Process Or Composition For Sterility Or Package Integrity Test Patents (Class 436/1)
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Patent number: 7390465Abstract: A system and a method to detect biological and chemical agents in a sealed contained at, for example, a mail-processing center. The system includes filtration and vacuum subsystems cooperatively working to draw an air sample from the interior of the particulate containment system for evaluation by a biosensor or chemical analyzer to detect the presence of a contaminant. The vacuum subsystem includes a vacuum generator, flow meters, and pressure regulators to accommodate the varying volume within the particulate containment system. The filtration system includes an inlet filter and a high efficiency particle air filter (HEPA) filter. The inlet filter removes coarse impurities, such as dust and dirt, from the incoming air to improve sensor efficiency. The HEPA removes contaminants from the air sample prior to being released to the surrounding environment, thereby eliminating the possibility of spreading the contamination outside the particulate containment system.Type: GrantFiled: December 23, 2002Date of Patent: June 24, 2008Assignee: Lockheed Martin CorporationInventor: John T. Swider
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Patent number: 7364210Abstract: A tamper-proof seal is disclosed for use in connection with sterilization containers. The seal includes a body portion including a sterilization indicating material and a tongue extending from the body portion. The tongue may be in the form of a laminate consisting of a pair of substantially inert outer layers sandwiching a high shrink inner layer. The tongue is designed to engage the latch mechanism of a sterilization container when the container is in the closed position and the latch mechanism is in a latched position. Upon exposure of the container to sterilization conditions, the tongue shrinks, causing the outer layers to fold upon themselves to form at least one pleat. The container latch mechanism cannot be opened without fracturing the tongue of the seal, thereby providing visible evidence of the latch mechanism being opened.Type: GrantFiled: February 24, 2005Date of Patent: April 29, 2008Assignee: Medin CorporationInventors: Jay D. Schainholz, Eugene Ogman, Amos Shamir
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Publication number: 20080064109Abstract: A game system includes a game apparatus and a controller. The controller is furnished with an acceleration sensor for detecting accelerations in at least two axis directions. Game processing corresponding to the kind of an acceleration input by means of the controller is executed. For determining the kind, reference timing when acceleration in a first-axis direction is below a threshold value to take on a minimum value is detected. Then, it is determined whether or not an angle between acceleration change vectors before and after the reference timing is equal to or more than a predetermined angle. When the angle is not equal to or more than the predetermined angle, it is determined that the acceleration input is an acceleration input in any one of the two-axis directions, and when the angle is equal to or more than the predetermined angle, it is determined that the acceleration input is an acceleration input in a direction including the two-axis directions as components.Type: ApplicationFiled: February 2, 2007Publication date: March 13, 2008Applicant: Nintendo Co., Ltd.Inventor: Yuichiro Okamura
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Patent number: 7334681Abstract: A storable gas inflation/evacuation system and sealing system. The systems are removably connectible to a proximal portion of a guidewire assembly which has an occlusive balloon at a distal portion. The invention includes provision for indicating the presence of oxygen which is undesirable. The storable aspect concerns a sealable container isolating systems components from ambient atmosphere and an oxygen-sensitive material located within the sealable container. The oxygen-sensitive material is initially inactive but activated by exposure to radiation so as to visually change in response to post-radiation oxygen exposure.Type: GrantFiled: January 18, 2007Date of Patent: February 26, 2008Assignee: Possis Medical, Inc.Inventors: Michael J. Bonnette, Eric J. Thor, Mark L. Jenson
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Patent number: 7300770Abstract: An elastomeric article that contains a chromogen that undergoes a detectable change in color in the presence of one or more microbes is provided. For example, in one embodiment, the chromogen is a solvatochromic dye (e.g., Reichardt's dye) that undergoes a color change in the presence of bacteria or other microbes. More specifically, such dyes may respond to differences in polarity between microbe components (e.g., cell membrane, cytoplasm, etc.) and the environment outside the cell. Alternatively, other mechanisms may be wholly or partially responsible for the interaction between the dye and the microbe, such as acid-base reactions, redox reactions, and so forth.Type: GrantFiled: April 28, 2005Date of Patent: November 27, 2007Assignee: Kimberly-Clark Worldwide, Inc.Inventors: Stephanie M. Martin, John Gavin MacDonald, Allison Salyer Bagwell, Jason Lye, Robert B. Johnson
