Silicon Containing Coating Patents (Class 427/452)
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Publication number: 20100159151Abstract: Methods of making components having calcium magnesium aluminosilicate (CMAS) mitigation capability including providing a component; applying an environmental barrier coating to the component, the environmental barrier coating having a separate CMAS mitigation layer including a CMAS mitigation composition selected from the group consisting of zinc aluminate spinel, alkaline earth zirconates, alkaline earth hafnates, rare earth gallates, beryl, and combinations thereof.Type: ApplicationFiled: December 19, 2008Publication date: June 24, 2010Inventors: GLEN HAROLD KIRBY, BRETT ALLEN BOUTWELL, JOHN FREDERICK ACKERMAN
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Patent number: 7736747Abstract: A method of joining two silicon members and the bonded assembly in which the members are assembled to place them into alignment across a seam. Silicon derived from silicon powder is plasma sprayed across the seam and forms a silicon coating that bonds to the silicon members on each side of the seam to thereby bond together the members. The plasma sprayed silicon may seal an underlying bond of spin-on glass or may act as the primary bond, in which case through mortise holes are preferred so that two layers of silicon are plasma sprayed on opposing ends of the mortise holes. A silicon wafer tower or boat may be the final product. The method may be used to form a ring or a tube from segments or staves arranged in a circle. Plasma spraying silicon may repair a crack or chip formed in a silicon member.Type: GrantFiled: June 1, 2006Date of Patent: June 15, 2010Assignee: Integrated Materials, IncorporatedInventors: James E. Boyle, Laurence D. Delaney
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Publication number: 20100143602Abstract: A method for coating a substrate is provided in that a plasma jet is produced from a working gas, at least one precursor material is fed to the working gas and/or the plasma jet and is reacted in the plasma jet and at least one reaction product of at least one of the precursors is deposited on at least one surface of the substrate and/or on at least one layer arranged on the surface. At least one of the deposited layers improve the optical transmission properties of the substrate.Type: ApplicationFiled: November 30, 2009Publication date: June 10, 2010Inventors: Andreas HEFT, Andreas Pfuch, Arnd Schimanski, Bernd Gruenler, Martin Polster
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Publication number: 20100129636Abstract: An abradable coating may include a rare earth silicate. The abradable coating may be deposited over a substrate, an environmental barrier coating, or a thermal barrier coating. The abradable coating may be deposited on a gas turbine blade track or a gas turbine blade shroud to form a seal between the gas turbine blade track or gas turbine blade shroud and a gas turbine blade. The abradable coating may also include a plurality of layers, such as alternating first and second layers including, respectively, a rare earth silicate and stabilized zirconia or stabilized hafnia.Type: ApplicationFiled: November 24, 2009Publication date: May 27, 2010Applicant: Rolls-Royce CorporationInventors: Michael Cybulsky, Kang N. Lee, Raymond J. Sinatra
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Publication number: 20100081558Abstract: This invention relates to ceramic powders comprising a zirconia-based component, e.g., yttria-stabilized zirconia, and an (alumina+silica)-based component, e.g., mullite. The ceramic powders are useful for forming thermal shock resistant coatings having the same composition, through deposition by thermal spray devices. This invention also relates to thermal barrier coating systems suitable for protecting components exposed to high temperature environments, such as the thermal environment of a gas turbine engine. This invention further relates to forming free-standing solid ceramic articles.Type: ApplicationFiled: October 2, 2006Publication date: April 1, 2010Inventor: Thomas Alan Taylor
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Publication number: 20100055339Abstract: A method is for forming a wear resistant coating on a workpiece. The method includes atomizing a metallic liquid including molybdenum in an atmosphere to form a crystalline metallic powder including molybdenum. The crystalline metallic powder is milled to form a nanocrystalline metallic powder including molybdenum. Moreover, the method includes thermal spraying the nanocrystalline metallic powder including molybdenum onto the workpiece.Type: ApplicationFiled: August 26, 2008Publication date: March 4, 2010Inventors: Sachin R. Shinde, Anand A. Kulkarni
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Publication number: 20100055340Abstract: A method for coating the core ceramic particles by emulsion flame spray is provided. In particular, the method forms a core ceramic particle simultaneously with coating the surface of the formed core ceramic particles by emulsion flame spray pyrolysis. The core ceramic particle may be coated in a single stage by emulsion flame spray pyrolysis conventionally used in the art, through putting coating material precursor into the oil phase of emulsion solution at a stage of preparing emulsion solution in emulsion flame spray pyrolysis process.Type: ApplicationFiled: August 28, 2009Publication date: March 4, 2010Applicant: KOREA ADVANCED INSTITUTE OF SCIENCE AND TECHNOLOGYInventors: Seung Bin Park, Shin Ae Song
