Removing Excess Coating Material Patents (Class 427/235)
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Publication number: 20120024790Abstract: The present invention provides sol-gel germania-coated chromatography separation columns with improved stability under extreme pHs and high temperatures. Also provided are methods of preparation and uses of the sol-gel germania-coated separation columns of the present invention.Type: ApplicationFiled: June 1, 2011Publication date: February 2, 2012Applicant: University of South FloridaInventors: Abdul Malik, Chengliang Jiang, Li Fang
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Patent number: 8105513Abstract: The present invention relates to a pipette tip which is fitted with a porous organic monolith which is doped with active particles. Due to a unique polymerization method, the extraction tips stay highly permeable which allows sample to pass through the monolithic bed. The extraction tip represents an ideal tool for solid phase extraction, especially for desalting, isolating and purifying biomolecules such as peptides and proteins.Type: GrantFiled: June 5, 2009Date of Patent: January 31, 2012Inventors: Alexander Bonn, Guenther Bonn, Christian Huck, Bernhard Maerk, Harald Sonderegger, Mathias Rainer, Douglas T. Gjerde
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Publication number: 20120009100Abstract: The present invention relates to a pipette tip (10), for aspirating and dispensing pipetting fluid, which extends along a pipette tip longitudinal axis (L), a first axial longitudinal end region (16) of the pipette tip (10), as a pipetting longitudinal end region (16), comprising a pipette opening (12), through which pipetting fluid can flow in the course of operation, and a second axial longitudinal end region (18) of the pipette tip (10), as a coupling longitudinal end region (18), which opposes the pipetting longitudinal end region (16) in the axial direction, comprising a coupling shape, for coupling, preferably releasable coupling, to a coupling counter-shape of a pipette device, the pipette tip (10) comprising an outer hydrophobic region (32) on the outside (30) thereof and an inner hydrophobic region (26) on the inside (28) thereof, each having a quadratic roughness in a range of 100 nm to 1000 nm, preferably of 150 nm to 750 nm and particularly preferably of 200 nm to 500 nm, and having a peak-to-peakType: ApplicationFiled: July 12, 2011Publication date: January 12, 2012Applicant: HAMILTON BONADUZ AGInventors: Vinzenz KIRSTE, Renato NAY, Rainer BECKBISSINGER
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Patent number: 8092863Abstract: The invention relates to methods for manufacturing lightweight building boards (1) starting from a workpiece (2) which comprises two thin-walled cover layers (4, 6) and at least one core layer (8) which is disposed between the cover layers (4, 6) and is made of a light filling material, the at least one core layer (8) possessing cavities and having a lower average density than the cover layers. The method comprises the following steps: forming in the workpiece (2) at least one groove (10) which extends through at least one first cover layer (4) and at least partly through the at least one core layer (8) and circumscribes at least a portion of a contour of the lightweight building board (1) to be manufactured; introducing a hardenable mass (12) into the at least one groove (10); at least partly hardening the hardenable mass (12); and making a separating cut along the at least one groove (10), so the at least partly hardened mass (12) is separated in the longitudinal direction of the groove.Type: GrantFiled: May 9, 2008Date of Patent: January 10, 2012Assignee: Homag Holzbearbeitungssysteme AGInventors: Johannes Schmid, Achim Gauss
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Patent number: 8084085Abstract: A method of manufacturing a microstructure includes filling a microchannel with a slurry including a sol-gel binder, removing a portion of the slurry from the microchannel such that a slurry layer is disposed on or between the plurality of microchannel walls, and heating the microstructure for a sufficient time and at a sufficient temperature to cure and bind the slurry layer to the microchannel walls.Type: GrantFiled: December 17, 2004Date of Patent: December 27, 2011Assignee: Corning IncorporatedInventor: Christophe Remy
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Publication number: 20110259519Abstract: A method of coating the inner surfaces of gas passages of a gas delivery system for a plasma process system such as a plasma etching system includes (a) flowing a fluidic precursor of a corrosion-resistant material through the gas passages and depositing a layer of the fluidic precursor to completely coat the inner surfaces of the gas passages; (b) removing excess fluidic precursor from the inner surfaces; (c) curing the deposited layer of the fluidic precursor to form a corrosion-resistant material coating.Type: ApplicationFiled: April 23, 2010Publication date: October 27, 2011Applicant: Lam Research CorporationInventors: Ian Kenworthy, Duane Outka, Fangli Hao, Leonard Sharpless, Yijun Du
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Method for masking cooling holes and device for using in a masking process for masking cooling holes