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Patent number: 7300796Abstract: A test environment and an associated method of testing and analyzing a semiconductor package material containing a molding compound, for stability in a sustained oxygen environment. Test samples are exposed to a pressurized gas containing oxygen, under elevated temperature below the glass transition temperature of the molding compound. Control samples are exposed to a pressurized inert gas under similar or more severe conditions of gas pressure, temperature, and humidity. At least one characteristic common to the test samples and the control samples is measured. A determination is made as to whether there exists at least one significant difference between the at least one measured characteristic of the test samples and the control samples.Type: GrantFiled: September 9, 2003Date of Patent: November 27, 2007Assignee: International Business Machines CorporationInventors: Joseph K. V. Comeau, Adele M. Mahoney, Jason P. Ritter, Gerald J. Scilla, Charles H. Wilson
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Publication number: 20070243618Abstract: The present invention provides a system, method and composition for detecting exposure of the contents of a container to one or more gases using a gas sensitive package sensor. The gas sensitive package sensor includes a ruthenium-based luminescence indicator composition having a ruthenium-based luminescence compound having one or more optical properties dispersed within a gas permeable polymer matrix. Exposure to one or more gases modifies the one or more optical properties of the ruthenium-based luminescence compound.Type: ApplicationFiled: April 11, 2006Publication date: October 18, 2007Applicant: OxySense, Inc.Inventors: David Wayne Hatchett, Byron Lee Bennett, Devinder Pal Singh Saini
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Patent number: 7282349Abstract: Solvatochromic dyes are used herein to indicate the presence of bacteria by incorporating them into various substrates such as films, woven and nonwoven fabrics, paper towels, coform and airlaid materials and bonded carded webs. These dyes change color in response to a change in polarity of the environment. Since water is a polar solvent and most bacteria are made from non-polar substances, the presence of bacteria changes the polarity of the environment, triggering a change visible by the unaided eye. A lateral flow device incorporating solvatochromic dyes and a method of detecting bacteria are also included.Type: GrantFiled: December 16, 2003Date of Patent: October 16, 2007Assignee: Kimberly-Clark Worldwide, Inc.Inventors: Jason Lye, John Gavin MacDonald, Ning Wei
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Patent number: 7276380Abstract: The present invention provides a transparent liquid inspection apparatus capable of identifying a boundary between a transparent liquid applied on a base material which provides a multi-piece product and the base material, and automatically inspecting an applied condition of the transparent liquid without influence of a background of the base material. A projected image of an illumination source (2) is reflected on a surface of the transparent liquid as a mirror, the projected image is picked up by cameras (41 to 44), and the image is analyzed by an image processing unit (8), thereby inspecting an amount of displacement of the transparent liquid from a predetermined application position and expansion of the surface of the transparent liquid.Type: GrantFiled: July 30, 2001Date of Patent: October 2, 2007Assignee: Matsushita Electric Industrial Co., Ltd.Inventor: Teruaki Fukuyama
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Patent number: 7247482Abstract: A sterilization process challenge device has a sterilization indicator contained within a container; and a variable diffusion restriction into said container.Type: GrantFiled: June 28, 2006Date of Patent: July 24, 2007Assignee: Ethicon, Inc.Inventors: Anthony Lemus, Debra Timm
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Publication number: 20070160493Abstract: Apparatus for treating allografts, having a sonication tank configured to transmit ultrasonic energy to the interior of the tank; a treatment canister rotatably positioned in said sonication tank, and configured to receive allografts therein; and a treatment fluid source in fluid communication with said treatment canister. Methods of treating allografts and methods for determining microbial contamination using the apparatus.Type: ApplicationFiled: November 7, 2006Publication date: July 12, 2007Applicant: ALLOSOURCEInventors: Chad J. Ronholdt, Simon Bogdansky, Alan Hooks
