller mass of indicator material than has been used in conventional flowing liquid systems.