Patent number: 8021719Abstract: A method of masking cooling holes of a turbine component, in particular a turbine blade or vane, for a coating process is provided. The component includes an external surface to be coated, at least one internal cavity having an opening towards the outside of the component, and cooling holes extending from the at least one internal cavity to the external surface. The method comprises the steps of: filling the cooling holes with a masking material and hardening the masking material. The masking material, water, is used to fill in the cooling holes. The hardening is done by freezing the water to water ice. A method of coating an external surface of a turbine component and a device for use in a masking process for masking cooling holes in a turbine component are also provided.Type: GrantFiled: February 19, 2009Date of Patent: September 20, 2011Assignee: Siemens AktiengesellschaftInventor: Andreas Graichen -
Publication number: 20110101122Abstract: Provided is a multi-channel electrospray emitter. The emitter includes a plurality of separate or distinct capillaries, each capillary being one channel and terminating in a nozzle, from which the analyte is sprayed. The nozzles may be raised above a face of the electrospray emitter. The multi-channel electrospray emitter may comprise a microstructured fibre. In one embodiment, the microstructured fibre may be a photonic crystal fibre.Type: ApplicationFiled: September 21, 2010Publication date: May 5, 2011Inventors: Richard D. Oleschuk, Graham Gibson, Ramin Wright
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Publication number: 20110104427Abstract: A method for forming a glass substrate comprises the steps of forming a glass blank with opposing substantially planar surfaces and at least one edge, coating the glass blank in silica-alumina nanoparticles, the silica-alumina nanoparticles comprising an inner core of silica with an outer shell of alumina, annealing the coated glass blank to form a conformal coating of silica-alumina around the glass blank, and polishing the coated glass blank to remove the conformal coating of silica-alumina from the opposing substantially planar surfaces thereof.Type: ApplicationFiled: November 3, 2009Publication date: May 5, 2011Applicant: WD MEDIA, INC.Inventor: SHOJI SUZUKI
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Patent number: 7923060Abstract: There is disclosed a method of manufacturing a thin and uniform ceramic filter formed with less membrane formation times and having less defects. A ceramic sol whose average pore diameter after the sol itself has been formed into a membrane is larger than that of a ceramic separation membrane and is 10 nm or less is brought into contact with the surface of a ceramic separation membrane having an average pore diameter of 0.5 to 10 nm, and the ceramic separation membrane having the ceramic sol is dried and then fired to repair a defect portion of the ceramic separation membrane.Type: GrantFiled: September 6, 2007Date of Patent: April 12, 2011Assignee: NGK Insulators, Ltd.Inventors: Manabu Isomura, Tatsuya Hishiki, Ichiro Wada
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Publication number: 20110059241Abstract: A composition and method for inhibiting white rust formation on galvanized surfaces. The composition includes thiols, polymeric dithiocarbamates, and xanthates. The composition may be introduced onto the galvanized surface, especially in an industrial water system, using a variety of different methods or programs including integrating with current programs or developing a new program.Type: ApplicationFiled: November 12, 2010Publication date: March 10, 2011Inventor: Srikanth S. Kidambi
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Patent number: 7901735Abstract: A method for continuously coating the inside of a continuously extruded hollow profiled bar made of elastic material and a liquid wiper and a device for removing excess coating agent from the chambers of a hollow profiled member. A hollow profiled bar is directed through a stationary supply of a liquid coating agent on a bent, arc-shaped track, whereby inner walls of the hollow profiled bar are moistened with coating agent, and the hollow profiled bar is guided along a rising track directly after running through the coating agent supply. Excess coating agent is wiped off one or plural inner walls with the aid of liquid wipers mounted inside the hollow chambers, the hollow profiled bar being continuously moved relative to the liquid wipers. The liquid wipers include at least one magnet or magnetizable material and a wiping lip that touches the inner walls while being located downstream of the coating agent supply in a zone of a sloped track of the hollow profiled bar.Type: GrantFiled: December 24, 2004Date of Patent: March 8, 2011Assignee: Evonik Rohm GmbHInventors: Dieter Foerster, Juergen Krautter, Manfred Schneider
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Patent number: 7858149Abstract: Methods and systems for cleaning, coating and sealing leaks in existing pipes, in a single operation. A piping system can be cleaned in one pass by dry particulates forced and pulled by air throughout the piping system by a generator and a vacuum. Pipes can be protected from water corrosion, erosion and electrolysis, extending the life of pipes such as copper, steel, lead, brass, cast iron piping and composite materials. Coatings can be applied to pipes having diameters up to approximately 6?. Leak sealants of at least approximately 4 mils thick can cover insides of pipes, and can include novel mixtures of fillers and epoxy materials, and viscosity levels. A positive pressure can be maintained within the pipes during applications. Piping systems can be returned to service within approximately 96 hours.Type: GrantFiled: January 4, 2007Date of Patent: December 28, 2010Assignee: Pipe Restoration Technologies, LLCInventors: Larry Gillanders, Steve Williams, John Laborde