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Patent number: 7205152Abstract: A self-contained closed loop system and method for detecting contaminants in, on, and around objects. The system includes an air duct subsystem connecting at least one sensor to a sealed housing containing a rotating container. Air from the sealed housing is circulated past a sensor to detect, for example, biological or chemical contaminants. If a contaminant is detected, an indicator is set and a contaminant neutralizer is optionally injected into the air duct subsystem.Type: GrantFiled: July 22, 2002Date of Patent: April 17, 2007Assignee: Lockheed Martin CorporationInventor: John T. Swider
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Patent number: 7189355Abstract: The present invention relates to a chemical indicator that is used to determine whether instruments and other products to be sterilized have experienced a sterilization treatment process or to confirm whether sterilization has been efficiently performed, by the color tone change of the indicator when sterilizing medical instruments and other products and the like by a hydrogen peroxide low temperature plasma sterilizing method. The present invention provides an indicator for plasma sterilization, wherein an ink comprising a colorless chromogenic pigment, a coloring assistant, a binder (a binding agent) and a solvent for dissolving these, is applied to or printed on a base material, and wherein a color tone change of the indicator occurs by a hydrogen peroxide low temperature sterilization method.Type: GrantFiled: June 15, 2001Date of Patent: March 13, 2007Inventors: Masao Mikumo, Kenji Kazama, Yoshio Jo
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Patent number: 7186373Abstract: A method and apparatus for sensing the concentration of a gaseous sterilant in a sealable enclosure. An indicator is provided that has a chemistry such that the indicator changes color when exposed to vaporized hydrogen peroxide (VHP). The chemistry is adapted to react when exposed to a specific minimum concentration of vaporized hydrogen peroxide for a specific minimum period of time. In this manner, it can be visually determined whether articles (e.g., medical instruments and like devices) located within the sealable enclosure have been exposed to a minimum threshold of vaporized hydrogen peroxide.Type: GrantFiled: July 22, 2003Date of Patent: March 6, 2007Assignee: Steris Inc.Inventor: Michael A. Centanni
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Patent number: 7176030Abstract: A disposable medical item for use with medical equipment includes circuitry forming an electrical path between the item and medical equipment. The circuitry is coupled to a medical equipment controller or independent microprocessor and includes a fuse. The controller transmits a status signal over the path in response to the equipment receiving the item. A disabled fuse prevents traversal of the path by the status signal, thereby indicating prior item use. If the controller does not detect the status signal, medical equipment operation is disabled. Otherwise, the controller transmits over the path a signal sufficient to disable the fuse to indicate item use and verifies the disabled fuse status. If the disabled fuse status is verified, the controller enables equipment operation. The controller periodically checks the fuse status during equipment operation and disables operation in response to a prior used item inserted into the medical equipment.Type: GrantFiled: June 17, 2002Date of Patent: February 13, 2007Assignee: O.R. Solutions, Inc.Inventors: Durward Faries, Jr., Bruce Heymann, David Hendrix
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Patent number: 7157048Abstract: The present invention relates to a contamination detector associated with a double bar code that includes coded indicia used to identify the presence of conditions indicative of microbial contamination, including toxic contaminants, bacterial metabolites, and other microbial secretions. Of the two bar code symbols associated with the contamination detector, the first identifies the product or container, while the second bar code symbol is designed to identify the presence of contaminants. When contamination is not detected, the first bar code symbol is scanner readable, whereas the second bar code symbol is not. Once contamination is detected, bars in both bar code symbols can appear or disappear causing the first bar code symbol to become scanner unreadable and the second bar code symbol to become scanner readable.Type: GrantFiled: February 11, 2003Date of Patent: January 2, 2007Assignee: Sira Technologies, Inc.Inventors: Robert M. Goldsmith, Catherine H. Goldsmith, James G. Woodaman
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Patent number: 7156597Abstract: A dual bar code for detecting contamination. When no contamination is present, a first bar code identifies the product. When contamination is present a second bar code identifies the presence of contaminants.Type: GrantFiled: February 11, 2003Date of Patent: January 2, 2007Assignee: SIRA Technologies, Inc.Inventors: Robert M. Goldsmith, Catherine H. Goldsmith, James G. Woodaman
