Abstract: A process for preparing a surface for adhesive bonding to a second surface having the steps of abrasion cleaning the surface and then applying an adhesive thereon, wherein the improvement over prior art processes comprises the displacement of atmospheric gases from the surface by means of a dry inert gas. The abrasion cleaning is preferably achieved by bombarding the surface with particulate matter and removing the particulate matter before application of adhesive to the surface. The process is suitable for preparing metal surfaces for metal to metal bonds.

Abstract: A method for activating titanium surfaces for subsequent plating with metallic coatings comprising:(a) wet peening the titanium surface to be plated using fine-grain Al.sub.2 O.sub.3,(b) pickling the peened surface with a fluoridic solution at room temperature for several minutes, and(c) activating the surface with a solution containing chromium, fluorine, and arsenic or antimony at temperatures of 35.degree. to 100.degree. C. for fifteen to fifty minutes.The molar ratio of fluorine to arsenic or antimony is between six and seven, and the molar ratio of chromium to antimony or arsenic is between three and six.

Abstract: The life of AAS cuvettes coated with pyrolytic graphite is increased to more than 3000 injections when the coated substrata are additionally coated at least once with pyrolytic graphite, pyrolytic graphite layers having an overall thickness of 20-80 .mu.m then being applied.

Abstract: An improved method for coating a porous metal laminated structure having air flow holes on the coated side of the structure including in part, the steps of roughening an exposed surface of the porous laminated material and thereafter spraying a bond layer on the roughened surface at an angle selected to coat it with a thin bond coat layer while depositing only a limited amount of the bond coat material internally of the air flow holes and thereafter spray coating the bond coated surface with a top ceramic coat of heat resistant composition and characterized by requiring a bond coat for adherence to the porous metal laminated material and wherein the top ceramic coat spray angle is inclined opposite to that of the spray angle of deposition of the bond coat material to prevent deposition of the top coat on bond material internally of the air flow holes so as to prevent bonding of the ceramic top coat in the air flow holes thereby to minimize restriction of flow through the air flow hole in the exposed surface o

Abstract: A process for making a multilayer bearing material is provided which comprises a backing layer, an intermediate layer of aluminum and an outer overlay layer. The backing layer and aluminum layer are roll bonded together to form a composite strip which is then fed into a molten bath of overlay material which provides for good adhesion to the aluminum and also for good bearing material properties. The aluminum surface of the composite is then cleaned to remove surface oxide and the composite is removed from the bath into a guide means and through a gate which controls the thickness of the overlay so that upon solidification of the molten overlay material a finished bearing material is produced. The fusion bonding of overlay material to the composite is performed in a single operation.

Abstract: A cladding process and apparatus in which steel strip or sheet is cladded with a metal of lower melting point, e.g. lead, by maintaining a bank of constant level of the molten cladding material between a belt and the strip or sheet substrate which passes along an inclined path and is cooled to harden the molten material thereon. During the cooling process the applied material is compressed against the substrate.

Abstract: A metal article is coated on and at an edge thereof where at least two planar surfaces meet. The coating is carried out by initially coating the article at least partially at and on the edge, one surface at the edge is freed from coating in a mechanical way or an edge and a surface free from coating is prepared simultaneously in a mechanical way, as e.g. cutting off or sawing off part of the article. The exposed metal surface is then etched to form protecting coating projections and the etched surface is selectively coated. The article obtained has excellent and uniform resistant properties all over its surfaces.

Abstract: In an X-ray tube rotary anode having a supporting body (1) of molybdenum alloy, a target (2) of tungsten alloy, and a rough tungsten layer, applied by flame spraying to the whole surface of the anode except the focal path (4), for improving heat radiation, the rough tungsten layer does not adhere well to the tungsten alloy target, and particles of the rough tungsten layer may become detached in use, degrading the performance of the X-ray tube. To alleviate this problem, the whole surface of the anode, except the focal path (4), is blasted with steel grit, steel grit particles embedded in the anode are removed with acid, and the whole surface of the anode, except the target (2), is coated with a rough tungsten layer (3) by plasma spraying.