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Patent number: 7829142Abstract: Disclosed herein is a method for aluminiding an internal passage of a metal substrate comprising injecting a slurry composition that comprises a powder comprising aluminum, a binder selected from the group consisting of colloidal silica, an organic resin, and a combination thereof, into the internal passage; applying compressed air to the internal passage to facilitate distribution of the slurry composition throughout the internal passage; and, heat treating the slurry composition under conditions sufficient to remove volatile components from the composition, and to cause diffusion of aluminum into a surface of the internal passage.Type: GrantFiled: June 21, 2006Date of Patent: November 9, 2010Assignee: General Electric CompanyInventors: Lawrence Bernard Kool, Michael Howard Rucker
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Publication number: 20100269504Abstract: A fuel system for delivering fuel to an engine includes a fuel tank, a hot section in fluid communication with the fuel tank for delivering fuel for combustion by the engine, and a coating applied to at least a portion of the hot section for reducing fuel coking. The coating includes a fluorine functional group and a silane functional group.Type: ApplicationFiled: April 24, 2009Publication date: October 28, 2010Applicant: Hamilton Sunstrand CorporationInventors: Marc E. Gage, Haralambos Cordatos
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Publication number: 20100272890Abstract: A method for producing a ceramic honeycomb filter having predetermined plugs comprising immersing the end portions of a ceramic honeycomb structure having large numbers of flow paths, with its end surface covered with a mask provided with holes only at positions corresponding to the predetermined flow paths, in a plugging material slurry, so that the plugging material slurry is introduced into the end portions of the predetermined flow paths, and removing plugging material protrusions formed in the flow paths that should not be plugged.Type: ApplicationFiled: June 24, 2010Publication date: October 28, 2010Applicant: Hitachi Metals, Ltd.Inventors: Toyohide KUMAGAE, Shinya Tokumaru, Hirohisa Suwabe
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Publication number: 20100247401Abstract: Disclosed is a device for performing radiation assisted chemical processing including a fluid path, defined at least in part by a first surface of a wall transparent to radiation useful for performing radiation assisted chemical processing, and a gas discharge or plasma chamber arranged for producing the radiation, wherein the chamber is defined at least in part by a second surface of the transparent wall, opposite the first A related method of forming a photocatalytic reactor comprises among other steps the step of wash-coating the fluid path so as to deposit a photocatalytic material therein, wherein the step of wash-coating includes depositing, and not depositing or removing photocatalytic mate?al, respectively, on a first portion or from a second portion of the of non-circular cross section of the path, the second portion including at least some of the first surface of the wall of transparent materialType: ApplicationFiled: November 25, 2008Publication date: September 30, 2010Inventors: Philippe J. Barthe, Thierry Luc Alain Dannoux, Alexandre Michel Mayolet
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Publication number: 20100221537Abstract: A fiber structure for propagating one or more zero group-velocity modes is provided. The fiber structure includes a cladding arrangement comprising a photonic crystal having a complete bandgap at a specified index. A core is formed in a selective region of the cladding arrangement. The core allows the propagation of the one or more group-velocity modes.Type: ApplicationFiled: February 26, 2010Publication date: September 2, 2010Inventors: Ardavan Farjadpour, John D. Joanopoulos, Steven G. Johnson
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Publication number: 20100189895Abstract: In a method for coating the inner walls of pipes (11), and in a coating device suitable for coating, a combined heating and cooling device (19) having heating areas (21) and cooling areas (22) is used for the method. This device can be guided along the pipe (11) to be coated, wherein a fluid (16) containing the coating active agent is supplied to the interior of the pipe. The combined heating and cooling treatment for the pipe supports the process of coating formation. The cooling process is subject to a desired profile by the use of the cooling area (22) and is not determined by chance, in contrast to the cooling process in the prior art.Type: ApplicationFiled: June 13, 2008Publication date: July 29, 2010Inventors: Frank Arndt, Jens Dahl Jensen, Ursus Krüger, Gabriele Winkler
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Patent number: 7744948Abstract: An electroluminescence device includes a tubular first electrode, an electroluminescence layer formed on an inner surface of the first electrode, and a second electrode formed on an inner surface of the electroluminescence layer. A method for manufacturing the electroluminescence device includes: causing the inner surface of the first electrode to be lyophilic with respect to an electroluminescence layer forming liquid; conducting the electroluminescence layer forming liquid into and out of the inside of the first electrode, thereby forming a liquid film of the electroluminescence layer forming liquid on the inner surface of the first electrode, which inner surface is lyophilic with respect to the electroluminescence layer forming liquid; and forming the electroluminescence layer by drying the liquid film of the electroluminescence layer forming liquid formed on the inner surface of the first electrode.Type: GrantFiled: July 25, 2006Date of Patent: June 29, 2010Assignee: Seiko Epson CorporationInventor: Naoyuki Toyoda