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Patent number: 7148066Abstract: Systems and methods providing for the introduction of a dye, particularly a xanthene dye, and more particularly a rhodamine dye, to liquid anhydrous ammonia to discourage theft of the anhydrous ammonia and provide for leak detection in storage vessels. The dye will stain objects which come into contact with the liquid anhydrous ammonia allowing for the detection of such contact. Generally, the staining will be visible to the naked eye, but may also fluoresce when exposed to a particular light source such as ultra violet (UV) light.Type: GrantFiled: August 2, 2004Date of Patent: December 12, 2006Assignee: GloTell Products, Inc.Inventors: Tim Bickett, Frank Eiter
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Patent number: 7141214Abstract: Water-based chemical indicator inks for ethylene oxide sterilization processes and methods for its use. The chemical indicator ink contains at least one pH indicator dye selected from the group consisting of Bromocresol green, Bromophenol blue, Methyl red, Ethyl orange, and combinations thereof. The pH indicator dye undergoes an irreversible color change when exposed to ethylene oxide vapor in the presence of low-temperature steam, but when exposed to other sterilization processes either does not undergo a color change or undergoes a color change that is different than is obtained when exposed to ethylene oxide.Type: GrantFiled: June 29, 2004Date of Patent: November 28, 2006Assignee: Illinois Tool Works Inc.Inventor: Shobha Shakher Puntambekar
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Patent number: 7118857Abstract: Methods and compositions for detection of microbial contaminants in peritoneal dialysis solutions are provided. The methods and compositions employ modified bioburden testing and the detection of peptidoglycan. A novel cause of aseptic peritonitis is provided—aseptic peritonitis associated with gram positive microbial contamination of a dialysis solution. Peptidoglycan is a major component of a gram positive bacterial cell wall and thus can serve as a marker for gram positive bacteria. In this regard, testing for peptidoglycans can be utilized to effectively prevent peritonitis in patients that use the peritoneal dialysis solutions, such as peritoneal dialysis solutions that contain a glucose polymer including an icodextrin and the like.Type: GrantFiled: February 27, 2004Date of Patent: October 10, 2006Assignees: Baxter International Inc., Baxter Healthcare S.A.Inventors: Leo Martis, Mehul Patel, Joseph A. Giertych, James W. Mongoven, Jacqueline A. Kunzler, William F. Owen, Jr.
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Patent number: 7105350Abstract: A method for evaluating the integrity of the closure on a hot-filled container in which the hot-filled container is subjected to a pressurized spray of cooling medium, including the step of providing a cooling medium having an effective amount of a fluorescing dye contained therein, is provided. The sealed container then is sprayed with the cooling liquid. After the container has exited the cooling portion of the filling and sealing operation, the container is subjected to ultraviolet light to activate any fluorescing dye which may have migrated past the closure into the interior of the container. The container is then viewed to determine the presence or absence of activated dye.Type: GrantFiled: August 30, 2002Date of Patent: September 12, 2006Assignee: Tropicana Products, Inc.Inventors: Tammy Foster, Tammy Svoboda
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Patent number: 7091042Abstract: A sterilization process challenge device has a sterilization indicator contained within a container; and a variable diffusion restriction into said container.Type: GrantFiled: November 2, 2001Date of Patent: August 15, 2006Assignee: Ethicon, Inc.Inventors: Anthony Lemus, Debra Timm
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Patent number: 6936223Abstract: A chemical indicator of an aurin moiety in a substrate to detect the presence of an oxidizing agent.Type: GrantFiled: March 28, 2002Date of Patent: August 30, 2005Assignee: Ethicon, Inc.Inventors: Thomas G. Lippold, Nitu Kohli, Pascale D. Endo, Henry K. Hui, Szu-Min Lin
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Patent number: 6924147Abstract: A polymeric food spoilage sensor comprises a polymer containing a polyazamacrocyclic transition metal complex. The complex selectively binds biogenic amines, such as cadaverine, putrescine and histamine, which are released by food spoilage microorganisms. The polymer undergoes a detectable color change upon exposure to biogenic amine, thus indicating that food spoilage has probably occurred. In one embodiment, the polymer is molecularly imprinted with the biogenic amine to impart selective binding affinity. The polymer is easily incorporated in common food containers and can be employed in fiber optic detection devices.Type: GrantFiled: July 15, 2003Date of Patent: August 2, 2005Assignee: The Johns Hopkins UniversityInventors: Craig A. Kelly, George M. Murray, O. Manuel Uy
