Abstract: Removing of a casting core from a metal casting leaves at least one opening in a surface of the metal. The opening is filled with a sacrificial material. The metal and sacrificial material are machined at the opening. After the machining, a remainder of the sacrificial material is removed.

Abstract: A polymer assisted deposition process for deposition of metal nitride films and the like is presented. The process includes solutions of one or more metal precursor and soluble polymers having binding properties for the one or more metal precursor. After a coating operation, the resultant coating is heated at high temperatures under a suitable atmosphere to yield metal nitride films and the like. Such films can be conformal on a variety of substrates including non-planar substrates. In some instances, the films can be epitaxial in structure and can be of optical quality. The process can be organic solvent-free.

Abstract: A method of coating ultrahard abrasive particles having vitreophilic surfaces, or treated to render their surfaces vitreophilic, are coated with an oxide precursor material, which is then heat treated to dry and purify the coats. The heat treated, coated ultrahard abrasive particles are further treated to convert the coats to an oxide, nitride, carbide, oxynitride, oxycarbide, or carbonitride thereof, or an elemental form thereof, or a glass.

Abstract: A process for synthesizing particles of an oxide corresponding to a formula selected from: Li4Ti5O12; Li(4-?)Z?Ti5O12; and Li4Z?Ti(5-?)O12, said process including the steps of: a) preparing an intimately dispersed ternary mixture of TiOx—LiZY-carbon, wherein x is a number between 1 and 2, z is 1 or 2, Y is a radical chosen from the group consisting of CO3, OH, O and TiO3 or a mixture thereof, and the carbon is a carbon powder selected from the group consisting of natural or artificial graphite, carbon black, Shawinigan black, Ketjen black and cokes; b) heating the dispersion at a temperature of between 400 and 1,000° C.; and c) if appropriate, adding a source of at least one metal Z to the ternary mixture, wherein the operating conditions are chosen in such a way as to yield a conversion of the initial products respectively into Li4Ti5O12, Li(4-?)Z?Ti5O12, Li4Z?Ti(5-?)O12.

Abstract: A treated refractory material includes a sintered porous refractory material having one or more protective materials disposed within pores of the refractory material, wherein the protective material is selected from the group consisting of aluminum oxide, chromium oxide, silica, rare earth oxides, rare earth zirconates, titanium oxide, mullite, zirconium oxide, zirconium silicate, yttrium oxide, magnesium oxide, iron oxide, and blends thereof. Methods of preparing the treated refractory material are also provided. The treated refractory material provides protection from the penetration of slag and extends the service life of the refractory.

Abstract: Disclosed is a mica paper composite and a process for making the mica paper composite. Particularly disclosed is a process for chemically planarizing the surface of a mica composite. Articles comprising the mica paper composite are also disclosed.

Abstract: The invention relates to thin, hydrogen-permeable, sulfur-resistant membranes formed from multi-layers of palladium or palladium-alloy coatings on porous, ceramic or metal supports, methods of making these membranes, methods of repairing layers of these membranes and devices that incorporate these membranes.

Abstract: Certain example embodiments of this invention relate to the development of temperable UV blocking coatings having enhanced UV blocking efficiency and aesthetic appearance on stock sheets of glass substrates using large-scale wet coating manufacturing methods. A glass substrate is provided. A base coat is curtain coated on the glass substrate from a oxide precursor material including zinc, cerium, titanium, and silicon precursor materials. The base coat is cured. A top coat is roll coated, directly or indirectly, on the base coat, with the top coat being a sacrificial cross-linked organic polymer-based layer. The substrate is heat treated with the base coat and the top coat thereon. The base coat and the top coat are substantially uniform in thickness, and the heat treating removes substantially all of the top coat while causing substantially no cracking in the base coat.

Abstract: The present invention provides methods for making improved zeolite and crystalline silicoaluminophosphate (SAPO) membranes, in particular SAPO-34 membranes, on a porous support through improved removal of the organic structure-directing templating agent. A calcining step is performed in an oxygen free atmosphere, such as under a vacuum or inert gas, to remove the organic templating agent. By removing the templating agent in the absence of oxygen, the calcination step can remove a greater amount of the templating agent than comparable template removal steps conducted in the presence of oxygen and the calcination step can be conducted at significantly lower temperatures. The membranes of the present invention provide increased permeance while maintaining comparable selectivity for gas separations, particularly carbon dioxide (CO2) and methane (CH4) separations and separations at high temperatures.