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Patent number: 7740898Abstract: An electroluminescence device includes a tubular first electrode, an electroluminescence layer formed on an inner surface of the first electrode, and a second electrode formed on an inner surface of the electroluminescence layer. A method for manufacturing the electroluminescence device includes: conducting an electroluminescence layer forming liquid into and out of the inside of the first electrode, thereby forming a liquid film of the electroluminescence layer forming liquid on the inner surface of the first electrode; and forming the electroluminescence layer by drying the liquid film of the electroluminescence layer forming liquid formed on the inner surface of the first electrode. This facilitates modification of the size or the shape of the electroluminescence device and thus improves productivity for manufacturing the electroluminescence device.Type: GrantFiled: July 25, 2006Date of Patent: June 22, 2010Assignee: Seiko Epson CorporationInventor: Naoyuki Toyoda
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Publication number: 20100130109Abstract: A system and method for restoring water supply pipes in buildings is provided. Compressed air is blown through one end of a cold water supply pipe, such as a cold water riser, and elsewhere on the pipe the cold water supply pipe is connected to the hot water supply pipe by an air hose. Compressed air may alternatively be blown through one end of the hot water supply pipe. To clean the pipe, abrasive particles are introduced into the stream of compressed air upstream of the section of pipe to be cleaned. To line the pipe, an epoxy coating is introduced into the stream of compressed gas upstream of the section of pipe to be lined.Type: ApplicationFiled: November 26, 2008Publication date: May 27, 2010Applicant: RIKOS LTD.Inventor: Marc Leben
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Publication number: 20100124608Abstract: Disclosed is a coated substrate including a substrate coating applied to at least one substantially flat surface of the substrate, the coating including at least one of an axial concavity and a circumferential curvature, the substrate being configured for disposal parametrically about a moving component.Type: ApplicationFiled: September 29, 2006Publication date: May 20, 2010Applicant: GENERAL ELECTRIC COMPANYInventors: Curtis Alan Johnson, Yuk-Chiu Lau, Joshua Lee Margolies, Herbert Chidsey Roberts, III
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Publication number: 20100112208Abstract: A method is presented describing in situ preparation of the titania-based sol-gel PDMS coating and its immobilization on the inner surface of a fused silica microextraction capillary. Sol-gel titania-poly (dimethylsiloxane) (TiO2-PDMS) coating was developed for capillary microextraction (CME) to perform on-line preconcentration and HPLC analysis of trace impurities in aqueous samples. The sol-gel titania-based coatings demonstrated strong pH stability and enhanced extraction capability over other commercially available GC coatings. Extraction characteristics of a sol-gel titania-PDMS capillary remained practically unchanged after continuous rinsing with a 0.1 M NaOH solution (pH=13) for 12 hours.Type: ApplicationFiled: October 23, 2009Publication date: May 6, 2010Inventors: Abdul Malik, Tae-Young Kim
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Publication number: 20100112207Abstract: The present invention is directed to a process and apparatus for thermally spray coating the inside surface of a hydro-drive device, namely a Kort, so as to improve hydro-flow thrust and reduce the consumption of fuel for a vessel comprising the adapted Kort. The process of the present invention comprises thermally spraying a thermoplastic material in the area of the interior wall of the Kort that comes in close proximity to the propeller of the hydro-drive device. The closer the propeller comes to the interior wall of the Kort, the less friction and cavitations produced. Since friction and cavitations increases fuel consumption of the vessel, any reduction in the clearance between the wall of the Kort and the propeller tips directly reduces fuel consumption. At the same time, a reduction in clearance also increases the thrust of the hydro-drive device.Type: ApplicationFiled: November 3, 2008Publication date: May 6, 2010Inventor: Thomas Gardega
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Patent number: 7678416Abstract: In a method of coating a substrate, inner walls of flow channels of the substrate are coated with a slurry. A plurality of flow channels each opened at both end faces are formed in the substrate. The method includes a step of storing a predetermined amount of slurry in a slurry container in which the end of the substrate, where the flow channels of the substrate are opened, can be inserted under pressure into the slurry container. A step of inserting the substrate with the end of the substrate being downward in the slurry container and dipping the substrate under pressure to the slurry liquid surface, and a step of extending the slurry along the inner wall of the flow channels by blow-opening the respective flow channels in a state of up-turning the slurry container together with the substrate.Type: GrantFiled: December 5, 2005Date of Patent: March 16, 2010Assignee: Cataler CorporationInventors: Hiromasa Suzuki, Shingo Sakagami, Tomoyuki Goshima, Tamio Kosaka