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Patent number: 6895340Abstract: An analytical method and apparatus using principal component analysis of nuclear magnetic resonance (NMR) data for rapid molecular structure/function pattern recognition. The presence of a molecular substructure in an organic compound is determined by comparing principal components calculated from chemical shift values of the substructure in selected compounds with those calculated from the chemical shift values of the organic compound. Alternatively, principal components are calculated from the intensities of NMR signals for a full spectrum, or selected regions thereof, to determine whether an organic compound belongs to or is excluded from a set of structurally related compounds. Also, the presence of a pharmacophore in an organic compound can be determined by comparing the principal components derived from data on a set of compounds known to bind to a particular receptor, or have a common biological effect, with the principal components of the data set of the organic compound.Type: GrantFiled: April 11, 2002Date of Patent: May 17, 2005Assignee: Bristol-Myers Squibb CompanyInventors: Feng Xu, Steven E. Klohr, David Detlefsen
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Patent number: 6884394Abstract: A reader for a sterilization indicator having sterilizing agent sensitive indicia is described. The indicator allows a sterilization cycle to be monitored without the need for a user to subjectively distinguish between color, quality or intensity of display patterns.Type: GrantFiled: August 5, 1999Date of Patent: April 26, 2005Assignee: 3M Innovative Properties CompanyInventors: Rodney K. Hehenberger, Phillip A. Bolea, Bernard A. Gonzalez
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Patent number: 6867044Abstract: A method and system for detecting chemical or biological hazards in items is provided. A plurality of incoming mail mailboxes each include a sampler to sample air from a letter that is tested using a first sensor. Source information corresponding to hazard flagged mail pieces is utilized to block mail from that source at other mailboxes.Type: GrantFiled: December 19, 2001Date of Patent: March 15, 2005Assignee: Pitney Bowes Inc.Inventors: Robert A. Cordery, Karin A. Russo, Ronald P. Sansone
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Patent number: 6852539Abstract: A contaminant detection system for mail is provided. A tray of mailpieces is transported along a transport path into a chamber that has a negative pressure maintained by a vacuum system. The tray of mail enters the chamber and is quickly decelerated, such as, for example, by hitting a stop. The quick deceleration compresses the mailpieces in the tray, thereby ejecting air, dust and other particles from the mailpieces into the surrounding environment inside of the chamber. The vacuum system draws the ejected air, dust and other particles into a sampling system that monitors for the presence of a possible biohazard. If any type of contaminant is found in the ejected air, dust and other particles, the tray can be held for further investigation of the mailpieces. If no contaminants are detected, the tray is accepted and the mailpieces are further processed.Type: GrantFiled: December 18, 2001Date of Patent: February 8, 2005Assignee: Pitney Bowes Inc.Inventors: Robert A. Cordery, Pushpavadan S. Nagarsheth, Joseph E. Wall
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Publication number: 20040265170Abstract: The present invention provides a hydrogen peroxide indicator that includes a substrate on which is disposed an indicator composition that includes at least one of a select group of colorants. As a result of contact with hydrogen peroxide, the colorants change color, and even become colorless, thereby providing an indication of the presence of hydrogen peroxide.Type: ApplicationFiled: July 14, 2004Publication date: December 30, 2004Applicant: 3M Innovative Properties CompanyInventor: David M. Read
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Publication number: 20040241862Abstract: Water-based chemical indicator inks for ethylene oxide sterilization processes and methods for its use. The chemical indicator ink contains at least one pH indicator dye selected from the group consisting of Bromocresol green, Bromophenol blue, Methyl red, Ethyl orange, and combinations thereof. The pH indicator dye undergoes an irreversible color change when exposed to ethylene oxide vapor in the presence of low-temperature steam, but when exposed to other sterilization processes either does not undergo a color change or undergoes a color change that is different than is obtained when exposed to ethylene oxide.Type: ApplicationFiled: June 29, 2004Publication date: December 2, 2004Inventor: Shobha Shakher Puntambekar