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Publication number: 20100004110Abstract: The invention relates to a corrosion resistant reactor tube, method for providing a passivating or corrosion resistant coating to the inside of the reactor tube, and a method of making high bismuth glass powders using the corrosion resistant reactor tube.Type: ApplicationFiled: July 2, 2008Publication date: January 7, 2010Applicant: E.I.du Pont de Nemours and CompanyInventors: Michael F. Barker, John James Barnes, Rob Cockerill, Howard David Glicksman, Warren Harrell, James J. Krajewski, Michele L. Ostraat, Jay Scott Schickling, Barry Edward Taylor
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Publication number: 20090324930Abstract: An environmental coating system for silicon based substrates wherein a porous intermediate barrier layer having an elastic modulus of about 30 to 150 GPa is provided between a silicon metal containing bondcoat and a ceramic top environmental barrier layer.Type: ApplicationFiled: June 25, 2008Publication date: December 31, 2009Applicant: UNITED TECHNOLOGIES CORPORATIONInventors: Sonia Tulyani, Tania Bhatia
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Publication number: 20090316268Abstract: Methods for producing a quartz glass component with reflector layer are known in which a reflector layer composed of quartz glass acting as a diffuse reflector is produced on at least part of the surface of a substrate body composed of quartz glass. In order, taking this as a departure point, to specify a method which enables cost-effective and reproducible production of uniform SiO2 reflector layers on quartz glass components, it is proposed according to the invention that the reflector layer is produced by thermal spraying by means of SiO2 particles being fed to an energy carrier, being incipiently melted or melted by means of said energy carrier and being deposited on the substrate body. In the case of a quartz glass component obtained according to the method, the SiO2 reflector layer is formed as a layer which is produced by thermal spraying and has an opaque effect and which is distinguished by freedom from cracks and uniformity.Type: ApplicationFiled: December 13, 2007Publication date: December 24, 2009Inventors: Waltraud Werdecker, Rolf Gerhardt, Juergen Weber
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Publication number: 20090304943Abstract: A method for forming a ceramic containing composite structure is proposed comprising the steps of (a) feeding a ceramic component that sublimes and a metallic or semi-conductor material that does not sublime into a thermal spray apparatus, (b) spraying the ceramic component and the metallic or semi-conductor material onto a substrate, whereby the ceramic component and the metallic or semi-conductor material deposit on the surface of the substrate, and (c) keeping the metallic or semi-conductor material on the substrate surface plastic during spraying at least in the region where the metallic or semi-conductor material actually strikes the surface.Type: ApplicationFiled: March 20, 2006Publication date: December 10, 2009Applicant: SULZER METCO VENTURE LLCInventors: David S. Gollob, Thomas H. Piquette, James Derby, Omar Basil Al-Sabouni, Richard Karl Schmid, Jacobus Cornelis Doesburg
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Patent number: 7624500Abstract: The disclosure relates to circuits and methods for the manufacture of circuits, such as those which avoid the formation of undesirable short circuit paths. One such method maintains a layout area of a fluid composition receiving layer within a layout area of a dielectric layer. Another such method relates to the application of fluid composition receiving layers, conductive layers, and dielectric layers, such as in the provision of printed circuits.Type: GrantFiled: August 15, 2007Date of Patent: December 1, 2009Assignee: Lexmark International, Inc.Inventors: Xiaorong Cai, Michael John Dixon, Yimin Guan, Elios Klemo, Bryan Dale McKinley, Paul Sacoto, Jeanne Marie Saldanha Singh, George Nelson Woolcott, Frank Edward Anderson
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Patent number: 7596882Abstract: A treater oven for drying a prepreg includes: a pipe conduit configured such that the prepreg is able to pass therethrough; a the first structure connected to one side of the pipe conduit and supplying heated air to the pipe conduit; and the second structure connected to the other side of the pipe conduit and discharging the heated air from the pipe conduit. The first structure includes: an air supply portion connected to a heat exchanger and supplying the heated air; an air distribution discharge portion discharging the heated air supplied from the air supply portion through a pair of discharging outlets in both sides of the prepreg; and at least one perforated plate symmetrically disposed in air passageways of the air distribution discharge portion.Type: GrantFiled: May 13, 2005Date of Patent: October 6, 2009Assignee: LG Chem, Ltd.Inventors: Ye-Hoon Im, In-Seon Kim, Sang-Phil Han