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Publication number: 20100047845Abstract: The present application is directed to methods of improving cell culture vessel assays. In one aspect the application is directed to a method of reducing the curvature of the meniscus comprising applying a coating material to the interior wall of the vessel, wherein the coating material provides a receding contact angle of about 90 degrees with aqueous solutions and culture media. In another aspect, the application is directed to a method of labeling cells in a first solution by generating droplets of a second solution containing at least one cell-labelling agent and allowing the droplets of the second solution to contact the surface of the first solution.Type: ApplicationFiled: February 26, 2008Publication date: February 25, 2010Applicant: STEMCELL TECHNOLOGIES INC.Inventors: Steven Woodside, Jason Dowd, Gary Dossantos, Oliver Egeler
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Publication number: 20100004132Abstract: A method of conditioning a tubular clay material to enable its loading with an active, the method comprising the step of exposing the tubular clay material to a chemical agent in a manner such that the agent sorbs to a surface of the clay material that is internal of the tube, the chemical agent being selected such that, when the agent is sorbed to the clay material internal surface, the affinity of the tubular clay material for the active is altered.Type: ApplicationFiled: July 26, 2006Publication date: January 7, 2010Applicant: THE UNIVERSITY OF SYDNEYInventors: Cameron John Kepert, Malcolm Edward Roland Green, Sarah Jane Antill
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Patent number: 7608298Abstract: A method of manufacturing a ceramic porous membrane on inner wall surfaces of through holes of a porous base member. The through holes of the base member are arranged in a vertical direction, a ceramic sol liquid having a temperature difference of 50° C. or less between the sol liquid and the base member is supplied to the inner wall surface of the base member, the liquid supply is stopped when the sol liquid exceeds an upper end portion of the base member, and then the sol liquid is extracted from the bottom of the base member. After the sol liquid is completely extracted, a pressure difference is created so that a pressure on the side of an outer peripheral surface of the base member is lower than that on the side of the inner wall surface of the base member.Type: GrantFiled: September 21, 2007Date of Patent: October 27, 2009Assignee: NGK Insulators, Ltd.Inventor: Kei Tanaka
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Publication number: 20090208175Abstract: A hollow fiber has a hollow tube, a reflecting film formed on an inner wall of the hollow tube, and the reflecting film is a first metal film formed by baking a first metal nano particle solution including a first metal nano particle. The hollow fiber may have a transparent film on the first metal film. The transparent film is formed by baking or chemically reacting from a second metal nano particle included in a second metal nano particle solution.Type: ApplicationFiled: February 19, 2009Publication date: August 20, 2009Inventors: Akihito HONGO, Yoshinori Kurosawa, Masahiro Ohkawa, Hiroaki Takamiya
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Patent number: 7569283Abstract: An aluminizing composition includes an aluminum-based powder, an inert organic pyrolysable thickener, and a binder selected from the group consisting of colloidal silica, at least one organic resin, and combinations thereof. A method for aluminizing an internal passage of a metal substrate comprises injecting the organic-based aluminizing composition into the internal passage, heat treating the composition under conditions sufficient to remove volatile components from the composition, to cause diffusion of aluminum into surface regions of the internal passage, and to cause decomposition of at least some pyrolysable thickener particles, and burnishing excess material from the internal passage.Type: GrantFiled: January 3, 2007Date of Patent: August 4, 2009Assignee: General Electric CompanyInventor: Lawrence Bernard Kool
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Publication number: 20090191335Abstract: A method for continuously coating the inside of a continuously extruded hollow profiled bar made of elastic material and a liquid wiper and a device for removing excess coating agent from the chambers of a hollow profiled member. A hollow profiled bar is directed through a stationary supply of a liquid coating agent on a bent, arc-shaped track, whereby inner walls of the hollow profiled bar are moistened with coating agent, and the hollow profiled bar is guided along a rising track directly after running through the coating agent supply. Excess coating agent is wiped off one or plural inner walls with the aid of liquid wipers mounted inside the hollow chambers, the hollow profiled bar being continuously moved relative to the liquid wipers. The liquid wipers include at least one magnet or magnetizable material and a wiping lip that touches the inner walls while being located downstream of the coating agent supply in a zone of a sloped track of the hollow profiled bar.Type: ApplicationFiled: December 24, 2004Publication date: July 30, 2009Applicant: ROEHM GMBH & CO. KGInventors: Dieter Foerster, Juergen Krautter, Manfred Schneider