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Patent number: 6815206Abstract: A sterilization system uses a sterilization process monitoring device which is capable of indicating the efficacy of the sterilization process. To enhance accuracy of the monitoring function, the monitoring device is located in such a fashion that an antimicrobial agent used in the process can only reach the monitor through an area containing the article to be sterilized.Type: GrantFiled: December 21, 2000Date of Patent: November 9, 2004Assignee: Ethicon, Inc.Inventors: Szu-Min Lin, Su-Syin Wu
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Patent number: 6794191Abstract: There is disclosed a process for melting a luminescent oxygen sensitive compound into extruded polymer films. Specifically, there is disclosed a process for thermal melting of oxygen-sensitive indicators into common packaging polymers used for commercial packaging of products, such as foods. The oxygen-sensitive indicators can be used for real-time monitoring of oxygen in commercial packaging operations.Type: GrantFiled: June 25, 2001Date of Patent: September 21, 2004Assignee: Photonic SystemsInventors: David L. Putnam, Todd Hubbard
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Patent number: 6790411Abstract: The present invention provides a hydrogen peroxide indicator that includes a substrate on which is disposed an indicator composition that includes at least one of a select group of colorants. As a result of contact with hydrogen peroxide, the colorants change color, and even become colorless, thereby providing an indication of the presence of hydrogen peroxide.Type: GrantFiled: December 2, 1999Date of Patent: September 14, 2004Assignee: 3M Innovative Properties CompanyInventor: David M. Read
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Patent number: 6749807Abstract: A single-use cartridge C contains a dose of a concentrated decontaminant for providing a decontaminant solution upon mixing with water. The cartridge is inserted into the well (16) of a decontamination system (A). Fresh water and then the decontaminant solution are recirculated through the well during a decontamination cycle. The cartridge includes a porous region (42), through which the decontaminant solution flows. Impregnated in the porous region is a chemical indicator (44), such as crystal violet, which gradually changes color on exposure to the decontaminant. The indicator provides a semi-quantitative indication of the integrated level of the decontaminant in the solution over time for determining whether an acceptable level of the decontaminant was present for decontamination. A preferred embodiment of the cartridge C includes nested inner and outer water-penetrable cups (50,150,70,170) for holding first and second reagents. The two cups are sealed together adjacent upper open ends (56,92,156,192).Type: GrantFiled: May 19, 1999Date of Patent: June 15, 2004Assignee: Steris CorporationInventors: Brian E. Schindly, Christopher M. Fricker, George E. Grignol
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Patent number: 6737274Abstract: A comparator for use with a time-temperature indicator wherein the time-temperature indicator includes an active portion having an initial color and which undergoes chemical changes as time elapses and at a rate related to the temperature of the surrounding environment and wherein the chemical changes produce changes in the color of the active portion. The comparator comprises a substantially planar support member, and a plurality of comparator stages located on the support member. Each comparator stage comprises a first portion having a reference color and a second portion having a predetermined color that is the same as one of the colors to which the active portion of the time-temperature indicator changes.Type: GrantFiled: February 4, 1999Date of Patent: May 18, 2004Assignee: United States of America as represented by the Secretary of the ArmyInventor: Bruce Butler Wright
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Publication number: 20040092022Abstract: The invention is a measuring device for detecting temperature-dependent measured values or temperature-dependent combinations of physical influencing factors, in particular for measuring temperatures in sterilizing apparatus, with at least one measuring mechanism.Type: ApplicationFiled: September 15, 2003Publication date: May 13, 2004Inventor: Albert Bosch
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Publication number: 20040043492Abstract: A method for evaluating the integrity of the closure on a hot-filled container in which the hot-filled container is subjected to a pressurized spray of cooling medium, including the step of providing a cooling medium having an effective amount of a fluorescing dye contained therein, is provided. The sealed container then is sprayed with the cooling liquid. After the container has exited the cooling portion of the filling and sealing operation, the container is subjected to ultra violet light to activate any fluorescing dye which may have migrated past the closure into the interior of the container. The container is than viewed to determine the presence or absence of activated dye.Type: ApplicationFiled: August 30, 2002Publication date: March 4, 2004Inventors: Tammy Foster, Tammy Svoboda