Abstract: A method for forming an ordered array of nanocrystals where a hydrophobic precursor solution with a hydrophobic core material in an organic solvent is added to a solution of a surfactant in water, followed by removal of a least a portion of the organic solvent to form a micellar solution of nanocrystals. A precursor co-assembling material, generally water-soluble, that can co-assemble with individual micelles formed in the micellar solution of nanocrystals can be added to this micellar solution under specified reaction conditions (for example, pH conditions) to form an ordered-array mesophase material. For example, basic conditions are used to precipitate an ordered nanocrystal/silica array material in bulk form and acidic conditions are used to form an ordered nanocrystal/silica array material as a thin film.

Abstract: The present invention relates to a method for producing a material suitable for producing ceramic oxide coatings, comprising the following steps: (a) preparing at least one first compound of a metal cation, selected from the cations of manganese, cerium, gadolinium, and/or yttrium, having at least one organic anion or an anion comprising an organic part, (b) dissolving or suspending the compound(s) prepared according to (a) in a protic, hydrolytically active solvent, such that the compound(s) is (are) present in a completely dissolved or colloidally dispersed form, (c) heating the suspension or solution thus formed in a closed vessel to at least 80° C., and (d) expanding and cooling the suspension or solution thus formed. Using said method, amorphous macromolecules are obtained, comprising molecular or polycyclic complexes having a primary particle size of <1 nm and an agglomerate size of 5 to 120 nm, preferably 10 to 80 nm.

Abstract: Described are lithium iron phosphate cathode materials for lithium secondary batteries and methods of preparation thereof. Better cathode materials may be produced by two carbon processes. The first carbon process comprises mixing lithium compounds, iron compounds, phosphorous compounds and a first carbon additive, and heating the mixture to a first temperature. The second carbon process comprises adding a second carbon additive to the to the product of the first carbon process and heating the mixture to a second temperature. The cathode material so produced exhibits superior electrical properties.

Abstract: An insulating mat for an exhaust gas treatment device thermally stable to at least 900° C., wherein the insulating mat contains inorganic fibers uniformly coated with a metal oxide including at least one of aluminum oxide, titanium oxide, zirconium oxide, or mixtures thereof; wherein said fibers are uniformly coated with the metal oxide by precipitating metal hydroxide corresponding to the metal oxide on the fibers, followed by converting the precipitated metal hydroxide to the metal oxide. A method of increasing the thermal stability of inorganic fibers for use in an exhaust gas treatment device insulating mat including the inorganic fibers, including uniformly coating the fibers with a metal oxide of at least one of aluminum oxide, titanium oxide, zirconium oxide or mixtures thereof by a chemical precipitation process.

Abstract: Known techniques for forming nanoparticles require a multiple-step process to coat a surface with nanoparticles. The present invention provides a single-step process that requires the deposition of a substrate in a mixture of a solvent, ligands and organometallic precursors. The mixture containing the substrate is heated under pressure in a dihydrogen environment for a predetermined period of time, during which supercrystals of nanoparticles form on the substrate.

Abstract: This invention relates to organometallic precursor compounds represented by the formula (H)mM(R)n wherein M is a metal or metalloid, R is the same or different and is a substituted or unsubstituted, saturated or unsaturated, heterocyclic radical containing at least one nitrogen atom, m is from 0 to a value less than the oxidation state of M, n is from 1 to a value equal to the oxidation state of M, and m+n is a value equal to the oxidation state of M, a process for producing the organometallic precursor compounds, and a method for producing a film or coating from the organometallic precursor compounds.