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Patent number: 7597938Abstract: A method of making an oven door, or other coated article, is provided so as to have a color suppression coating on a substrate such as a glass substrate. Flame pyrolysis (or combustion CVD) is used in depositing at least part of a color suppression coating. For example, in an example embodiment of this invention, flame pyrolysis can be used to deposit a single SnO2 layer from suitable Sn inclusive precursor(s), or alternatively a multi-layer coating may be formed at least partially using flame pyrolysis. In another example embodiment, the coating may include a base layer of silicon oxide formed using flame pyrolysis, and another layer of tin oxide formed in any suitable manner over the base layer of silicon oxide.Type: GrantFiled: November 29, 2004Date of Patent: October 6, 2009Assignee: Guardian Industries Corp.Inventor: Scott V. Thomsen
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Publication number: 20090218213Abstract: A sputter target for sputtering a silicon-containing film is provided. The target includes a silicon-containing sputter material layer, and a carrier for carrying the sputter material layer, wherein the sputter material layer contains less than 200 ppm iron.Type: ApplicationFiled: February 18, 2009Publication date: September 3, 2009Applicant: APPLIED MATERIALS, INC.Inventors: Roland TRASSL, Wolf FRITSCHE
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Publication number: 20090202735Abstract: The invention provides a powder comprising at least 95% by number of fused grains, with the following chemical composition, as a percentage by weight based on the oxides, for a total of 100%: 0?BaO?40.8%; 0?SrO?31.8%; 27.2%?Al2O3?31.3%; 32%?SiO2?36.9%; other species?1%; the quantity of at least one of the oxides BaO and SrO being more than 0.3%, the size of said grains being such that D5?5 ?m and D95?150 ?m.Type: ApplicationFiled: February 13, 2008Publication date: August 13, 2009Applicant: SAINT-GOBAIN CENTRE DE RECHERCHES ET D'ETUDES EUROPEENInventors: Samuel Noel Patrice MARLIN, Howard Wallar
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Publication number: 20090176110Abstract: A coating system and process capable of providing erosion and corrosion-resistance to a component, particularly a steel compressor blade of an industrial gas turbine. The coating system includes a metallic sacrificial undercoat on a surface of the component substrate, and a ceramic topcoat deposited by thermal spray on the undercoat. The undercoat contains a metal or metal alloy that is more active in the galvanic series than iron, and electrically contacts the surface of the substrate. The ceramic topcoat consists essentially of a ceramic material chosen from the group consisting of mixtures of alumina and titania, mixtures of chromia and silica, mixtures of chromia and titania, mixtures of chromia, silica, and titania, and mixtures of zirconia, titania, and yttria.Type: ApplicationFiled: January 8, 2008Publication date: July 9, 2009Applicant: GENERAL ELECTRIC COMPANYInventors: Surinder Singh Pabla, Jon Conrad Schaeffer, Vinod Kumar Pareek, David Vincent Bucci, Thomas Moors, Jane Marie Lipkin
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Publication number: 20090162561Abstract: Methods for making barrier coatings including a taggant involving providing a barrier coating, and adding from about 0.01 mol % to about 30 mol % of a taggant to the barrier coating wherein the taggant comprises a rare earth element selected from lanthanum, cerium, praseodymium, neodymium, promethium, samarium, europium, gadolinium, terbium, dysprosium, holmium, erbium, ytterbium, and lutetium, salts thereof, silicates thereof, oxides thereof, zirconates thereof, hafnates thereof, titanates thereof, tantalates thereof, cerates thereof, aluminates thereof, aluminosilicates thereof, phophates thereof, niobates thereof, borates thereof, and combinations thereof.Type: ApplicationFiled: December 19, 2007Publication date: June 25, 2009Inventors: GLEN HAROLD KIRBY, Stephen Mark Whiteker, Brett Allan Boutwell, Jessica Lee Licardi
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Publication number: 20090130326Abstract: An interlayer insulating film enabling an enhancement in a signal processing speed to be obtained, of which a dielectric constant is 2.2 or less. There is provided a method of forming a film on a substrate in accordance with a chemical vapor deposition process, comprising: the feeding step of feeding (c-C5H9)2Si(OCH3)2 by inert gas bubbling; and the deposition step of causing any of decomposition product resulting from decomposition of the (c-C5H9)2Si(OCH3)2 fed in the above feeding step to deposit on the substrate.Type: ApplicationFiled: January 10, 2006Publication date: May 21, 2009Applicant: TRI CHEMICAL LABORATORIES INC.Inventors: Hideaki Machida, Ikuyo Muramoto, Young Hua Xu
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Publication number: 20090123659Abstract: A modified flame-spraying method for producing self-cleaning surfaces by a dry coating process penetrates particles in a hot air or flame stream into the softened substrate surface. The process can be applied to textiles and other articles having plastic surfaces.Type: ApplicationFiled: November 25, 2008Publication date: May 14, 2009Applicant: CREAVIS Gesellschaft fuer Tech. und Innovation mbHInventors: Markus Oles, Edwin Nun