Abstract: There is disclosed a method for producing an electrical circuit board comprising the steps of selectively treating a portion of a conductive metal sheet in a pattern substantially corresponding to a predetermined printed circuit configuration and in a manner which renders the pattern portion of the sheet essentially adherent to a resin, placing the treated pattern portion of the sheet in direct contact with a layer of resin on the surface of an insulating substrate to form an assembly, uniformly heating the assembly to an elevated temperature to selectively bond the substrate to the treated pattern portion of the sheet, cutting the sheet along the perimeter of the pattern portions and stripping the non-pattern portions of the sheet from the substrate to form a circuit board.

Abstract: A method of treating metal sliding contact surfaces is disclosed. The method comprises pitting the surface (as by shot-blasting with glass or sand), impregnating the pitted surface with a dry lubricant (such as powdered graphite or MoS.sub.2), and roughening the impregnated surface to partially close the pits and to generate "peaks" of metal which are worn away during a bedding-in of the interengaging sliding contact surfaces.

Abstract: An automotive back window for flush glazing is manufactured by subsurface scoring a glass sheet to define an automotive back window blank in the sheet surrounded by sheet supporting glass portions. An endless band of ceramic paste is silk screened over the score as screen portions beyond the screen pattern are supported by the supporting glass portions. The sheet is thereafter baked to remove volatiles in the paste, the supporting glass portions removed from the blank and the blank having the baked pattern is bent and/or tempered.

Abstract: An automotive window is manufactured by silk screening a pattern of a ceramic paste on a piece of glass having peripheral dimensions greater than the peripheral dimensions of the window. During the silk screening, portions of the screen extending beyond the pattern are supported by glass portions extending beyond the window to prevent bending of the screen near the pattern. The piece is scored through the pattern to define the window or a window blank within the piece and thereafter the glass around the window is removed. The window is then tempered at which time the ceramic paste fuses to the window.

Abstract: A method of tensioning metallic strips on a slitting line is combined with the steps of uncoiling a metallic web having a non-uniform cross sectional thickness from an uncoiler, slitting the web into a plurality of strips having varying thicknesses, and recoiling the strips into individual strip coils on a recoiler, the tensioning method being the additional step of depositing a strippable polymeric compound onto thinner strips so that the effective cross sectional thicknesses of the thinner strips is increased to that of the thicker strips so that the strip coils formed from the strips are of similar diameter and recoil the strips at the same rate, thereby preventing the formation of slack strips. The apparatus includes a hot melt unit for generating strippable plastic in liquid form, a hot melt gun communicating with the apparatus, a support frame and movable arm on which the gun is mounted, and a motor driving a rack and pinion for positioning the hot melt gun over a selected strip coil.

Abstract: According to the present invention the microporous surface of a corrodible metal body is protected against corrosive agents of the atmosphere and even such severely corrosive agents as those found in marine environments, by an impregnation in the pores of an inner protective material, preferably oil, that is substantially impervious to corrosive agents, and a covering of outer protective material, preferably resin, that is intimately bonded to the outer surface of the metal and bridges over the impregnated pores. After the impregnation, any of the inner protective material such as oil that may remain on the outer surface of the metal is selectively removed, while the inner protective material in the pores is selectively retained, whereby a secure, intimate bond of the covering to the metal is assured to protect the metal from corrosion initiating from the outside, while the inner protective material remains operatively disposed in the pores to protect the covering from corrosive undermining.

Abstract: To provide an electrically conductive p-type wafer backside for semiconductor integrated circuit chips (die), a process is provided consisting of applying a thin layer of aluminum on a silicon dioxide free surface of the chip, followed by a layer of gold, then alloying the metals to diffuse the gold and traces of aluminum into the chip surface. The surface thus prepared can then be advantageously die attachable to a receiving surface by either eutectic alloy or conductive polymer techniques.

Abstract: Apparatus for forming a tube, preferably of flexible thermally insulating material, comprises a cutting head 14 with a pair of concentric cutting edge 16, 18 which cooperates with a presser head 28 to cut rings 50 of material from a sheet 48 presented to the cutting head. The rings are stacked up on a guide bar 32 and sprayed with a coating composition to consolidate them into a tube which may be collected on a take-up drum in a continuous manner.

Abstract: A process for enhancing the adhesion of coatings applied to the surfaces of glass-ceramic articles. The surface area to be coated is roughened before the article is completely cerammed. When the article is subjected to elevated temperatures for the purpose of converting the green glass to a glass-ceramic, flaws produced by the abrasion step are healed. The coating can be applied before or after the ceramming step.