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Patent number: 7497221Abstract: A method for cleaning a tube-shaped chamber after performing at least one deposition process includes equipping a tube-shaped cleaner into a loading chamber, loading the tube-shaped cleaner into the tube-shaped chamber and injecting a cleaning gas, and cleaning the tube-shaped chamber using the tube-shaped cleaner.Type: GrantFiled: June 22, 2005Date of Patent: March 3, 2009Assignee: Hynix Semiconductor Inc.Inventor: Woo-Seock Cheong
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Patent number: 7498056Abstract: The method for reconditioning ducts in air conveying or processing networks envisages generating an air flow with maximum turbulence between two openings of the duct sections to be treated. An aerosol is then generated inside the airflow, consisting of a film-forming product with liquid droplets of predetermined average size, in the vicinity of an upstream section of the duct to be treated relative to the direction of movement of the air flow. The droplets containing polymer precursors are deposited on the inner surface of the duct forming a liquid film which, after a crosslinking step, results in the formation of a uniform and continuous solid coating. Measurement data identifying the geometric form of the duct to be treated are converted during a calculation step performed using a model into at least one pair of values for the flowrate and average size of the droplets, respectively.Type: GrantFiled: October 14, 2005Date of Patent: March 3, 2009Inventor: Francesco Viola
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Publication number: 20080220181Abstract: Nanotubes loaded with materials, such as active species, and methods to load materials into nanotubes are disclosed. The method includes flowing a medium containing the material to be loaded through the interior volume of the nanotube, wherein it is retained, optionally by a crosslinking or polymerization reaction. Flowing the medium occurs under different conditions and processes, including centrifuging and size exclusion methods.Type: ApplicationFiled: August 24, 2007Publication date: September 11, 2008Applicant: Philadelphia Health & Education Corporation, d/b/a Drexel University College of MedicineInventors: Nadarajan S. Babu, Elisabeth S. Papazoglou, Peter D. Katsikis
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Patent number: 7413773Abstract: Internally colored glass and glass-like blocks (10) and the method for making them. No means for coating the internal cavities (26) of clear glass and glass-like hollow blocks has been available. Color coating provides aesthetically pleasing structures. Internally colored glass and glass-like blocks may be used in building internal room dividers, providing colorful building designs and for providing color relief in heretofore otherwise drab structures.Type: GrantFiled: July 31, 2003Date of Patent: August 19, 2008Inventors: John McCoy, Deborah Elliott
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Patent number: 7407568Abstract: A novel on-line method is presented for the extraction and preconcentration of amino acids using a sol-gel coated column coupled to a conventional UV/vis detector. Extraction, stacking and focusing techniques are used in the preconcentration procedures. Sol-gel coatings are created by using N-Octadecyldimethyl[3(trimethoxysilyl)proply] ammonium chloride (C18-TMS) in the coating sol solutions. The resulting sol-gel coating carries a positive charge. For extraction, the pH of the samples is properly adjusted to impart a net negative charge to amino acids. A long plug of the sample is then passed through the sol-gel coated capillary to facilitate extraction via electrostatic interaction between the positively charged sol-gel coating and the negatively charged amino acid molecules. The focusing of the extracted amino acids is accomplished through desorption of the extracted amino acid molecules carried out by local pH change. The described procedure provides 150,000-fold enrichment effect for alanine.Type: GrantFiled: November 10, 2003Date of Patent: August 5, 2008Assignee: University of South FloridaInventors: Abdul Malik, Wen Li, David P. Fries
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Publication number: 20080131598Abstract: The process permits to strengthen a lever made of ceramic material. Ceramics is strong, but brittle, thus, in the course of lever operation it may undergo external mechanical forces, such as sudden impact, that generally cause cracks and spalling. After such damage ceramic pieces may separate from the ceramic support. The utility proposes to strengthen a ceramic lever with a special glue coating made of one of series of thermoplastic glue melts and applied to the internal surface of ceramic lever cavity. The solution has as its object to improve a ceramic lever strengthening process comprising application of glue coating made of a series of thermoplastic glue melts to the internal surface of a ceramic lever cavity according to which the glue coating undergoes thermal treatment at between about 80° C. and 180° C. before application to the internal surface of ceramic lever cavity.Type: ApplicationFiled: November 20, 2007Publication date: June 5, 2008Inventor: Igor Grigorovich Gumennyy