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Patent number: 7531232Abstract: A component for a vacuum apparatus for use in a plasma processing apparatus or a film forming apparatus for a semiconductor or the like, in which a surface is covered with a ceramic and/or metallic thermal spray film and projection-shaped particles of a width of 10-300 ?m, a height of 4-600 ?m and an average height/width ratio of 0.4 or higher are present within a range of 20-20,000 particle/mm2 on the surface of the thermal spray film. The thermal spray film has a porosity of 10-40%, shows a high adhering property to a film-shaped substance, is free from a product contamination by particles generated by a peeling of the film-shaped substance and can be continuously used over a prolonged period.Type: GrantFiled: October 15, 2004Date of Patent: May 12, 2009Assignee: Tosoh CorporationInventors: Koyata Takahashi, Osamu Matsunaga, Michio Okamoto
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Patent number: 7527832Abstract: A plasma spray process for structuring self-cleaning glass surfaces and self-cleaning glass surfaces formed according to the process. Molten or heat softened particles of inorganic material are plasma spray deposited onto the surface of a substrate to create a micro-rough surface. If desired, a hydrophobic top coating layer can optionally be applied to the micro-rough surface. The micro-structured surface formed according to the invention is durable and self-cleaning.Type: GrantFiled: April 27, 2005Date of Patent: May 5, 2009Assignee: Ferro CorporationInventors: George E. Sakoske, Martin Baumann, Enos A. Axtell, III
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Patent number: 7504008Abstract: In a method of refurbishing a deposition target, a surface of the target is provided in a process zone. An electrical arc is generated in the process zone, and a consumable metal wire is inserted into the process zone to form liquefied metal. A pressurized gas is injected into the process zone to direct the liquefied metal toward the surface of the target to splatter the liquefied metal on the surface, thereby forming a coating having the metal on at least a portion of the surface of the target that exhibits reduced contamination from the environment.Type: GrantFiled: March 12, 2004Date of Patent: March 17, 2009Assignee: Applied Materials, Inc.Inventors: Trung T. Doan, Kenny King-Tai Ngan
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Publication number: 20090068405Abstract: A ceramic-resin composite roll (1) comprises a metal roll core (2), a foundation layer (3) formed on the outer circumferential surface of the metal roll core (2) and a thermally sprayed ceramic film (4) formed on the outer circumferential surface of the foundation layer (3). The thermally sprayed ceramic film (4) includes a ceramic particle layer in which adjacent ceramic particles are fused and bonded to each other and a layer of a resin (6) penetrating into the spaces among the ceramic particles (5) from the surface of the ceramic particle layer to the surface of the foundation layer (3).Type: ApplicationFiled: February 19, 2007Publication date: March 12, 2009Applicant: Yamauchi CorporationInventor: Hiroya Shimazaki
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Publication number: 20090053533Abstract: A corrosion-resistant member comprising a base material having formed thereon a spayed coating having high corrosion resistance to corrosive gases or plasma, and a process of producing the same are disclosed. The corrosion-resistant member comprises a base material having formed thereon a sprayed coating, the sprayed coating being formed on the site of the base material to be exposed to corrosive gases or plasma and comprising Si, O, N, Group 2a element, and at least one element selected from the group consisting of Al, B, Zr and Ti, or comprises a base material having formed thereon a sprayed coating, the sprayed coating being formed on the site of the base material to be exposed to corrosive gases or plasma and comprising Si, O, N, Group 3a element, and at least one element selected from the group consisting of B, Zr and Ti.Type: ApplicationFiled: October 23, 2008Publication date: February 26, 2009Applicant: TOSOH CORPORATIONInventors: Masanori Abe, Koyata Takahashi
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Patent number: 7479306Abstract: A low-k dielectric material with increased cohesive strength for use in electronic structures including interconnect and sensing structures is provided that includes atoms of Si, C, O, and H in which a fraction of the C atoms are bonded as Si—CH3 functional groups, and another fraction of the C atoms are bonded as Si—R—Si, wherein R is phenyl, —[CH2]n— where n is greater than or equal to 1, HC?CH, C?CH2, C?C or a [S]n linkage, where n is a defined above.Type: GrantFiled: May 18, 2005Date of Patent: January 20, 2009Assignee: International Business Machines CorporationInventors: Daniel C. Edelstein, Stephen M. Gates, Alfred Grill, Michael Lane, Qinghuang Lin, Robert D. Miller, Deborah A. Neumayer, Son Van Nguyen