Abstract: Sulfonato-organosilanol compounds and aqueous solutions and compositions thereof are provided which have at least one sulfonato-organic substituent therein. The weight percentage of oxygen in the compounds is at least about 30% and the weight percentage of silicon in the compounds is not greater than about 15%, these percentages being taken with reference to the water-free acid form of the compounds. Hydrophilic siliceous surfaces and processes for imparting hydrophilicity to such surfaces are also provided.

Abstract: A roller of the type useable as either of the pair of pressure applying rollers used in an instant photographic camera wherein a film unit consisting of a photosensitive element, an image receiving element and a rupturable pod containing a processing fluid is passed between a pair of pressure applying rollers which apply compressive pressure to the film unit so as to rupture the pod and dispenses the processing fluid between and in contact with the photosensitive element and the image receiving element to initiate a diffusion transfer process. The roller has a round roller body having fine surface irregularities and a plated layer of nickel which is reduction separated on the surface of the roller by using the roller material as a catalyst. The plated layer separated on the surface of the roller is of uniform thickness. The roller may be heat hardened after the nickel layer is reduction separated.

Abstract: Sodium nitrite in liquid form is deposited on a substrate and allowed to crystallize thereby forming a thin layer on the substrate. The substrate is either dipped into a solution containing sodium nitrite or into sodium nitrite in the molten state and then pulled out again. Subsequent drying or cooling of the wetted substrate top surface causes the crystalline film to form. Alternatively, sodium nitrite in a liquid state is applied to the top surface of the substrate and the substrate is rotated to assure an even distribution of the sodium nitrite. Again, drying or cooling causes the crystalline layer to form. The so manufactured unit is shown as part of a pyroelectric radiation detector, as image receiver in a television camera tube and as the storage element in a field effect transistor arrangement.

Abstract: This invention relates in general to the manufacture of segmented mirror solar collector troughs and specifically to the method and apparatus employed to initially subject the faceted segments to a lateral compression by the application of a vacuum prior to impregnating the segments in a fiberglass substrate which maintains the compressive force when the vacuum is removed.

Abstract: A process is disclosed for applying a thick inset of an antifriction or a thermosetting resin on a metallic surface, comprising the steps of forming a set of parallel and adjoining grooves on said metallic surface, jumping-up alternately the intergroove ridges in order to extend the anchorage surface for the resin and sintering the resin, such as Teflon, on the metallic surface which has been so prepared.

Abstract: An abrasive particle and method are provided for cleaning and rust-proofing steel prior to painting by subjecting the steel to abrasion with abrasive particles coated with a binder such as a synthetic resin which is compatible with the paint to be applied, and a corrosion resistant salt which has a solubility of not more than 20 grams per liter in water at 20.degree. C. The corrosion resistant composition is deposited on the steel surface as it is abraded.

Abstract: A method of and apparatus for uniformly debossing and perforating a ribbon of thermoplastic sheet material or film through the use of vacuum in combination with a flash heating source such as a flow of hot air. The apparatus causes a ribbon of such film to be forwarded from a supply such as a roll of thermoplastic material, then about a circumferentially extending portion of a rotating debossing-perforating cylinder, and then downstream where the debossed and perforated film may be further processed or where it may be wound on a spool to form a roll thereof. The debossing-perforating cylinder comprises a perforated tubular member through which a plurality of independently adjustable levels of vacuum can be applied from within the cylinder to circumferentially spaced sections of the film in contact with the exterior surface of the perforated tubular member. The apparatus further causes a virtual curtain of hot air to be directed radially inwardly towards a predetermined zone of the perforated tubular member.

Abstract: A coating of the inorganic zinc type which has, among other uses, excellent performance in the cathodic protection of metal from corrosion, especially when exposed to hot water. The coating is composed of mixture of zinc dust, extremely fine, high purity aluminum, sodium aluminum silicate and red iron oxide or titanium dioxide. Clay may be added for flow control and/or thixotrophy. The powder mixture is mixed with an alcoholic solution of partially hydrolyzed ethyl silicate liquid to form a slurry, and the slurry is thereafter sprayed or otherwise applied to a metal substrate to provide a coating having a thickness of 2 to 10 mils. Drying of the coating acts to evaporate the alcohol, and exposure to atmospheric humidity will fully hydrolyze the ethyl silicate to produce a dense, hard, tightly adherent coating which provides excellent corrosion resistance in a hot water environment.