Abstract: A method of preparing a lanthanide-doped nanoparticle sol-gel matrix film having a high signal to noise ratio is provided. The sol-gels are also provided. A method of preparing light emitting sol-gel films made with lanthanide doped nanoparticles, for the production of white light is also provided. The method comprises selecting lanthanides for the production of at least one of green, red and blue light when excited with near infrared light, preparing nanoparticles comprising the selected lanthanides, stabilizing the nanoparticles with ligands operative to stabilize the nanoparticles in an aqueous solution and selected to be substantially removed from the sol-gel matrix film during synthesis, incorporating the stabilized nanoparticles into a sol-gel matrix and heating to increase the signal to noise ratio of the luminescence by substantially removing the low molecular weight organic molecules. Additionally, light emitting sol-gel films made with lanthanide doped nanoparticles are provided.

Abstract: Disclosed is a method for producing regularly arranged nanowires from a nanowire-forming material on a substrate. Said method is characterized by the following steps: a) the material is introduced into a carrier liquid at a load remaining at least three orders of magnitude below the loading capacity of the carrier liquid; b) a guiding member is placed on the substrate; c) the substrate is heated to a temperature at which a thin film of the carrier liquid undergoes spinodal decrosslinking on the substrate; d) a film of the carrier liquid that is loaded with material is applied to the heated substrate in the surroundings of the guiding member, where a gradient of the average film thickness is obtained perpendicular to the contour of the guiding member; and e) the carrier liquid is evaporated such that the material is left along lines extending perpendicular to the gradient of the film thickness.

Abstract: The invention provides a method for the self-assembly of organometallics within a sacrificial amphiphilic template in order to produce uniform mesoporous carbon composites coated with the organometallic component.

Abstract: Liquid-based indium selenide and copper selenide precursors, including copper-organoselenides, particulate copper selenide suspensions, copper selenide ethylene diamine in liquid solvent, nanoparticulate indium selenide suspensions, and indium selenide ethylene diamine coordination compounds in solvent, are used to form crystalline copper-indium-selenide, and/or copper indium gallium selenide films (66) on substrates (52).

Abstract: A substrate is provided that has a metallic layer on a substrate surface of a substrate. A film made of a two dimensional (2-D) material, such as graphene, is deposited on a metallic surface of the metallic layer. The metallic layer is dewet and/or removed to provide the film on the substrate surface.

Abstract: Methods of manufacturing and coating glass including depositing an inorganic oxide on an exterior surface of the glass, and then applying an organofunctional silane to the glass over the inorganic oxide. The methods also may include applying an organic coating to the glass over the organofunctional silane, and curing the organic coating.

Abstract: An article including a substrate and a layer of a homogeneous metal-oxyfluoride intermediate film disposed on the substrate, the intermediate film containing a rare earth metal, an alkaline earth metal, and a transition metal. The intermediate film has a defect density less than 20 percent and, upon thermal treatment, is capable of converting to a homogeneous rare earth metal-alkaline earth metal-transition metal-oxide superconductor film with a stoichiometric thickness greater than 1 ?m and up to 5 ?m. Also disclosed is another article including a substrate and the homogeneous superconductor film with a stoichiometric thickness greater than 1 ?m and up to 5 ?m. Further, methods of making these two articles are described.

Abstract: A composite article includes a substrate and a protective layer disposed on the substrate. The protective layer has a silicon-aluminum-carbon-nitrogen solid solution composition and microstructure.

Abstract: A catalyst for selective hydrogenation of hydrocarbons is presented. The catalyst selectively hydrogenates acetylenes and diolefins to increase the monoolefins in a product stream. The catalyst includes a layered structure with an inert inner core and an outer layer bonded to the inner core, where the outer layer is a metal oxide and has at least two metals deposited on the outer layer.

Abstract: A method for fabricating crystalline surface structures (4) on a template (1). The method comprises the steps of providing a template (1) into a reaction environment, wherein one or more elements (3) required for the formation of the crystalline surface structure (4) are contained within the template (1); heating the template (1) inside the reaction environment to increase the mobility of the element (3) within the template (1), and to increase the surface diffusion length of the element (3) on the template-environment interface; and activating the template (1) by altering the conditions within the reaction environment, to make the mobile element (3) slowly migrate towards the template-environment interface and to make the element (3) organize on the surface of the template (1) as a crystalline structure (4).

