Abstract: Oil-borne preservative-impregnated wood is post-treated by:(A) contacting the preservative-impregnated wood in a closed vessel with steam and collecting a water-containing condensate generated in the vessel;(B) applying a vacuum which is sufficient to reflux water condensate to remove at least some surface deposits from the wood and to distill water out of the vessel leaving an oil-preservative solution in the vessel;(C) releasing the vacuum; and(D) recovering the post-treated wood from the vessel.

Abstract: The invention relates to an upwardly closed assembly and a simpler upwardly open assembly for uniformly loading one-piece carrier members, more particularly for catalysts, with a desired quantity of dispersions or solutions, the assembly being in the form of a cup receiving the bottom part of the carrier member and a distributor head for placing in sealing-tight manner on the carrier and having a perforated tray, formed with drip spouts at each outlet mouth, for distributing the applied liquid and, in the case of the upwardly-closed embodiment, including a cover and a number of pipes on the distributor head for supplying liquid, aerating and deaerating and a discharge pipe in the cup. The invention also relates to a method of operating the assembly and having features providing inter alia for movement of the distributor head relative to the carrier members in order to improve the distributor of liquid over the top surface of the carrier.

Abstract: A method of depositing a silicon dioxide film on the surface of a substrate such as alkali-containing glass by bringing the substrate into contact with a treating solution comprising a hydrosilicofluoric acid solution supersaturated with silicon dioxide, which is obtained by increasing the temperature of a hydrosilicofluoric acid solution substantially saturated with silicon dioxide.

Abstract: A method for forming a pigment containing film on a work-piece includes the steps of circulating coating liquid containing pigment through a circulation path, and pulverizing the pigment to disperse the pigment in the coating liquid during the circulating step. The method further includes the steps of dipping a work-piece in the coating liquid during the circulating step, and raising the work-piece from the coating liquid. An apparatus for forming a pigment containing film on a work-piece includes a coating tank, having an inflow portion and an overflow portion, for holding coating liquid containing pigment, and a circulation path having one end connected to the inflow portion of the coating tank and the other end connected to the overflow portion of the coating tank, for circulating the coating liquid. In the circulation path, a pulverizing device is arranged for pulverizing the pigment to disperse the pigment in the coating liquid and to cause the coating liquid to flow in the circulation path.

Abstract: Plant for treating water from a first pipe to protect the internal walls of a pipework, including a storage tank (R) for powdered lime, a loop (2) for bleeding water from the first pipe (1), a lime saturator (S) located on the loop (2), and structure (3, 4, 5) for adding powdered lime from the storage tank (R) into the saturator (S). The loop (2) includes, upstream of the saturator (S), relative to the direction of water flow, a decarbonator (D) fed with water which is to be treated. A second pipe (6, 2) which connects the outlet of the saturator (S) with the first pipe (1) includes a loop (7) for recycling a part of the material from the saturator (S) to the decarbonator (D). The structure for adding powdered lime includes a pipe (5) which receives the powdered lime and which connects the outlet of the decarbonator (D) with the inlet of the saturator (S).

Abstract: The present invention is a painting and filtration system wherein the system is capable of non-continuous operation, and wherein the system is capable of automatically removing impurities from the filtration system during operation. The system is particularly characterized by utilizing a solvent holding tank associated with a filtration unit, and sensors located in the solvent holding tank which generate signals to a controller which functions to activate and deactive the filtration system and functions to control the flow of liquid throughout the system so that the filtration unit can be cleaned when necessary during operation.

Abstract: Apparatus and a method is shown for continuously, in an on-line production, applying a layer of coating material to the horizontal upper surface of a fiber glass blanket and the opposed vertical edge surfaces in a generally even layer and curing the applied material to form surface and edge coated fiber glass duct liner material.

Abstract: A method and apparatus are disclosed for the treatment of paint sludge and for reducing volatile organic compound emissions from a paint spraybooth operation, thereby obtaining a recyclable material for use in new coating products. In such an operation, uncured paint resins mixed with volatile organic compounds are sprayed onto an article to be painted and at least a portion of the overspray is mixed with water to form a waste stream containing water, uncured paint resin, volatile organic compounds and inorganic substances. The method includes the steps of: removing a portion of the water and liquid volatile organic compounds from the waste stream; heating the resultant sludge to volatilize the residual water and liquid volatile organic compounds and to cure the uncured paint resin; collecting the residual solids stream, and removing all of the volatilized organic compounds from the resultant stream, thereby generating a volatile organic compound-free gas effluent.