Abstract: A mechanical plating process in which a work piece is plated without the necessity of tumbling the work piece in a barrel. A plating member having a plurality of plating elements is positioned with the plating elements adjacent a surface to be plated. Void spaces between the plating elements form reservoirs for liquid plating medium, containing a carrier liquid and plating metal particles. The liquid plating medium is supplied to the work area and to the reservoirs formed by the void spaces. A mechanical plating layer is formed by the plating metal particles by moving the plating member over the work surface with the plating elements, such as bronze wire elements, urged against the work surface. Additional plating medium is supplied to the work area and to the reservoirs during the plating operation to build up an adherent, mechanically applied, metal coating. The plated metal particles are preferably supplied to the work zone in flocculated form.

Abstract: A method for forming a drive wire hole in a ferrite toroid phase shifter pted to operate in the millimeter frequency range. The ferrite toroid is fabricated by the arc plasma spray process. A slab of boron nitride is initially bonded to the dielectric insert of the ferrite toroid and the ferrite powder is arc plasma sprayed on the composite boron nitride-dielectric structure. The formed ferrite toroid is then annealed, and during the annealing process, the boron nitride slab is completely sublimated to form the required drive wire hole.

Abstract: The invention contemplates a method and means for making a dryer or the like roll having a ferrous metal surface provided with a surface coating of a hardfacing alloy, the ferrous metal surface having a thermal conductivity relative to silver taken as 1 cal/cm.sup.2 /cm/.degree.C./sec of at least about 0.06 the hardfacing alloy being a hardfacing heat, corrosion and wear resistant iron-group metal-base alloy mechanically and metallurgically bonded to said ferrous metal surface which is preferably made of cast iron, the hardfacing alloy coating having a thickness ranging from about 0.01 to 0.15 inch, the thermal conductivity of said coating being at least 0.05.

Abstract: Method of making a high power laser mirror. Essentially the mirror consists of a refractory composition substrate which is polished to an optical finish and overcoated with a high reflectivity metal and a dielectric film disposed to cover the high reflectivity metal.The method includes the hot pressing of the refractory composition, especially silicon carbide, to form a substrate following which an optical finish is polished on one surface thereof. Thereafter, a metal film with a high reflectivity is applied to cover the optical surface and then a dielectric film is deposited over the high reflectivity metal film. Both films are deposited employing process of vacuum evaporation for deposition on the substrate. As thus combined, the mirror exhibits low optical absorptivity, high thermal conductivity, low weight, and low coefficient of thermal expansion. Since the substrate is formed of a hard refractory composition, an excellent optical finish can be polished on the surface thereof.

Abstract: A method of maintaining edge strength of a piece of glass i.e. preventing unintentional damage such as chips and/or scratches to the edges of the piece of glass during handling, processing and/or shipping is disclosed. A sheet of glass having dimensions greater than the desired size of the piece of glass is cut from a glass ribbon. The sheet of glass is pseudosubsurface scored or subsurface scored within the edges to define the piece of glass and to provide trim around the piece of glass which trim protects the edges of the piece of glass against unintentional damage. Thereafter, the sheet of glass is stored or processed, e.g., coating a surface of the sheet of glass with a transparent metal coating. The trim is removed from the sheet of glass at a fabrication station and the piece of glass having edges free of unintentional damage is used in the fabrication of a product e.g., a multiple glazed unit.

Abstract: A method of making composite material which provides low friction surfaces for materials in rolling or sliding contact. The composite material is self-lubricating and oxidation resistant up to and in excess of about 930.degree. C. The composite material is comprised of a metal component which lends strength and elasticity to the structure, a fluoride salt component which provides oxidation protection to the metal but may also enhance the lubrication qualities of the composite.

Abstract: In a process for forming an extremely hard-wearing rubber or bearing surface on a metal machine part, particles of hard grit, such as carbide grit, are deliberately formed into the surface using a resiliently-loaded tool, so that the surface becomes permanently impregnated with the hard particles. During the operation the particles can conveniently be contained in a slurry that flows over the surface. After impregnation, a lapping operation is performed on the impregnated surface using a fine carbide grit.