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Publication number: 20090008068Abstract: This invention relates to a method of manufacturing an aluminum heat exchanger tube. In forming a thermally sprayed layer 21 on a surface of an aluminum flat tube by thermally spraying Al—Si alloy thermal-spraying particles, quenching the thermally sprayed thermal-spraying particles in a molten state to make them adhere to the tube core 2a. The surface of the thermally sprayed layer 21 is smoothed with, e.g., reduction rolls to form a brazing layer 20. With this method, brazing defects due to fin detachment, erosion to the tube of the brazing material, etc., can be prevented, resulting in good brazing performance.Type: ApplicationFiled: April 8, 2005Publication date: January 8, 2009Applicant: SHOWA DENKO K.KInventors: Kazuhiko Minami, Tomoaki Yamanoi, Takenori Hashimoto
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Patent number: 7473443Abstract: There are provided a silicon-film-forming composition containing silicon particles and a dispersion medium and a method for forming a silicon film by forming a coating film of the silicon-film-forming composition on a substrate and subjecting the coating film to instantaneous fusion, a heat treatment or a light treatment. According to the composition and the method, a polysilicon film with a desired thickness which may be used as a silicon film for a solar battery can be formed efficiently and easily.Type: GrantFiled: August 15, 2003Date of Patent: January 6, 2009Assignee: JSR CorporationInventors: Yasuo Matsuki, Haruo Iwasawa, Hitoshi Kato
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Publication number: 20080317966Abstract: In a thermally sprayed, gastight protective layer for metal substrates, especially those based on Fe, Ni, Al, Mg and/or Ti, wherein the spray powder for the purpose comprises at least two components, of which the first is a silicate mineral or rock and the second is a metal powder and/or a further silicate mineral or rock, the silicate mineral or rock component in the spray powder has an alkali content of less than 6 per cent by weight.Type: ApplicationFiled: May 30, 2008Publication date: December 25, 2008Applicant: MARKISCHES WERK GMBHInventor: Vadim VERLOTSKI
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Publication number: 20080292806Abstract: The present disclosure relates to an apparatus and method for plasma ion deposition and coating formation. A vacuum chamber may be supplied formed by a hollow substrate having a length, diameter and interior surface. A plasma may be formed within the chamber while applying a negative bias to the hollow substrate to draw ions from the plasma to the interior surface of the hollow substrate to deposit ions onto the interior surface and forming a coating. The coating may have a Vickers Hardness Number (Hv) of at least 500.Type: ApplicationFiled: May 23, 2007Publication date: November 27, 2008Applicant: SOUTHWEST RESEARCH INSTITUTEInventors: Ronghua WEI, Christopher RINCON, James H. ARPS
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Publication number: 20080268165Abstract: Inorganic porous substrates and methods of making inorganic porous substrates utilizing nanoparticles deposited onto a base substrate are described. The inorganic porous substrates are useful for biological applications, for example, biomolecule attachment such as DNA, RNA, protein and the like. The inorganic porous substrates are also useful for cell growth applications.Type: ApplicationFiled: August 10, 2007Publication date: October 30, 2008Inventors: Curtis Robert Fekety, Yichun Connie Wang, Joseph Marc Whalen
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Publication number: 20080264176Abstract: The invention relates to a method of depositing an alumina coating on a part having a silicon carbide surface. The method comprises the following steps: a) depositing a silicon adhesion underlayer on the SiC surface by chemical vapor spraying; and b) depositing a coating on the silicon adhesion underlayer by atmospheric thermal spraying. The invention also provides a device for measuring deformation, which device comprises a first alumina coating obtained by atmospheric thermal spraying onto the silicon adhesion underlayer deposited on the silicon carbide layer covering the substrate of the part, a free filament strain gauge placed on the coating, and an additional alumina coating obtained by atmospheric thermal spraying onto the strain gauge.Type: ApplicationFiled: April 24, 2008Publication date: October 30, 2008Applicant: SNECMAInventors: Pierre Bertrand, Christian Coddet, Sophie Costil, Frederic Leman, Sebastien Lukat
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Publication number: 20080241523Abstract: The invention relates to a substrate of which at least one part of the surface thereof has been rendered hydrophobic and, for said purpose, has a hydrophobic surface structure consisting of an essentially-mineral silicon-containing sub-layer and an outer layer comprising a hydrophobic agent which is grafted onto said sub-layer. The invention is characterised in that the outer hydrophobic agent layer is applied to the sub-layer while the surface of the latter is in an activated state before being brought into contact with said hydrophobic agent. The invention also relates to rain-repellent glass comprising one such substrate, which is particularly suitable for use in the automobile, aviation, construction, electric household appliance and ophthalmic lens industries.Type: ApplicationFiled: February 23, 2005Publication date: October 2, 2008Applicant: SAINT-GOBAIN GLASS FRANCEInventors: Arnaud Huignard, Maxime Duran