Abstract: The present invention relates to a tank for use in recovering and reusing resist compositions, which comprises (a) means for measuring the viscosity of a previously used resist composition introduced into the recovery tank; (b) line means for feeding a solvent into the recovery tank; (c) line means for introducing the previously used resist composition into the recovery tank; (d) line means for discharging the viscosity adjusted resist composition from the recovery tank; and (e) means for opening the solvent feed line means described above in (b) when the viscosity as measured by the viscosity measuring means described above in (a) is higher than a predetermined viscosity, and means for closing the same when the predetermined viscosity is reached.

Abstract: A gravure coating device and method for applying a coating to a first side of a traveling continuous web. A pair of spaced rollers support the web on the second side while a gravure roller located between the rollers tangentially contacts the first side of the web. A doctor blade is utilized to remove excess coating from the gravure roller while a nozzle is utilized to apply the coating material to the gravure roller.

Abstract: A method for regenerating a carbon slurry used to produce a black matrix-type phosphor screen of a cathode ray tube is disclosed, in which excess carbon slurry is collected after the completion of a carbon-coating process onto a cathode ray tube panel. This collected carbon slurry is regenerated by means of an ion-exchange resin.

Abstract: Non-adherent copper metal particles ("fines") formed in a plating bath during the course of autocatalytic electroless copper deposition onto activated substrate surfaces are oxidized and redissolved in the bath by brief application of current between an anode element and a cathode element immersed in the bath, the anode element being comprised of an anode surface substantially parallel and proximate to the bottom surface of the vessel containing the bath.

Abstract: A forced air, ambient temperature, evaporator coupled to an electroless copper plating bath and to a purification system for replenishing and maintaining the stability of the plating bath, which bath tends to become depleted as the result of the reduction of water soluble cupric salt in an alkaline solution under copper plating and reducing conditions and in which the rate of evaporation of water from the surface thereof is insufficient to preclude growth in the volume thereof resulting from liquid additions thereto required to replace consumed constituents, thus giving rise to a need for bailout to prevent overflow thereof, solves the following problems: evaporation is independent of plating bath geometry; very high evaporation rates enable bailout to be zero at all plating loadings and plating thicknesses; the high evaporation rates provide sufficient cooling whereby the electroless copper solution can be introduced directly to the purification system with no additional cooling; dragout losses may be comple

Abstract: An apparatus coupled to an electroless copper plating bath for analyzing controlling, on-line, the primary constituents of the bath is described. The apparatus detects and controls not only the copper concentration of the bath by optical means, but the concentrations of hydroxyl ion, formaldehyde reducing agent and cyanide ion as well.

Abstract: An electroless copper plating bath is improved so as to facilitate its regeneration in an electrodialysis cell. The bath includes elevated amounts of an added salt, preferably as Na salt. The elevated sodium ion level serves as additional counter-cation to hydroxyl ion which is produced at the cathode of the electrodialysis cell. The excess anion from the added salt increases the rate of out-migration of by-products, such as formate ions and sulfate ions, relative to hydroxyl ions through an anion permselective membrane.

Abstract: This invention relates to particle coaters and in particular to a method and apparatus for a circulating bed particle coater which is particularly adapted for coating small diameter particles.

Abstract: Shaped articles, e.g., bars, of semiconductor-grade, ultra-pure silicon, are facilely and efficiently produced by thermally decomposing/pyrolyzing a monosilane feedstream on a red-heated silicon support member, whereby high purity silicon is deposited thereon, and then recycling the majority of the by-product reaction admixture into said monosilane feedstream.