Abstract: The present invention concerns a novel method of making short silane treated inorganic glass fibers and mineral wool fibers with a very low shot content and the fibers thus produced.

Abstract: A method of preparing a heat-transfer member having a porous metallic heat-transfer interface comprising the steps of:(a) disposing at least one surface of a substrate in contact with a solution containing a salt of a thermally conductive metal, and(b) depositing said metal from said solution upon said substrate so as to form a dendritic metallic layer thereon constituting said porous heat-transfer interface.

Abstract: A method for producing a barrier in a thermally insulated container lined with polyurethane foam for storage or transport of liquefied gases, wherein a plurality of layers of an epoxy resin formulation and a glass-fiber material are applied in a particular sequence resulting in a barrier of superior quality essentially free of pinhole flaws.

Abstract: A novel light scattering reflector and methods of making and using it are disclosed. The reflector, which can advantageously be used in conjunction with liquid crystal displays, includes a layer carrier formed of glass or rigid PVC foil. The layer carrier is roughened by sandblasting, impressing with a grooved die, or by other techniques to provide an irregular surface. A reflective metal coating is subsequently evaporated onto the roughened surface to complete the reflector structure. Auxiliary materials may also be coated onto the layer carrier to improve the characteristics of the device.

Abstract: A multilayer dielectric mirror wherein the mirror substrate is of garnet. Chemical-mechanical final polishing of the substrate provides a surface relatively free of inhomogeneous strain for the deposition thereon of relatively homogeneous individual layers for a multilayer dielectric mirror coating.

Abstract: This invention is directed to a process for forming a hydrophobic and highly oleophilic coating on an aluminum surface which comprises treating the aluminum surface under aqueous alkaline conditions with a long chain aliphatic carboxylic acid (or an equivalent carboxylate compound), such as isostearic acid, which has one or more short secondary alkyl groups on or near the nonpolar end of the carboxylate compound. The coating can be formed by treating the surface with an aqueous alkaline solution which contains the carboxylic acid or the coating can be formed by mechanically deforming or upsetting the aluminum surface to expose a fresh aluminum surface to a carboxylic acid (or its equivalent) and a compound which generates alkaline conditions on the aluminum surface. In the latter instance, the carboxylic acid and alkaline compound is preferably incorporated into a metal-working lubricant used to facilitate deformation.

Abstract: This invention relates to the formation of a hydrophobic and usually oleophilic coating on an aluminum surface by mechanically deforming or upsetting the aluminum surface to disrupt the natural oxide coating in the presence of alkaline agents and a long chain aliphatic carboxylic acid or other equivalent long chain aliphatic carboxylate compounds. Preferably, the carboxylic acid and alkaline agent are incorporated into a metal-working lubricant which is maintained on the aluminum surface during fabrication, such as rolling, so that the hydrophobic coating is formed simultaneously with fabrication and thereby avoid the necessity of a separate coating operation.

Abstract: A portable automated coating plant is formed in sections that are transported individually to various work sites and the sections are assembled in end-to-end relationship for progressively cleaning and coating steel members, or the like. The members are passed in sequence through a shot blast machine a coating system, and a dryer.

Abstract: Disclosed is a photomask and a method for the manufacture thereof. A metal stencil is disposed on a glass substrate such that only preselected areas of the glass which are to be made opaque are exposed. A grit-etch step follows in which depressions are formed in the glass substrate in the preselected areas. Fusible masking material is sprayed in the depressions through the metal stencil. The masking material is preferably in particulate form in a volatile carrier liquid. The carrier liquid is preferably first driven off and, then, the combination is exposed to a relatively high temperature that fuses the masking material to the substrate.

Abstract: This invention is the production of a plain bearing having an aluminum interlayer and a metal overlay on the interlayer. The overlayer is for example cast on the interlayer so that it can constitute substantially the final bearing surface without machining after casting or roll-bonding. In order to enable the overlay to be cast on, the interlayer is abraded while below the surface of a tinning or other coating material in a material so that oxides can be removed from the aluminium surface and the coating applied to it without its becoming re-oxidised, and then the overlay can be applied to the coating.