Abstract: A method for forming well-aligned metallic nanowires includes: (a) providing a substrate formed with a crystal layer thereon; (b) disposing the substrate in such a manner that the crystal layer faces downwardly; (c) applying a metal salt solution, which contains metal ions therein, to the crystal layer on the substrate; and (d) subjecting the metal ions in the metal salt solution on the crystal of TiO2 layer to a reduction treatment, thereby resulting in reduced metal that grows downward toward earth's gravity.

Abstract: A glass-containing molding composition is prepared by incorporating glass powder into a thermoplastic resin at a glass load ratio of 40 to 70 percent by weight, in which the glass powder is composed of solid spherical glass particles which have an average particle size of 10 to 40 ?m and whose surfaces are totally covered with a silane compound and which exhibits reduction ratios of melt flow rate on a parabolic curve with the increase of glass load ratios and has a reduction ratio of melt flow rate of 3/4 to 1/4 within a glass load ratio in a range of 40 to 64 percent by weight.

Abstract: The invention relates to open-pore biocompatible surface layers for implants, which layers are arranged over virgin surfaces of the implants, wherein pores of the open-pore surface layers are connected to form coherent pore networks and the surface layers have a specific internal surface area of ?0.06 ?m/?m2, preferably ?0.035 ?m/?m2 and especially ?0.025 ?m/?m2, measured by image analysis as a 2D-boundary line per unit of surface area in a metallographic microsection at 100× magnification. The invention further relates to methods of producing such surface layers, to implants coated therewith and to possible uses of the surface layers.

Abstract: The present invention provides a coating liquid including organic metal complexes represented by Chemical Formula 1. R1-R8 in Chemical Formula 1 is one of the followings (1)-(4): (1) a group represented by CnH2n+1 (aforementioned n is an integral number equal to or larger than 0); (2) a group represented by COOR9 (aforementioned R9 is a group represented by CmH2m+1, and aforementioned m is an integral number equal to or larger than 0); (3) a halogen atom; and (4) CN or NO2.

Abstract: According to a method for forming a coating system on a turbine engine component substrate that comprises a nickel-based superalloy substrate having at least one refractory metal included therein, a nickel-based layer is formed on the substrate, the nickel-based layer comprising at least one active material selected from the group consisting of elemental silicon and a silicon compound. The at least one active material is then diffused into the substrate. An yttrium-modified platinum aluminide bond coating, or a MCrAlX bond coating, may be then formed over the active material-modified nickel-based layer.

Abstract: A method is disclosed for growing metal (including semiconductor metal) nanowires from a film deposited on a substrate. In an illustrative embodiment tin and silicon are co-deposited, such as by sputtering, on a silicon substrate at, for example, ambient temperature. The deposited tin and silicon do not mix and the film has a tin phase dispersed in a higher melting, lower coefficient of thermal expansion, silicon phase. Upon heating, the tin expands against the silicon and expels small tin wires from the upper surface of the film. Other metal or metal alloy wires may be formed in a like manner using a matrix material and substrate in film deposition that don't mix with the metal composition and, when heated, force the expanding metal to extrude from the film surface as small diameter wires.

Abstract: The present invention relates to a structural object coated with a superhydrophobic nanostructure composite, the structural object being obtained by densely coating a surface of a solid substrate having a desired shape with a nanostructure obtained by combining a polymer having a polyethyleneimine skeleton with silica on the nanometer order, and bonding a hydrophobic group to the surface of the nanostructure, and a process for producing the structural object. The present invention also relates to a structural object coated with a superhydrophobic nanostructure composite, the structural object being obtained by removing the polymer having the polyethyleneimine skeleton from the nanostructure and bonding a hydrophobic group to the surface of the residual nanostructure containing silica as a main constituent component, and a process for producing the structural object. Furthermore, the present invention provides a method of using the structural object as a container for transferring an aqueous solution.