Abstract: A forced air, ambient temperature, evaporator coupled to an electroless copper plating bath and to a purification system for replenishing and maintaining the stability of the plating bath, which bath tends to become depleted as the result of the reduction of water soluble cupric salt in an alkaline solution under copper plating and reducing conditions and in which the rate of evaporation of water from the surface thereof is insufficient to preclude growth in the volume thereof resulting from liquid additions thereto required to replace consumed constituents, thus giving rise to a need for bailout to prevent overflow thereof, solves the following problems: evaporation is independent of plating bath geometry; very high evaporation rates enable bailout to be zero at all plating loadings and plating thicknesses; the high evaporation rates provide sufficient cooling whereby the electroless copper solution can be introduced directly to the purification system with no additional cooling; dragout losses may be comple

Abstract: Process for introducing bath components into electrolytic and currentless (electroless) baths for the deposition of metal for deposition of metal layers, especially for introducing reducing agents in currentless baths, characterized by the bath components being introduced are admixed by an inert gas flowing through the bath.

Abstract: Copper is plated onto a substrate from an electroless plating bath having a mix potential relative to a saturated calomel electrode of about minus 630 to about minus 675 millivolts at a temperature of about 73.degree. C. The mix potential of the bath is monitored and adjusted during the plating to maintain it at about minus 630 to about minus 675 millivolts with respect to a calomel electrode at a temperature of about 73.degree. C. The number of of plating void defects is thereby reduced.

Abstract: The present invention is a self-contained fingerprinting system which includes a spray container and a portable vapor tank. The spray container discharges into the protable vapor container a mist of atomized particles of cyanoacrylate ester in order to generate vapors thereof. The vapors in the portable vapor tank fume an object suspected of containing latent fingerprints. The portable vapor tank includes a shroud which encloses the vapors from the mist of atomized particles of cyanoacrylate ester, a first supporting member which supports the shroud and a second supporting member which supports the object in front of the spray container. The portable vapor tank also includes a timer which determines the duration of fuming with the vapors and purging apparatus which purges the vapors from the portable vapor tank. The purging apparatus is electrically coupled to the timer and activated thereby at the end of duration of fuming with the vapors.

Abstract: The paint denaturant composition of this invention includes mixing magnesium sulfate with complex silicate minerals. The complex silicate minerals disclosed include bentonite clay, kaolin clay, and diatomite preferably a mixture thereof. The paint denaturant composition as disclosed is preferably a slurry but may be a dry powder composition. Additives incorporating magnesium sulfate, or a combination of magnesium sulfate, a polyelectrolyte and water, are also disclosed for use with paint denaturant compositions including silicate minerals. The addition of a polyelectrolyte solution to the magnesium sulfate and complex silicate mineral paint denaturant composition is also disclosed for improving floculation prior to filtration or mechanical separation.

Abstract: A fluid wash spray paint system which includes a plurality of paint spray booths is provided. Each paint spray booth includes a fluid wash device to entrap paint overspray in a moving fluid to remove the overspray from the booth. The system also includes a sludge pit for collecting the fluid and entrapped paint overspray from the plurality of spray booths. An automatic feeder is provided to introduce a deflocculant powder into the fluid and entrapped paint overspray to cause the paint to settle as sludge to the bottom of the sludge pit. A centrifugal separator is provided to separate and remove the settled sludge from the fluid and to return the fluid to the sludge pit. The system further includes a pump to circulate the fluid from the sludge pit through the plurality of fluid wash spray devices to form a closed system.

Abstract: A method and apparatus for controlling surface chemistry on objects plated in an electroless plating bath. Cyclic voltammetry measurements are made for different pH conditions of the bath. Pourbaix diagrams are determined from these measurements which indicate the transition between metal species being plated by the bath. The open circuit potential of the bath is monitored by a potentiostat and compared with a setpoint open circuit potential which represents a desired metal species on the pourbaix diagram. The monitored open circuit potential and the setpoint are utilized to derive an error voltage. The error voltage will control the concentration of a chemical constitutent of the plating bath to maintain the desired method species on the plating surface.

Abstract: Nodule formation in a continuous electroless copper plating system is minimized by independently controlling the dissolved oxygen contents on the plating solution in the bath and in the associated external piping. The level of dissolved oxygen in the plating tank is maintained at a value such that satisfactory plating takes place. At the point where the plating solution leaves the tank, additional oxygen gas is introduced into the solution so that the level of dissolved oxygen in the plating solution in the external piping is high enough to prevent any plating from taking place in the external piping and so that in the external piping the copper is etched or dissolved back into solution. At the end of the external piping, the dissolved oxygen level is reduced so that the dissolved oxygen level of the plating solution in the tank is maintained at the level where plating will take place.