Abstract: A method of treating sucker rod comprising shot peening the rod to clean and harden the exterior surface thereof, preheating the rod, and coating the rod with a metal alloy by using an electric arc spray gun to provide a layer of alloy on the exterior surface thereof. The rod is subsequently cooled and then coated with a baked-on, plastic-like surface.In one embodiment of the invention, used rod is first degreased, and following the shot peening operation the rod is subjected to an electronic test to determine the symmetry of compositon of the metal, as well as to ascertain if any flaws are present therein. The rod is then coated with metal and subsequently sprayed with plastic as in the above recited example.

Abstract: A method for coating the faces of parts having faces and backs, includes assembling the parts so that the faces and backs thereof define two opposed coating surfaces. The parts may be staggered, and alternate parts have their faces disposed in opposite directions, with faces recessed with respect to the backs of the adjacent parts. Both coating surfaces therefore comprise a plurality of recessed part faces interspersed with part backs.A hardenable coating such as a molten hard facing material is applied to both of the coating surfaces and allowed to harden. After hardening, the surfaces are ground to reduce the thickness of the hardened coating sufficiently to expose the part backs, leaving a desired residual layer of coating adhered to the recessed part faces. The parts are then disassembled to provide a plurality of separate parts, each having a coating on the face thereof.

Abstract: In a method for continuously coating with a coating solution a plurality of running webs having discontinuous areas in the surface thereof, the improvement which comprises coarsening at least the surface of the web coated in the area of the web immediately following the discontinuous area of the web prior to the coating. The discontinuous areas in the surface can arise from the tape used to connect one web to another web or from projection in the surface of the web.

Abstract: The invention relates to a method of aluminizing the inside of the panel of a television picture tube. When aluminizing the inside of the panel, blisters caused by the vaporizing lacquer, are likely to develop in the layer of aluminum, especially on the side walls of the panel portion. When taking care in accordance with the invention, that the coat of lacquer is roughened prior to the performance of the aluminizing process, these blisters are avoided.

Abstract: A protected easy-open metal end for containers is disclosed that contains a scoreline which defines on the central portion of the end a removable panel portion and a residual lip portion. A layer of synthetic resin hot melt material is deposited on one of the central panel surfaces opposite the scoreline, whereupon after the hot melt is solidified, the end is post heated to effect softening of the hot melt so that the metal end surface is wetted thereby. The resultant bond between the hot melt and the metal end is so great that severing of the removable panel from the end effects corresponding severing of the hot melt layer to provide protective hot melt layers on the edges of each of the panel and the residual lip portions. The hot melt layer may be applied to the same or the opposite central panel surface that contains the scoreline, or on both surfaces to provide two-side protection.

Abstract: An apparatus and method for continuously cleaning and coating wire is disclosed in which rod having scale and other inpurities on its outer surface is first mechanically descaled by passage through a plurality of spatially positioned rollers, then cleaned by frictional scraping by at least two rotating and orbiting abrasive drums which scrape the entire outer surface of the rod. The cleaned rod is then covered by a coating solution and electrically heated to a temperature sufficient to bake a coating on the exterior surface of the rod. The rod is then passed to a drawing apparatus.

Abstract: There is disclosed a method for producing aluminum coated steel comprising cleaning the surface of a steel substrate by grid- or shot-blasting or by pickling followed by rinsing with water and thermal spraying with aluminum thereon in a thickness ranging from 30 to 300 microns while heating said surface sufficiently to maintain it at a temperature ranging from about 100.degree. to 500.degree.C.The aluminum coated steel may be thereafter be treated by heating it at a temperature ranging from 150.degree. to 600.degree.C for 3 minutes to 24 hours after it has been cold-rolled to a reduction of area from 5 to 80% or after it has been hot-rolled at a temperature ranging from 150.degree. to 600.degree.C.

Abstract: The invention relates to a method of aluminizing the inside of the panel of a television picture tube. When aluminizing the inside of the panel, blisters caused by the vaporizing lacquer, are likely to develop in the layer of aluminum, especially on the side walls of the panel portion. When taking care in accordance with the invention, that the coat of lacquer is roughened prior to the performance of the aluminizing process, these blisters are avoided.