Organic Solvent Extraction Patents (Class 554/12)
  • Patent number: 5739364
    Abstract: A method for removal of selected substances from carbonaceous material by use of a solvent is provided comprising: (a) introducing the carbonaceous material containing the selected substances into an extraction zone to form a bed; (b) introducing a gas which at a given pressure liquifies at a higher temperature than the solvent, the introduction being made under a pressure and at a temperature to cause the temperature and pressure of the extraction zone to be sufficient to cause the solvent to liquify when the solvent is introduced to the extraction zone; (c) introducing into the extraction zone the solvent capable of extracting the selected substance; (d) passing the solvent through the bed of carbonaceous material to extract the substances from the material; (e) removing the resulting substance/solvent mixture from the extraction zone to a separation zone under conditions which will maintain the solvent in liquid form as it is passed through the bed of carbonaceous material and out of the extraction zone to
    Type: Grant
    Filed: June 10, 1996
    Date of Patent: April 14, 1998
    Assignee: University Research & Marketing
    Inventor: Henry L. Franke
  • Patent number: 5728851
    Abstract: A process for removing fats and oils from prepared animal-derived fried-derived food products, particularly fried meat, poultry, and fish products. The method involves treating the animal-derived fried-derived food product with a normally gaseous solvent at effective temperatures and pressures.
    Type: Grant
    Filed: April 21, 1995
    Date of Patent: March 17, 1998
    Assignee: University Research & Marketing
    Inventor: Henry L. Franke
  • Patent number: 5707673
    Abstract: In a solvent extraction process for the extraction of an extractive from extractive-containing material employing in an extraction zone operating under extraction conditions a process solvent, whereby a miscella comprising a portion of the process solvent and a portion of the extractive, and an extractive-depleted substrate is formed, the improvement to which comprises: (a) removing the miscella from the extraction zone under extraction conditions, (b) filtering the miscella by use of a microfiltration, an ultrafiltration, a nanofiltration, or a reverse osmosis membrane, under conditions which achieve a differential pressure across said membrane, to separate the solvent in the miscella from the extractive in the miscella, and (c) recycling under extraction conditions at least a portion of the separated solvent to the extraction zone.
    Type: Grant
    Filed: October 4, 1996
    Date of Patent: January 13, 1998
    Assignee: PreWell Industries, L.L.C.
    Inventors: John E. Prevost, Robert D. Clay, John R. Fielding
  • Patent number: 5672371
    Abstract: The resinous fraction comprising toxic p-coumaric acid derivatives is extracted from jojoba press-cake by means of an apolar mixture of solvents which mixture is a selective eluter for said p-coumaric acid derivatives. Particularly the extraction is performed with a mixture of acetone and hexane comprising up to 70 vol. % acetone or with a mixture of methyl ethyl ketone and hexane comprising up to 80 vol. % methyl ethyl ketone.
    Type: Grant
    Filed: November 17, 1995
    Date of Patent: September 30, 1997
    Inventor: Andre d'Oosterlynck
  • Patent number: 5663374
    Abstract: The invention discloses novel triterpene derivatives of azadirachtin of the formulae 2 to 11 of the drawings and a process for isolating new triterpene derivatives of azadirachtin from the various parts of the neem plant(Azadirachta indica A-Juss), which process comprises grinding the parts of the neem plant to get a powder, extracting the powder with a binary immiscible solvent consisting of one polar and another non-polar solvent in a ratio of 1:2 to obtain an extract, filtering the extract to get a filtrate having two layers, one layer containing lipids and the other layer containing the new triterpene derivatives of azadirachtin and water soluble constituents including sugars, separating the layers by known methods, concentrating the layer containing the new triterpenes of the formulae 2-11 including derivatives of azadirachtin and water soluble salts, treating the resultant concentrate with a polar solvent and if necessary, warm the concentrate having the solvent, and filtering/decanting the resultant so
    Type: Grant
    Filed: January 11, 1996
    Date of Patent: September 2, 1997
    Assignee: Council of Scientific & Industrial Research
    Inventors: Bhimsen Annacharya Nagasampagi, Supada Rambhau Rojatkar, Mandakini Moreshwar Kulkarni, Vimal Shantaram Joshi, Vidya Sudhir Bhat, Mukund Gangadhar Sane, Nagaraj Ramanuj Ayyangar
  • Patent number: 5599376
    Abstract: A process for recovering edible oil and bleaching clay from an edible oil-bleaching clay waste stream and for recovering edible oil and nickel catalyst from a hydrogenated edible oil-nickel catalyst-filter aid waste stream; the recovered bleaching clay may be reused directly and the recovered nickel catalyst and filter aid mixture is pelletized for metallurgical nickel recovery.
    Type: Grant
    Filed: November 27, 1995
    Date of Patent: February 4, 1997
    Inventor: John D. Camp
  • Patent number: 5525746
    Abstract: An improved low temperature process for extracting oil from oil-bearing materials by extracting the oil-bearing material in an extraction zone with a normally gaseous solvent selected from propane, butane, and mixtures thereof. As the resulting solvent/oil mixture is passed through the bed of extracted oil-bearing material, from the extraction zone, and to a separation zone, it is done so under conditions that will maintain the solvent in liquid form. The resulting extracted materials have substantially more of their protein and vitamin value intact when compared with similar materials extracted by more conventional high temperature methods. The present process is also a lower energy consuming process than more conventional, extractive processes.
    Type: Grant
    Filed: June 30, 1994
    Date of Patent: June 11, 1996
    Assignee: Univesity Research & Marketing Inc.