Abstract: An apparatus, process and distributor for providing thin, uniform coating of thixotropic materials on substrates, especially on cylinders. The distributor equally subdivides the coating composition from entry ports to a plurality of exit ports.

Abstract: The present invention relates to a method for obtaining a tenacious in-situ coating deposition of calcite on the inner surface of water pipes at very high rates. The calcite producing ingredients are supplied to the water stream in quantities supplementing concentrations available in the natural water used, giving the required supersaturation levels by addition of suitable salts to provide an aqueous lining solution supersaturated with respect to calcium carbonate containing dissolved calcium and carbonate ions. The method consists in maintaining the suspended calcium carbonate particles concentrations in the lining solution below 300 ppm, the excess suspended particles being removed by physical means. The calcite coating deposition according to the present invention has the advantage that it occurs at the rate of above 5 microns/h and even above 50 microns/h, maintaining a completely corrosion-free system during the coating. The method is applicable to lead pipes, cement mortar linings or asbestos pipes.

Abstract: Solid particles or viscous liquid droplets of core material are encapsulated in a coating material largely as single particles with a single coherent coating, by feeding a suspension of the two materials onto a rotating surface. The suspension is centrifugally dispersed by the rotating surface into relatively large coated particles and relatively small droplets of coating material. Only the size of the droplets of unused coating corresponds to the droplets formed from atomization of the liquid coating material. The size of the coated particles depends on the size of the uncoated particles and is much less dependent upon the atomization characteristics of the rotating surface. Upon being thrown from the rotating surface, or falling from that surface, the droplets and coated particles are solidified by exposure to air and are separated by sieving, or the like. The solidified droplets of pure coating material may be recycled into the suspension.

Abstract: A coating method wherein a part of coating liquid supplied from a liquid supplying device is circulated through a closed passage running somewhere between the liquid supply device and a liquid delivery nozzle of a liquid applying section from the liquid applying section to the liquid supply device while the coating process is in operation. The amount of liquid circulated in the closed passage is 0.5 to 10 times the amount of liquid supplied by the liquid supply device.

Abstract: The present invention relates to improvements in impregnated wood preserving processes utilizing naphthalene containing preservative agents comprising recovering that portion of the naphthalene stripped from the preservative agent during a drying phase in the process and returning said recovered naphthalene portion to the impregnation phase of said process.

Abstract: A method for stabilizing the iron salt content of a PVDC latex autodeposition bath by: filtering a metered portion of the bath to separate it into a filtrate containing the iron salts and a retentate containing the latex and pigment particles; discarding the filtrate; recycling the retentate back into the bath; and adding D.I. water in a volume equal to that of the filtrate.

Abstract: A wet spray booth treating agent, characterized by containing melamine-aldehyde acid colloid solution and a method for the treatment of a wet spray booth, characterized by the use of the aforementioned treating agent.

Abstract: The present invention pertains to a method for coating metallic sheets which involves controlling the surface characteristics of the molten coating material in the area that the metal sheet enters and leaves so that the effect of contaminants on the coating operation will be minimized. The invention also pertains to an apparatus for carrying out this method.

Abstract: Method for controlling plating in an electroless plating process. The plating rate is continuously monitored. The plating rate is compared with a set point plating rate. A control voltage is derived proportional to the difference in plating rate and the desired plating rate, the integral of the difference, and the derivative of the difference. The control voltage is applied to a replenishment control for controlling the replenishment rate of a constituent chemical of the plating process.

Abstract: A method for treating hot glass containers that are moved through a treatment zone. The treatment zone is a system which utilizes heated compressed air aspirators rather than electric motor driven blowers to cause a treatment vapor laden air contained in chambers to be propelled across the width of the ware conveyor from both sides at adjacent, horizontally spaced, points in the conveyor length. The resultant streams of heated air and vapor laden air will impinge on the containers carried on the conveyor and are of a size to cover the container height to about the shoulder. The vapor and air that passes the containers from one direction is captured and fed to the chamber for feeding in the other direction. Thus the vapor laden air is recirculated from side to side with additional concentrated treatment vapors introduced to maintain a certain level of tin or titanium in the vapors so as to produce the metal oxide coating on the containers.