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Publication number: 20080233355Abstract: In order to avoid haloing when burning in a decoration on a glass ceramic substrate, the invention provides a method for producing a decorated glass ceramic substrate, in which a glass substrate is produced or provided, a layer containing silicon oxide is deposited on the substrate, decorative ink is applied on the layer containing silicon oxide and the decorative ink is burned in, wherein the layer containing silicon oxide is flame-pyrolytically deposited by sweeping over at least one region of the surface of a substrate with a flame and hydrolyzing a silicon compound added to the flame.Type: ApplicationFiled: November 3, 2005Publication date: September 25, 2008Applicant: SCHOTT AGInventors: Inka Henze, Michael Bug, Gerhard Hahn, Ottmar Becker, Veit Luther
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Publication number: 20080187767Abstract: A process for applying an oxidation resistant coating to an article includes the steps of mixing at least about 10% by volume to up to about 99% by volume of a slurry at least one silica based material having a viscosity of about 1×102 poise to about 1×107 poise at a temperature of about 1,292° F. (700° C.) to about 3,272° F. (1,800° C.) at least about 1% by volume to up to about 90% by volume of the slurry at least one oxygen scavenger, and a liquid medium to form the slurry; coating an article with the slurry to form a slurry coated article; and heat treating under an inert atmosphere the slurry coated article to form an article having at least one oxidation resistant coating layer containing the at least one oxygen scavenger.Type: ApplicationFiled: November 21, 2006Publication date: August 7, 2008Inventors: Xia Tang, Tania Bhatia, David C. Jarmon, Wayde R. Schmidt, Harry E. Eaton, John G. Smeggil
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Publication number: 20080166493Abstract: Anti-fouling coating compositions and methods of making and using those compositions are provided. In an embodiment, a coating composition comprises ceramic nanoparticles, wherein the coating composition is capable of inhibiting contaminants from adhering to a solid surface.Type: ApplicationFiled: January 9, 2008Publication date: July 10, 2008Applicant: INFRAMAT CORPORATIONInventors: T. Danny Xiao, Xinqing Ma, Kim Arnold Wynns, Meidong Wang, Jinxiang Dai
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Publication number: 20080138620Abstract: Method of producing a target by thermal spraying, especially by plasma spraying, said target comprising at least one compound based on atoms of different types chosen especially from the constituents M belonging to the (Zr, Mo, Ti, Nb, Ta, Hf, Cr) family and silicon, characterized in that at least one fraction of said compound, the constituents of which are bonded by covalent and/or ionic and/or metallic bonds, is injected into a plasma jet, said plasma jet spraying the constituents of said compound onto the target so as to deposit a coating of said compound on a surface portion of said target.Type: ApplicationFiled: February 3, 2006Publication date: June 12, 2008Applicant: Saint-Gobain Glass FranceInventors: Nicolas Nadaud, Dominique Billieres
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Publication number: 20080131611Abstract: Provided herein are methods and apparatuses, and resulting structures, for depositing ceramic coatings with preferred coating density, morphology and adherence for applications such as thermal protection of internally cooled components. Such components are found in, but not limited thereto, the hot sections of gas turbine and diesel engines and in turbo machinery. These coatings require a low thermal conductivity in the through thickness of the coating, high in-plane elastic compliance, high erosion and foreign object damage resistance and resistance to hot corrosion. The methods and apparatuses discussed herein provide, among other things, how to manipulate the process conditions in EB-DVD systems to deposit high quality, highly efficient TBS top coats as well as how to deposit high quality TBC top coats onto positions that are in the line-of-sight, as well as non-line of sight, of the vapor source.Type: ApplicationFiled: July 28, 2004Publication date: June 5, 2008Inventors: Derek D. Hass, Haydn N.G. Wadley
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Publication number: 20080124479Abstract: Process includes providing a silicide-containing bond coat layer overlying a silicon-containing substrate, optionally forming a silica scale layer adjacent to and overlying the bond coat layer by preoxidizing the bond coat layer, and providing an environmental barrier coating overlying the bond coat layer. The environmental barrier coating includes a corrosion resistant outer layer formed by reacting a metal source with the silica scale layer, if present, or with the silicide-containing substrate in the absence of the silica scale layer. The process may include providing a thermal barrier coating overlying the corrosion resistant outer layer. The silicon-containing substrate may include at least a portion of a gas turbine engine component selected from a turbine blade, vane, and blisk.Type: ApplicationFiled: February 5, 2008Publication date: May 29, 2008Inventors: Brian Thomas Hazel, Irene Spitsberg, Brett Allen Boutwell