Abstract: This invention relates to a process for making carbon coated graphitic anode powders for use in batteries including rechargeable lithium-ion batteries wherein the process includes a side product isotropic pitch for use as a precursor in other products and more preferably, as a coating material for other powder or particle products. The process includes the steps of solvent extraction of volatile materials from high volatile material green coke powder. When a desirable amount of the volatile materials have been extracted, the solvent strength is altered to cause some of the volatile materials to precipitate on the powder particles to coat the same. The coated and solvent-extracted particles are then separated from the solvent and oxidatively stabilized, then carbonized and preferably graphitized. The volatile materials remaining in the solvent are valuable and are recovered for use in other processes and other products.

Abstract: A centrifugal compressor comprises at least one stage suited to separate a liquid phase and a gas phase with the aid of at least one of a hydrophobic, super-hydrophobic, hydrophilic or super-hydrophilic surface layer, wherein the hydrophobic and/or super-hydrophobic surface layer is disposed on at least one of an inlet guide vane, impeller, return channel straight hub, or exiting hub bend; and the hydrophilic and/or super-hydrophilic surface is disposed on at least one of the impeller casing, diffuser casing, exiting casing bend, return channel straight hub, exiting hub bend, collection point, or drain.

Abstract: The invention relates to a dye composition comprising a dye, dye converter, binder, reducing agent, solvent and optionally basic agent. Further, the invention relates to a method for fabricating an oxygen indicator wherein a dye composition is applied over a substrate and reduced by heating, to an oxygen indicator fabricated by the method and to a package for detecting a leakage and/or variation in the oxygen content.

Abstract: A semiconductor wafer (10) is structured such that fine structures (3), such as membranes, bridges or tongues, with a thickness d<<D are formed, wherein D designates the thickness of the semiconductor wafer (10). Then particles of a desired material are applied. A temporal or spatial temperature gradient is generated in the semiconductor wafer (10), e.g. by progressive heating. In such a heating process the fine structures heat up more quickly and become hotter than the remaining wafer because they have a smaller heat capacity per area and cannot carry off heat as quickly. In this manner, the fine structures can be heated to a temperature that allows a sintering of the particles. For coating the semiconductor wafer (10) is brought into a reactor (11). A precursor compound of a metal is provided and fed to the reactor (11), where a reaction takes place during which the metal is transformed to a final compound and is deposited in the form of particles on the semiconductor wafer (10).

Abstract: Apparatuses and processes for maskless deposition of electronic and biological materials. The process is capable of direct deposition of features with linewidths varying from the micron range up to a fraction of a millimeter, and may be used to deposit features on substrates with damage thresholds near 100° C. Deposition and subsequent processing may be carried out under ambient conditions, eliminating the need for a vacuum atmosphere. The process may also be performed in an inert gas environment. Deposition of and subsequent laser post processing produces linewidths as low as 1 micron, with sub-micron edge definition. The apparatus nozzle has a large working distance—the orifice to substrate distance may be several millimeters—and direct write onto non-planar surfaces is possible.

Abstract: A metal pattern forming method includes the steps of: applying one of a metal salt solution and an acetylene compound solution onto the substrate, the acetylene compound solution containing an acetylene compound expressed by a general formula of: (R.

Abstract: Superconductor precursor solutions are disclosed. The precursor solutions contain, for example, a salt of a rare earth metal, a salt of an alkaline earth metal and a salt of a transition metal. The precursor solutions can optionally include a Lewis base. The precursor solutions can be processed relatively quickly to provide a relatively thick and good quality intermediate of a rare earth metal-alkaline earth metal-transition metal oxide.

Abstract: A composition of matter and a structure fabricated using the composition. The composition comprising: a resin; polymeric nano-particles dispersed in the resin, each of the polymeric nano-particle comprising a multi-arm core polymer and pendent polymers attached to the multi-arm core polymer, the multi-arm core polymer immiscible with the resin and the pendent polymers miscible with the resin; and a solvent, the solvent volatile at a first temperature, the resin cross-linkable at a second temperature, the polymeric nano-particle decomposable at a third temperature, the third temperature higher than the second temperature, the second temperature higher than the first temperature, wherein a thickness of a layer of the composition shrinks by less than about 3.5% between heating the layer from the second temperature to the third temperature.