Abstract: The invention concerns a process to recover paint from overspray whereby one collects paint which misses the target object by means of a collector device which is flushed on all side and floor surfaces with circulating water, concentrates the overspray extracted in the overspray-circulating water mixture from the collector device to an overspray content of approx 20%, then feeds the mixture to a filtration chamber in which the water is separated from the reclaimed raw paint, then measures the physical characteristics of the reclaimed paint, compares these with the physical characteristics of the fresh paint, then adjusts the characteristics of the reclaimed paint to the characteristics of the fresh paint material and mixes the reclaimed paint into the fresh paint. The invention also concerns as device to carry out the process.

Abstract: A process of insulatingly coating a front and a back surface of a printed circuit board is disclosed. A vessel has a large top opening for receiving coating liquid therein and has a plurality of small apertures formed in the bottom. The vessel is immersed into a pool of coating liquid contained in a reservoir for injection of coating liquid into the vessel. The vessel is pulled upward from the reservoir before a printed circuit board reaches the location of the vessel, whereby a coating liquid flows down through the plurality of apertures in the vessel as series of continuous thin streams in the form of strings. A printed circuit board disposed at an angle is fed through the shower thus formed. After passing through the shower, the board is pivotally driven to present a surface which has previously been facing downward upward, and the board is again fed in an inclined position through the shower.

Abstract: Chemical treatments for detackification and separation of over-sprayed paints and lacquers in spray booths without corrosion and pollution problems. Water used to wash the air in paint or lacquer spray booths in order to remove over-sprayed paint or lacquers is treated with alkali-metal zincates optionally further containing strong cationic polyamine to reduce the tackiness of paint and lacquer solids and thereby reduce the tendency of oversprayed paints and lacquers to adhere to walls, ceilings and floors of said spray booths and also to condition the paint and lacquer solids removed with the water so that they can be separated and the water recycled for further use in washing the air in the spray booth. Furthermore, very little corrosion of air ducts, walls and ceilings of said spray booths, due to concentrated salts from the added chemicals, is expected because both alkali metal zincates and cationic polyamines contain only trace amounts of chlorides and sulfates.

Abstract: Paint spray booth detackifying and clarification compositions and methods are disclosed. The compositions are pumpable, hectorite clay containing slurries. In addition to hectorite, which has been proven as a most effective detackifying agent, the slurries include thinning agents such as water soluble aliphatic and/or alicyclic amines. Water conditioning agents, such as water soluble polyphosphates are also made part of the slurry formulation.

Abstract: A method for plating a metal from an electroless plating bath onto a substrate is provided which includes providing a source of an electroless plating bath at a non-plating temperature in a master mixing tank; transferring at least a portion of the plating bath to at least one plating cell, changing the bath temperature to a plating temperature, and contacting the substrate to be plated with the bath at a plating temperature.

Abstract: A method of removing liquid solvent from wood after pressure treatment with a preservative solution evaporates the excess solvent by mechanically circulating heated vapor of the same solvent used in the preservative solution past the wood in an autoclave. The autoclave is maintained at a constant pressure by transferring evaporated solvent to a condenser at a rate equal to the evaporation rate of solvent from the wood in the autoclave. The heat extracted from the condensing solvent vapor provides the heat to the circulating vapor in the autoclave for evaporating additional liquid solvent from the treated wood. Preferably, the vapor transferred from the autoclave is compressed before its delivery to the condenser so that the heat needed for evaporation in the autoclave can be obtained by simple heat transfer of the excess heat from the condenser.

Abstract: Anti-caking agent is thoroughly distributed upon particulate hygroscopic materials, e.g., particulate inorganic salts such as potassium chloride and sodium chloride, by contacting an agitated stream of the particulate material with an aqueous dispersion of anticaking agent and then passing the treated material through a fluid bed of the treated particulate material. The pretreated particulate hygroscopic material is typically warm, i.e., has a temperature above 25.degree. C., and is cooled in the fluid bed which is fluidized with dehumidified, fluidizing gas having a temperature lower than the treated particulate hygroscopic material entering the bed. Cooled particulate hygroscopic material having a coating of anticaking agent distributed substantially uniformly over the surface of the particles and having a water content substantially the same as the pretreated warm particulate material is removed from the fluid bed.