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Publication number: 20080113106Abstract: Provided is a surface modification process in which the mixture molar ratio of air/hydrocarbon gas in a fuel gas including a reforming agent modifying compound containing a silane molecule silicon atom, titanium atom or aluminum atom, air and a hydrocarbon gas is set to a value in valu within a predetermined range, whereby a predetermined surface modification effect can be stably obtained for a solid material, regardless of differences of boiling points of reforming agent modifying compounds, environmental conditions of the surroundings, and the like. For this end, a flame produced from of the fuel gas, in which the mixture molar ratio of air/hydrocarbon gas is adjusted to 23 or more, together with a predetermined reforming agent modifying compound, is blown against toward the surface of a solid material by means of a surface modification apparatus.Type: ApplicationFiled: August 2, 2006Publication date: May 15, 2008Inventor: Yasuhiro Mori
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Publication number: 20080090071Abstract: The present invention relates to a method of coating a surface with nanoparticles, to a nanostructured coating that can be obtained by this method, and also to a device for implementing the method of the invention. The method is characterized in that it comprises an injection of a colloidal sol of said nanoparticles into a plasma jet that sprays them onto said surface. The device (1) comprises: a plasma torch (3); at least one container (5) containing the colloidal sol (7) of nanoparticles; a device (9) for fixing and for moving the substrate(S); and a device (11) for injecting the colloidal sol into the plasma jet (13) of the plasma torch. The present invention has applications in optical, electronic and energy devices (cells, thermal barriers) comprising a nanostructured coating that can be obtained by the method of the invention.Type: ApplicationFiled: October 20, 2005Publication date: April 17, 2008Applicant: COMMISSARIAT A L'ENERGIE ATOMIQUEInventors: Karine Valle, Philippe Belleville, Karine Wittmann-Teneze, Luc Bianchi, Franck Blein
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Patent number: 7338699Abstract: In film-forming devices and plasma-processing devices, filmy matter adheres to the surfaces of the inner parts and it peels to cause dust and particles in the devices. In the devices, the dust and particles contaminate the objects for film formation thereon or the objects to be processed with plasma. For preventing the objects from being contaminated with them, the inner parts of the devices must be frequently exchanged every time when they have received any minor filmy matter thereon, and this lowers the productivity in the devices. When a modified glass part of which the surface is modified with spherical or bell-like island projections having a width and a height of from a few ?m to a few hundreds ?m is used in a film-forming device and in a plasma-processing device, then its ability to hold the filmy substance having adhered thereto is good and its resistance to plasma is also good.Type: GrantFiled: October 30, 2003Date of Patent: March 4, 2008Assignee: Tosoh CorporationInventors: Koyata Takahashi, Masanori Kohgo, Osamu Matsunaga
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Publication number: 20080023070Abstract: The present invention relates to a novel, unconventional methods and systems for the fabrication of silicon or silicon-germanium photovoltaic cell applications. In some embodiments high purity gaseous and/or liquid intermediate compounds of silicon (or silicon germanium) are converted directly to polycrystalline films by a thermal plasma chemical vapor deposition process or by a thermal plasma spraying technique. The intermediate compounds of silicon (or silicon germanium) are injected into the thermal plasma source where temperatures range from 2000 K to about 20,000 K. The compounds dissociate and silicon (or silicon germanium) is deposited onto substrates. Polycrystalline films having densities approaching the bulk value are obtained on cooling. PN junction photovoltaic cells can be directly prepared by spraying, or doped films after heat treatment are subsequently transformed to viable photovoltaic cells having high efficiency, low cost at a high throughput.Type: ApplicationFiled: July 26, 2007Publication date: January 31, 2008Inventor: Sanjai Sinha