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Publication number: 20040037741Abstract: The predicting of behavious such as spring back of a moulded composite component (22) made from fibre and resin materials (13, 14) comprises, determining the temperature at which the resin (14) passes from a liquid state to a solid state, constructing a finite element model, producing from the fibre and resin a plurality of elements E1 to En smaller than the required component (22) determining for each element E1 to En at different temperatures the difference between variation in size caused thermally and variation in size caused chemically, taking the information obtained and adjusting the finite element model in response thereto, to enable a coefficient of thermal expansion to be determined, and using the finite element model (26) to provide an indication of the behaviour of the cured moulded composite component (21) on being removed from a mould (28).Type: ApplicationFiled: March 20, 2003Publication date: February 26, 2004Inventor: Herve Barrellon
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Patent number: 6696296Abstract: This invention discloses a method for detecting a leak from a sealed optical device. The method includes steps of: A) injecting a target gas with no performance interference to the sealed optical device for leak detection followed by sealing the sealed optical device. B) placing the sealed device in a leak testing chamber and measuring a background level of the target gas in the leak testing chamber. C) heating the sealed device to a gas-expelling temperature for expelling the target gas from the leak in the sealed optical device. And, D) detecting the target gas in a one-part-per million (PPM) range in the leak-detecting chamber for an comparing with the background level of the target gas for determining the leak in the sealed optical device.Type: GrantFiled: March 5, 2001Date of Patent: February 24, 2004Assignee: Oplink Communications, Inc.Inventors: Jason Li, Steven Guoxin Zhu
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Publication number: 20040023397Abstract: A method of authenticating products or packaging by analyzing key ingredients on products or on product packaging is disclosed. Light-sensitive compounds can be used to identify the product or product packaging. The product or product package may include visible or invisible ink containing a particular light-sensitive compound. One or more light-sensitive compounds and ink, if used, may be printed in one or more locations on the product or product packaging to produce an authentication mark to inhibit inadvertent or intentional removal of the mark, thereby rendering the mark tamper-resistant. The mark is sealed to isolate the mark from the environment. A device may be used to irradiate the mark and read light absorption or emission. A controller determines the authenticity of the mark by comparing the emitted or absorbed properties to a standard.Type: ApplicationFiled: August 5, 2002Publication date: February 5, 2004Inventors: Rakesh Vig, Anthony Angelo Saglimbeni
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Patent number: 6676901Abstract: The present invention provides an oxygen indicator comprising: an oxygen indicating agent including a substrate and an oxygen indicator composition fixed at the surface of the substrate; and a single-sided self-adhesive plastic member having a self-adhesive layer on one side thereof, wherein the oxygen indicating agent is provided over the single-sided sedlf-adhesive plastic member by causing the oxygen indicator composition to closely contact the self-adhesive layer. Moreover, this invention provides a deoxidizer package with an oxygen indicating function, to which the oxygen indicator is pasted. This invention further provides a method and apparatus for fixing the oxygen indicator to an object.Type: GrantFiled: June 2, 2000Date of Patent: January 13, 2004Assignee: Mitsubishi Gas Chemical Company, Inc.Inventors: Hidetoshi Hatakeyama, Shigeo Tobari, Shigeharu Iwauchi, Masahiko Ohsawa
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Patent number: 6656429Abstract: A test pack for testing the adequacy of air removal in a prevacuum sterilizer.Type: GrantFiled: November 19, 1999Date of Patent: December 2, 2003Assignee: Propper Manufacturing Co., Inc.Inventor: John D. Dyckman
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Publication number: 20030207453Abstract: A sterilization monitor includes a substrate and an monitor composition. The monitor composition contains a colorant and a halogen source and undergoes a distinct color change when exposed to a peracid. The sterilization monitor can be used to monitor a sterilization process involving a peracid. A sterilization monitoring device, including a sterilization monitor enclosed in a housing having a vapor permeable barrier, can also be used to monitor a sterilization process.Type: ApplicationFiled: August 2, 2001Publication date: November 6, 2003Applicant: Minnesota Mining and Manufacturing Company, a Minnesota corporationInventors: Ramon T. Ignacio, Allan P. Piechowski