Abstract: A process is disclosed comprising a method for treating and conveying gas mixtures in a coating process employing a chemical, heterogeneous vapor-phase reaction in a reaction chamber in which the reaction product obtained in the reaction chamber is withdrawn from the reaction chamber, separated into at least one component, the withdrawn component is dosed and reintroduced into the reaction chamber.

Abstract: The invention relates to a method and an apparatus for the recovery of spraying substance when spraying elongated rolled stock. Difficulties are met when trying to recover water-dilutable or water-soluble coating agents since after evaporation of the solvent, i.e. the water, the film which is left can no longer be dissolved by water and thus it is no longer possible to recover this fraction of the spraying substance. According to the invention, therefore, it is proposed to carry out the spraying in a water-saturated atmosphere so that the excess spraying substance can easily be recovered. The apparatus is appropriately constructed to correspond to these circumstances.

Abstract: A thermography machine applies thermography powder to the printed surfaces of sheets. Excess powder is vacuumed from the sheets under the influence of suction generated by a cyclone separator which separates the excess powder from an air stream in which the powder is entrained. A static charge eliminator is provided for neutralizing the electrical charge on the powder particles to facilitate a smooth flow of the particles through the separator. The static charge eliminator includes a plurality of electrical charged pins across which is conducted a flow of outside air which is sucked through the static charge eliminator by the suction pressure from the separator. As the air flows across the charged pins, oxygen is converted to ozone and the ozone is conducted into contact with the powder particles within the separator. The pins have a contoured profile along their length to maximize the ozone-producing process.

Abstract: The present invention is a vapor phase activator pad which produces fluorescent vapor fumes for use in a self-contained fingerprinting kit. The vapor phase activator pad is placed into an enclosed area order to fume an object in the area suspected of containing latent fingerprints. The vapor phase activator pad includes a fluorescent dye impregnated gauze pad and a composition. The composition consists of specified chlorinated organic solvents. The gauze pad is chemically treated with the composition so that when a quantity of alkyl-cyanoacrylate is placed onto the vapor phase activator pad. The vapor phase activator pad generates fluorescent vapors of the chemical cyanoacrylate wherein the latent fingerprints become exposed when an ultraviolet light source is shined on the object suspected of containing the latent fingerprints.

Abstract: Apparatus for applying a primer paint coating onto a pipe wherein a structure movable along the pipe forms an enclosed annular cavity about the pipe. Primer paint fills the cavity and wets the complete circumference of the pipe. The cavity is filled by means of gravity flow with the surplus primer being collected in a reservoir and pumped back to the top of the cavity. Means are provided to wipe the primer to a predetermined thickness and returns the surplus to the reservoir. A gas rich environment surrounds the paint filled cavity and wiper means.

Abstract: A method and apparatus for applying granules to continuously moving strip asphaltic material comprises discharging granules onto tacky strip asphaltic material, continuously removing the non-adhered portion of the granules, sensing the amount of removed granules, and controlling the amount of granules discharged onto the asphaltic material in response to the sensed amount of removed granules.

Abstract: An apparatus for the recovery of solvents from coated parts during the drying step which consists of a means for heating the air used to dry the parts, an insulated drying chamber, a liquid spray scrubber, a refrigeration section to condense solvent and a cross-exchanger which allows air coming into the refrigeration section to be cooled by that exiting therefrom. The cooled solvent-lean air is then passed to the heating means before being recycled to the drying step.

Abstract: A method of applying liquid in a finely divided form onto a moving surface and an apparatus for carrying out that method. A flow of air containing suspended liquid particles is passed substantially parallel to the moving surface and across its direction of movement within a container which extends across the width of the moving surface. The container has a slit or a series of openings facing the moving surface, through which slit or openings at least a part of the liquid particles entrained in the air flow are deflected and passed substantially normal to the surface to be deposited thereon.