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Patent number: 7279078Abstract: A process for coating a non-uniform, thin-film, dichroic pattern to a wheel rim or motorcycle part. The thin-film coating adds a colored or iridescent pattern to the wheel rim or motorcycle part, while maintaining other characteristics, such as brilliance, shine, durability and general appearance. The coating is intentionally non-uniform. It may be varied, and may have different patterns and color among different articles, and even among different areas on the same article. The thin-film coating may be added by various techniques known in the art, but is preferably applied by sputtering a silicon or titanium target to obtain the thin-film on a chromed wheel rim.Type: GrantFiled: April 25, 2005Date of Patent: October 9, 2007Inventors: Micha Kapourchali, Nima Khalilian
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Patent number: 7186663Abstract: A method is provided for forming a Si and Si—Ge thin films. The method comprises: providing a low temperature substrate material of plastic or glass; supplying an atmosphere; performing a high-density (HD) plasma process, such as an HD PECVD process using an inductively coupled plasma (ICP) source; maintaining a substrate temperature of 400 degrees C., or less; and, forming a semiconductor layer overlying the substrate that is made from Si or Si-germanium. The HD PECVD process is capable of depositing Si at a rate of greater than 100 ? per minute. The substrate temperature can be as low as 50 degrees C. Microcrystalline Si, a-Si, or a polycrystalline Si layer can be formed over the substrate. Further, the deposited Si can be either intrinsic or doped. Typically, the supplied atmosphere includes Si and H. For example, an atmosphere can be supplied including SiH4 and H2, or comprising H2 and Silane with H2/Silane ratio in the range of 0–100.Type: GrantFiled: June 17, 2004Date of Patent: March 6, 2007Assignee: Sharp Laboratories of America, Inc.Inventors: Pooran Chandra Joshi, Apostolos T. Voutsas, John W. Hartzell
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Patent number: 7160584Abstract: A method for manufacturing a ceramic glow pin which is formed of more than two layers arranged especially coaxially to the axis of the glow pin and symmetrically. The layers of the layer structure are manufactured by co-extrusion.Type: GrantFiled: November 10, 2004Date of Patent: January 9, 2007Assignee: Beru AGInventors: Oliver Goeb, Hans Houben, Lutz Frassek, Henning Von Watzdorf, Martin Allgaier, Johann Weissenbacher
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Patent number: 7157145Abstract: An article is described comprising a substrate and a plasma polymer coating comprising silicon, oxygen and carbon bonded to the surface of the substrate, in respect of which coating the following applies in the case of determination by means of ESCA: the mole ratio O: Si is >1.25 and <2.6 and the mole ratio C: Si is >0.6 and <2.2, according to a preferred embodiment the coating contains at least 22 and at most 27 atomic percent Si, at least 25 and at most 50 atomic percent O and at least 25 and at most 50 atomic percent C based on its total atomic number without hydrogen and/or fluorine.Type: GrantFiled: June 28, 2002Date of Patent: January 2, 2007Assignee: Fraunhofer Gesellschaft zur Forderung der Angewandten Forschung E.V.Inventors: Klaus D. Vissing, Guido Ellinghorst, Gabriele Neese
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Patent number: 7153179Abstract: An electrical lead assembly for devices such as electrical lamps having a metallic foil for providing an electrically conducting path through a hermetic seal formed by pinch sealing a vitreous material. The metallic foil includes an oxidation-inhibiting coating of silica. In another aspect of the invention, methods of coating metallic foils with silica are disclosed. In yet another aspect of the present invention, an electrical lead assembly for lamps is provided wherein the metallic foil is extended to form an outer electrical lead for the lamp.Type: GrantFiled: November 7, 2003Date of Patent: December 26, 2006Assignee: Advanced Lighting Technologies, Inc.Inventor: Tryggvi Emilsson
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Patent number: 7112453Abstract: This invention provides methods of retentate chromatography for resolving analytes in a sample. The methods involve adsorbing the analytes to a substrate under a plurality of different selectivity conditions, and detecting the analytes retained on the substrate by desorption spectrometry. The methods are useful in biology and medicine, including clinical diagnostics and drug discovery.Type: GrantFiled: August 5, 2002Date of Patent: September 26, 2006Assignee: Ciphergen Biosystems, Inc.Inventors: T. William Hutchens, Tai-Tung Yip
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Patent number: 7101591Abstract: This invention provides a process for producing an organic polymer film whereby when using it as an interlayer insulating film in a semiconductor device, the film exhibits higher adhesiveness at its interfaces where other semiconductor materials are in contact with the lower and the upper surface of the film while an effective dielectric constant in the whole organic polymer film can be further reduced. Specifically, a plurality of organic monomers vaporized is sprayed onto a heated substrate surface via plasma generated in a reaction chamber to form a copolymer film comprising frame composed of a plurality of organic monomer units.Type: GrantFiled: July 1, 2002Date of Patent: September 5, 2006Assignee: NEC CorporationInventors: Yoshihiro Hayashi, Jun Kawahara