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Publication number: 20030199095Abstract: An ink composition for sensing carbon dioxide gas contains a pH indicator formed using a combination of two or more types of pH indicator components, binder, and solvent and allows easy visual observation of color changes of an indicating portion caused by the concentration of carbon dioxide gas. When the ink composition is applied to a carbon dioxide indicator and package, a pinhole and poor seal of a carbon-dioxide-ambient package are easily found.Type: ApplicationFiled: June 14, 2002Publication date: October 23, 2003Inventors: Kohei Yuyama, Minoru Oka, Hiroshi Honda, Shin Hamazaki, Shinya Ochiai, Noe Obinata, Hiroyuki Mizuma
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Patent number: 6630352Abstract: A sterilant challenge device (1), for use in testing the efficiency of the air removal stage of a sterilization cycle in a sterilizer, includes a tube (2) of thermally-insulating material, the bore of which is closed at one end (3) and open at the other for the entry of sterilant. A plurality of thermally-conductive masses (4) is located around the tube (2) and thermally-separated from one another by air gaps (14), and a temperature sensor is located in an opening (16) in one of the masses adjacent the closed end of the tube. An outer casing (5) defines an air space around the thermally-conductive masses and thermally insulates the masses from the heat in the sterilizer.Type: GrantFiled: March 28, 2001Date of Patent: October 7, 2003Assignee: 3M Innovative Properties CompanyInventors: Hackler Reiner, Robbert-Jan Hermsen, Wolfgang Kaps
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Publication number: 20030185706Abstract: A device for monitoring the expiration of goods includes a substrate and an unreacted composition affixed thereto which is intrinsically reactive to one or both of its thermal environment and the length of time following activation. The reactivity results in a color formation of the composition with the color formation being a single color upon reaction to one of said thermal environment or length of time and multiple colors upon reaction to both. The device may be a label affixed to a container containing the goods to be monitored or may be printed directly on a container.Type: ApplicationFiled: August 23, 2002Publication date: October 2, 2003Inventor: Hans O. Ribi
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Patent number: 6627443Abstract: The present invention relates to new color compositions which are especially suitable to be used in oxygen indicators. The compositions comprise iron(II), an agent containing pyrogallol entities and an organic acid.Type: GrantFiled: April 27, 2000Date of Patent: September 30, 2003Assignee: Fresenius Kabi ABInventors: Åke Stenholm, Lars Karlsson, Anders Löfgren, Bo Nystrom, Otto Skolling
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Publication number: 20030170901Abstract: A electronic system for tracking and monitoring articles to be subjected to a sterilization cycle is disclosed. The method uses a sterilization indicator and electronically links sterilization information with the articles subjected to the sterilization process. The indicator allows a sterilization cycle to be monitored without the need for a user to subjectively distinguish between color, quality or intensity of display patterns.Type: ApplicationFiled: November 25, 2002Publication date: September 11, 2003Applicant: 3M Innovative Properties CompanyInventors: Roland C. Kippenhan, Steven S. Kirckof, Philip A. Bolea, Richard M. Rumble, Rodney K. Hehenberger, Ramon T. Ignacio
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Publication number: 20030153085Abstract: A system and method for sorting of objects that includes a pathway network that has a plurality of pathways and one or more branch points. A fluid composition including one or more objects can be transported through the pathway network, where one or more of the objects are analyzed and sorted at one or more branch points based on the analysis of the objects.Type: ApplicationFiled: January 10, 2003Publication date: August 14, 2003Applicant: NeuroBioTexInventors: James F. Leary, Christopher J. Frederickson
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Patent number: 6596542Abstract: A chemical actinometer for determining the absolute level of exposure to ultraviolet light of a fluid to be treated for disinfection purposes. The actinometer includes a translucent sample cell through which the chemical actinometric fluid flows. The area of exposure of the actinometric fluid is controlled by allowing the ultraviolet light to pass through only a portion of the sample cell. A suitable actinometric fluid is a combination of iodide and iodate in a solution. The sample cell is positioned within an ultraviolet disinfection reactor at a position to receive ultraviolet light from the ultraviolet light source.Type: GrantFiled: January 8, 2001Date of Patent: July 22, 2003Inventor: Christopher R. Schulz