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Patent number: 7348039Abstract: A method of treating pipes to render the inner wall of the pipes resistant to corrosion and pre-mature deterioration. For new pipes, the inner wall is cleansed with a solvent, debris removed, and the inner wall dried. The inner wall is then coated with a corrosion-resistant primer and allowed to dry. The last step is to coat the inner wall with a corrosion- and chemical-resistant topcoat. More than one coat of primer and topcoat may be applied. The pipe may be re-treated by pumping a stripper through the inner wall removing all coating followed by cleansing and re-coating as described above.Type: GrantFiled: December 21, 2005Date of Patent: March 25, 2008Inventors: Jak Aklian, Hakob Grigoryan, Sargis Akliyan
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Patent number: 7192622Abstract: Process of masking cooling holes of a gas turbine component with an external surface, comprising a cavity and a plurality of cooling holes before coating the gas turbine component, comprising the steps of first applying a mask material to the cooling holes so that the cooling holes are filled at least closest to the external surface, whereby the mask material contains a substance which fluoresces under ultraviolet light and a filler material. Then the mask material within the cooling holes is thickening. An inspection using ultraviolet light to locate any unwanted residual mask material on the external surface is carried out and unwanted residual mask material is removed before the coating is applied to the external surface of the component and the masked cooling holes. In the end the mask material is removed from the cooling holes.Type: GrantFiled: November 24, 2004Date of Patent: March 20, 2007Assignee: Alstom Technology LtdInventors: John Fernihough, Andreas Boegli, Alexander Stankowski
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Patent number: 7094445Abstract: An article such as a hollow gas turbine blade has an internal cavity therein with an inlet and outlet. The outlet has an outlet minimum transverse dimension of from about 0.009 inch to about 0.012 inch. An aluminiding source powder has a minimum particle size of greater than about 0.0015 inch and not greater than about 0.005 inch. The aluminiding source powder is a mixture of from about 5 to about 15 percent by weight of a metallic aluminum-containing powder and from about 85 to about 95 percent by weight of a ceramic powder. The aluminiding source powder is flowed into the internal cavity through the inlet, and the article is heated with the aluminiding source powder in the internal cavity to a temperature of from about 1750° F. to about 2000° F., and for a time of from about 2 hours to about 12 hours, to deposit an aluminum-containing coating on the internal surface of the internal cavity. The aluminiding source powder is thereafter removed from the internal cavity through the inlet.Type: GrantFiled: May 7, 2002Date of Patent: August 22, 2006Assignee: General Electric CompanyInventor: Atul Natverlal Shah
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Patent number: 7090892Abstract: A method and apparatus for removing excess coating material from a honeycomb body of a catalytic converter. The coated honeycomb body is mounted on an eccentric tappet and is rotated around a first rotational axis with a first rotational frequency such that the distance from the center of gravity of the honeycomb body to the first rotational axis is at least 1.5 times the length of the honeycomb body. The honeycomb body is further rotated around a second rotational axis even out the coating material and provide a more uniform coating surface.Type: GrantFiled: October 13, 2004Date of Patent: August 15, 2006Assignee: Advanced Technology Products, Inc.Inventors: Robert Becker, Rolf Bruck
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Patent number: 7022381Abstract: A microvalve having a cast-in-place and lithographically shaped mobile, polymer monolith for fluid flow control in microfluidic devices and method of manufacture. The microvalve contains a porous fluorinated polymer monolithic element whose pores are filled with an electrically insulating, high dielectric strength fluid, typically a perfluorinated liquid. This combination provides a microvalve that combines high dielectric strength with extremely low electrical conductivity. These microvalves have been shown to have resistivities of at least 100 G? and are compatible with solvents such as water at a pH between 2.7 and 9.0, 1-1 propanol, acetonitrile, and acetone.Type: GrantFiled: June 30, 2003Date of Patent: April 4, 2006Assignee: Sandia National LaboratoriesInventors: Brian J. Kirby, David S. Reichmuth, Timothy J. Shepodd
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Patent number: 6972137Abstract: A process and apparatus are provided for the application of a fluoropolymer coating to the threads of an internally threaded fastener. The fastener has a body and a threaded bore extending to opposing ends of the body to define opposing first and second openings in the fastener. The fastener is moved on a conveyor along a path of travel with its threaded bore in a predetermined orientation. As the fastener moves along its path of travel, the first opening is closed by means of an obstructing member, while an air stream carrying entrained fluoropolymer powder is directed from a nozzle through the second opening and into the threaded bore. The nozzle is stationary and is located at an axially displaced position relative to the second opening of the fastener and immediately adjacent the conveyor. Preferably, the nozzle includes a diffuser which directs the air stream and entrained fluoropolymer powder into the fastener bore in a diverging pattern.Type: GrantFiled: May 1, 2003Date of Patent: December 6, 2005Assignee: Nylok CorporationInventors: Richard Duffy, Eugune Sessa