Abstract: A method of producing a silica coating by forming a silica precursor formulation that is coated on a substrate as a continuous liquid phase. The silica precursor formulation is then cured in an ammoniacal atmosphere to produce a continuous, interconnected, nano-porous silica network.

Abstract: A method and composition are provided for coating honeycomb seals and, more specifically, to a method and slurry for applying an aluminide coating onto honeycomb seals. The method includes preparing a slurry of a powder containing a metallic aluminum alloy having a melting temperature higher than aluminum, an activator capable of forming a reactive halide vapor with the metallic aluminum, and a binder containing an organic polymer. The slurry is applied to surfaces of the honeycomb seal, which is then heated to remove or burn off the binder, vaporize and react the activator with the metallic aluminum to form the halide vapor, react the halide vapor at the substrate surfaces to deposit aluminum on the surfaces of the seal, and diffuse the deposited aluminum into the surfaces to form a diffusion aluminide coating.

Abstract: A method of manufacturing gel containing wire connectors with a silicone gel that remains in an unseparated state wherein the temperature of the gel precursors are elevated before being mixed and dispensed into the cavity of a wire connector where the mixed gel precursors are allowed to cool and cure without the necessity of additional heating of either the mixed gel precursors or the wire connector.

Abstract: The invention relates to the use of light-colored or transparent particulate semiconductor materials or particulate substrates that are coated with said semiconductor materials as a hardening and/or drying additive and/or for increasing the thermal conductivity of lacquer systems and printing colors.

Abstract: Coating precursor materials, turbomachinery components, and methods of manufacturing the components are provided. In an embodiment, by way of example only, a coating precursor material includes a solid film lubricant component and a bonding component comprising at least one eutectic mixture, said at least one eutectic mixture selected from a group consisting of barium fluoride/nickel fluoride, barium fluoride/cobalt fluoride, and barium fluoride/barium fluoride-boron oxide.

Abstract: A method, apparatus and material produced thereby in an amorphous or crystalline form having multiple elements with a uniform molecular distribution of elements at the molecular level.

Abstract: A structure comprising a layer of graphene supported on a substrate wherein the substrate is pre-selected to have a coefficient of thermal expansion that is either matched within about 10% of that of graphene or mis-matched, thereby inducing controlled stress in the graphene layer to control electrical and/or mechanical properties of devices fabricated in the graphene layer.

Abstract: The present invention is related to a method for producing an enamelled steel substrate, said method comprising the steps of: providing a steel substrate, applying to a surface of said steel substrate a solution comprising a solvent, a polymer precursor, and at least one metal or metal oxide, said metal or metal oxide being suitable for promoting the adhesion of an enamel layer to the surface of the steel substrate, curing said steel sheet, thereby removing said solvent, and forming an organic layer comprising said at least one metal or metal oxide, applying to said organic layer, an enamel layer, followed by a firing step, to obtain the enamelled steel substrate.

Abstract: A substrate coated with a coating solution for an anti-reflective film is placed on a heat treatment plate and is heated. Nitrogen gas flows near the periphery of the heat treatment plate into a heat treatment space. An exhaust outlet is formed in an upper central portion of an inner cover, and the inner cover has an inner wall surface configured in the form of a tapered surface. This produces a smooth flow of nitrogen gas along the tapered surface to smoothly discharge a sublimate produced from the coating solution together with the gas flow outwardly through the exhaust outlet. After the heating process for a predetermined period of time is completed, the cover moves upwardly, and support pins move upwardly to thrust up the substrate from the heat treatment plate, thereby spacing the substrate apart from the heat treatment plate. This gradually decreases the temperature of the substrate.

Abstract: A method for producing fine, coated metal particles comprising the steps of mixing Ti-containing powder except for Ti oxide powder with oxide powder of a metal M, an M oxide having a standard free energy of formation meeting the relation of ?GM-O>?GTiO2; and heat-treating the resultant mixed powder at a temperature of 650-900° C. in a non-oxidizing atmosphere, thereby reducing the oxide of the metal M with Ti to provide the resultant fine particles of the metal M with TiO2-based titanium oxide coating.