    Inventor: Henry L. Franke
  • Patent number: 5516923
    Abstract: The invention relates to a process for extracting oil from an oil bearing plant material with the use of a solvent suitable for dissolving the oil in the plant material. Grounded plant material is deposited into a reactor vessel, and vacuum is created in the reactor vessel. Liquid solvent is introduced into the reactor vessel and allowed to contact the plant material for a time sufficient to dissolve oil from the plant material, while the temperature in the reactor vessel is maintained at a level which prevents denaturing of constituent components of the plant oil and the plant material. Additional solvent vapors are introduced into the bottom of the reactor to cause mixing of the plant material and the solvent and separate fine particulate matter from heavier particles. Pressurized heated solvent vapors are introduced into the top of the reactor vessel while the liquid solvent and oil combination is being removed from the bottom of the reactor vessel through filters.
    Type: Grant
    Filed: April 5, 1994
    Date of Patent: May 14, 1996
    Assignee: Agritech International
    Inventors: Roland M. Hebert, Robert J. Stonicher, Robert T. Tucker
  • Patent number: 5444089
    Abstract: The present invention provides anti-tumor neutral lipids of the endosperm of Job's tears (Coix lachrymajobi), a method to extract and refine it from the endosperm of Job's tears and a pharmaceutical composition containing the neutral lipids. The neutral lipids of the endosperm of Job's Tears and its pharmaceutical composition are indicated for anti-tumor effect, enhancement of immunity and protection from many diseases.
    Type: Grant
    Filed: September 14, 1993
    Date of Patent: August 22, 1995
    Assignees: Da P. Li, Zhejiang Provincial Hospital of Traditional Chinese Medicine
    Inventor: Da P. Li
  • Patent number: 5290959
    Abstract: An extraction process comprising contracting a material to be extracted with an extracting fluid at elevated pressure within a defined space, and separating the extracted fluid and extract as a mass, from the extracted material while reducing the volume of the defined space and while maintaining the elevated pressure within the defined space. Apparatus for carrying out the process is adapted to separate the extracting fluid and the extract, as a mass, from the extracted material, while maintaining elevated pressure and reducing the volume as the point of separation.
    Type: Grant
    Filed: February 21, 1992
    Date of Patent: March 1, 1994
    Assignee: Vitamins, Inc.
    Inventor: Wayne K. Rice
  • Patent number: 5281732
    Abstract: An improved low temperature process for extracting oil from oil-bearing materials by extracting the oil-bearing material in an extraction zone with a normally gaseous solvent selected from propane, butane, and mixtures thereof. As the resulting solvent/oil mixture is passed through the bed of extracted oil-bearing material, from the extraction zone, and to a separation zone, it is done so under conditions that will maintain the solvent in liquid form. The resulting extracted materials have substantially more of their protein and vitamin value intact when compared with similar materials extracted by more conventional high temperature methods. The present process is also a lower energy consuming process than more conventional, extractive processes.
    Type: Grant
    Filed: December 31, 1991
    Date of Patent: January 25, 1994
    Assignee: University Research & Marketing
    Inventor: Henry L. Franke
  • Patent number: 5278325
    Abstract: A vegetable oil process and assembly is disclosed for extracting oil from an oil bearing material such as soybean, corn and the like. The process comprises adding at least one reagent to the oil bearing material to form a slurry mixture. The slurry is heated at a preselected temperature for a preselected period of time preferably under a partial vacuum. This processing reduces the phospholipid and trace metal content in the oil extracted from the oil heating material. The oil product produced is light in color, shows no turbidity and exhibits minimal amount of phosphorus, calcium, magnesium and iron. The oil is ready for physical refining.
    Type: Grant
    Filed: July 30, 1990
    Date of Patent: January 11, 1994
    Inventors: Hans R. Strop, Richard R. Perry
  • Patent number: 5182406
    Abstract: The process for recovering vegetable oleaginous substances from oil-containing natural substances comprises a series of continuous combined pressing and extraction steps to increase and simultaneously to guarantee a high quality product for different kinds of natural substance starting materials. This is accomplished by subjecting the natural substances, conditioned and comminuted if necessary, after mixing with a solvent phase containing some oil to an intensive processing, mixing and extraction in the shear field of at least one rotor-stator unit and subsequently feeding the resulting liquid phase, through a filter if necessary, to a distillation column. The solid phase is extracted in successive stages until a residual oil content of 1% is reached and the solvent is fed back to a solid phase in a counterflow. The process as defined in my invention is universally applicable to all fat and oil-containing natural substances using suitable fluid extraction means.
    Type: Grant
    Filed: April 5, 1991
    Date of Patent: January 26, 1993
    Assignee: Dorr-Oliver Deutschland GmbH
    Inventor: Hubert Coenen
  • Patent number: 5166376
    Abstract: A process for refining vegetable oil from a miscella obtained by extraction of vegetable seeds with an organic solvent, which comprises permeating the miscella through an ultrafilter made of an inorganic microporous membrane having a pore size of from 30 to 100 .ANG. in a state heated at a temperature of from 50.degree. to 120.degree. C. to remove impurities contained in the miscella.
    Type: Grant
    Filed: September 26, 1991
    Date of Patent: November 24, 1992
    Assignees: Mitsubishi Kakoki Kaisha Ltd., Toto Ltd.
    Inventors: Shigemi Suzuki, Nobuyuki Maebashi, Shigeru Yamano, Hiashi Nogaki, Akio Tamaki, Akiteru Noguchi