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Patent number: 6949269Abstract: A method is taught for fabricating patterned silicon dioxide layers on process areas disposed perpendicularly or at an inclination to a substrate surface. Firstly, a starter layer having leaving groups is produced by non-conformal deposition of a reactive component. Tris(tert-butoxy)silanol is subsequently added. The addition of the tris(tert-butoxy)silanol leads to the formation of a silicon dioxide layer selectively only on the starter layer.Type: GrantFiled: October 21, 2003Date of Patent: September 27, 2005Assignee: Infineon Technologies AGInventors: Harald Seidl, Martin Gutsche
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Patent number: 6942892Abstract: The present invention provides a method for efficiently and completely removing a film deposited inside a film forming chamber. In addition, the invention provides a CVD apparatus using heating element which an in-situ cleaning method can be applied and its in-situ leaning method. The removal method of this invention comprises a method for removing a film deposited inside a chamber which can be exhausted and/or on a member placed in the chamber, wherein after the chamber is exhausted, a heating element, at least the surface of which is composed of platinum, disposed in said vacuum chamber, is heated at a prescribed temperature and a cleaning gas which is decomposed and/or activated by the heating element to generate an activated species that converts the deposited film into gaseous substance is introduced into the chamber.Type: GrantFiled: August 4, 2000Date of Patent: September 13, 2005Assignee: Anelva CorporationInventor: Keiji Ishibashi
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Patent number: 6905731Abstract: There are provided a dust generation preventing structure of a wafer storage case and a process for preventing dust generation thereof, wherein dust generation is effectively prevented by blocking or suppressing free movement of particles constantly generated from a surface of a wafer storage case of a synthetic resin with a coating layer of a surfactant, and a wafer storing method using the wafer storage case. The wafer storage case of synthetic resin is used for housing wafers, and a surface of the wafer storage case is coated with a coating layer of a coating agent to prevent dust generation from the surface.Type: GrantFiled: January 19, 2001Date of Patent: June 14, 2005Assignee: Shin-Etsu Handotai Co., Ltd.Inventor: Hideki Munakata
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Patent number: 6902761Abstract: The invention relates to a method for the interior metal-coating of glass tubes, with the metal-coated surface being a cylindrical shell. In accordance with the invention such a method comprises the following process steps: the glass tube is sealed off at either end; the glass tube is brought to a horizontal position: a sensitizer solution is introduced into the interior space of the glass tube in such a quantity that the interior space is only partly filled; the sensitizer solution is removed from the interior space after a certain dwell period; a mirror-coating solution is introduced into the interior space of the glass tube, with the entire interior surface of the glass tube being wetted by the mirror-coating solution; the used-up mirror-coating solution is removed from the interior space of the glass tube.Type: GrantFiled: October 7, 2002Date of Patent: June 7, 2005Assignee: Schott AGInventors: Stephan Tratzky, Heinz Dotzler, Matthias Müller, Joachim Pfeifer, Michael Siller, Leonid Schulz, Gottfried Haas
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Patent number: 6866810Abstract: A treatment method for the internal surface of a molded polyethylene plastics material container such as a drum, including the steps of: introducing an ionizable gas, such as argon, into the container; generating a plasma of the introduced gas by applying electric field of sufficient strength to the container and introduced gas, so as to cause an interaction with the internal surface of the container; coating the internal surface of the container with a curable epoxy-based first polymeric composition; and then curing the polymeric composition to form a coating on the internal surfaces of the container. A second coating, preferably with electrical conductive properties, may be applied and cured over the first coating. Conductive properties may be provided by including conductive particles such as antimony doped tin dioxide, graphite or metal powders, in the second composition.Type: GrantFiled: January 26, 2001Date of Patent: March 15, 2005Assignee: Harcostar Drums LimitedInventors: Qamar Uddin Ahmed, Michael David Christy, Phillip Andrew Wallis
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Patent number: 6844024Abstract: A method of coating a polymer onto an implant having at least one interstice. The method includes (1) providing a solution containing a polymer; (2) applying the solution onto the implant; (3) and removing the solution spanning the interstice by (a) contacting the outer surface of the implant with a surface of a substrate, so that the solution spanning the interstice is drawn to the surface of the substrate via affinity between them; or by (b) bursting and removing the solution spanning the interstice on the implant with an air pressure difference before drying; and (4) drying the solution to form a coating.Type: GrantFiled: June 13, 2003Date of Patent: January 18, 2005Assignee: AST Products, Inc.Inventors: Shih-Horng Su, Tung-Liang Lin