Halogen Containing Phase (e.g., Crystalline Or Noncrystalline, Etc.) Patents (Class 65/33.3)
-
Patent number: 11332377Abstract: A method for producing a polycrystalline silicon processed article includes removing a polycrystalline silicon rod, obtained by precipitating polycrystalline silicon on a silicon core wire held by a carbon member connected to an electrode in a reactor by the Siemens method, in a state in which the carbon member is included at the end portion thereof and processing the polycrystalline silicon rod. The polycrystalline silicon rod is detached from the electrode and the carbon member present on the end portion of the polycrystalline silicon rod is covered using a covering material until the processing, whereby the polycrystalline silicon rod and the carbon member are handled in a separated state.Type: GrantFiled: March 7, 2018Date of Patent: May 17, 2022Assignee: Tokuyama CorporationInventor: Ayao Akiyoshi
-
Patent number: 10273183Abstract: A soda-lime-silica glass-ceramic article having an amorphous matrix phase and a crystalline phase is disclosed along with a method of manufacturing a soda-lime-silica glass-ceramic article from a parent glass composition comprising 47-63 mol % SiO2, 15-22 mol % Na2O, and 18-36 mol % CaO. The crystalline phase of the glass-ceramic article has a higher concentration of sodium (Na) than that of the amorphous matrix phase.Type: GrantFiled: July 14, 2017Date of Patent: April 30, 2019Assignee: Owens-Brockway Glass Container Inc.Inventors: Scott P Cooper, Samuel Schuver, Carol A Click
-
Patent number: 9896376Abstract: A bonded ceramic component which is resistant to reactive halogen-containing plasmas, said component comprising ceramic portions which are bonded together by a bonding material which includes an oxyfluoride glass-ceramic-comprising transition area between interfaces of the ceramic portions, where the transition area includes from at least 0.1 volume % amorphous phase up to about 50 volume % amorphous phase.Type: GrantFiled: September 8, 2014Date of Patent: February 20, 2018Assignee: APPLIED MATERIALS, INC.Inventors: Jennifer Y. Sun, Ren-Guan Duan, Kenneth S. Collins
-
Patent number: 8936732Abstract: A white light emitting glass-ceramic. The chemical formula of the glass-ceramic is aSiO2.bAl2O3.cNaF.dCeF3.nDyF3.mAg, wherein a, b, c, d, n and m are, by mol part, 25-50, 15-30, 10-30, 10-25, 0.01-1 and 0.01-1, respectively, and a+b+c+d-100. A method for producing said glass-ceramic is also provided. Silver ion is doped in the glass-ceramic in the form of silver particles by means of sintering and reduction annealing treatment, and thus the luminescence properties of rare earth ion is improved.Type: GrantFiled: July 22, 2010Date of Patent: January 20, 2015Assignee: Ocean's King Lighting Science & Technology Co., Ltd.Inventors: Mingjie Zhou, Wenbo Ma, Fangyi Weng
-
Publication number: 20140200129Abstract: The invention relates to glass ceramics, which show high strength, high translucency, high chemical stability and which are still mechanically processible. The invention further refers to a method for producing a dental restoration comprising such glass or glass ceramic as well as the dental restoration itself.Type: ApplicationFiled: June 18, 2012Publication date: July 17, 2014Applicants: FRAUNHOFER-GESELLSCHAFT zur Förderung der angewandten Forschung e. V., DEGUDENT GMBH, VITA ZAHNFABRIK H. RAUTER GMBH & CO. KGInventors: Bernhard Durschang, Jörn Probst, Norbert Thiel, Michael Gödiker, Markus Vollmann, Udo Schusser, Carsten Wiesner
-
Patent number: 8771530Abstract: A method for producing a polarizing element includes: forming particulate materials of a metal halide on a glass substrate; forming a protective film that covers the particulate materials in a non-plasma environment; stretching the particulate materials by heating and stretching the glass substrate; and forming acicular metal particles by reducing the metal halide constituting the stretched particulate materials.Type: GrantFiled: February 22, 2013Date of Patent: July 8, 2014Assignee: Seiko Epson CorporationInventor: Yoshitomo Kumai
-
Publication number: 20140000315Abstract: A process is provided for obtaining a glassy material that is optically transparent to infrared radiation. The process includes: a step of amorphization, by mechanosynthesis, of an assembly of starting elements including at least one metallic element and at least one chalcogenide element, making it possible to form an amorphous powder; a step of hot densification, in a mould of predetermined dimensions, of the amorphous powder, making it possible to obtain a glass; and heat treatment, carried out during or after the hot densification step, in which the glass is heated to a temperature at which a portion of the glass is converted from an amorphous state to a crystalline state, making it possible to obtain, after cooling, a glass-ceramic.Type: ApplicationFiled: December 6, 2011Publication date: January 2, 2014Applicants: UNIVERSITE DE RENNES 1, CNRSInventors: Laurent Calvez, Xiang Hua Zhang, Mathieu Hubert, Gaëlle Delaizir
-
Publication number: 20130069005Abstract: A transparent glass ceramic emitting white light and preparation method thereof are provided. The chemical formula of the transparent glass ceramic is aSiO2.bAl2O3.cNa.dCeF3.xDyF3, wherein a, b, c, d, and x are mole fractions, a is 35˜50, b is 15˜30, c is 5˜20, d is 5˜20, x is 0.01˜1, and a+b+c+d=100. The transparent glass ceramic can be substituted for the combination of epoxy resin or silica gel and fluorescent powder to seal LED. The transparent glass ceramic has strong excitation spectrum with broadband at ultraviolet area, and can emit strong white light under the excitation of ultraviolet light.Type: ApplicationFiled: June 8, 2010Publication date: March 21, 2013Inventors: Mingjie Zhou, Fangyi Weng, Wenbo Ma
-
Patent number: 8263508Abstract: A phosphosilicate glass ceramic with nanoscale fluoroapatite and leucite crystals. The glass ceramic is very similar to natural tooth material in terms of its optical properties. The glass ceramic has a low linear thermal expansion coefficient and a low pressing temperature and is therefore particularly suitable for pressing on metal alloys to produce dental restoration.Type: GrantFiled: December 3, 2009Date of Patent: September 11, 2012Assignee: Ivoclar Vivadent AGInventors: Urs Bolle, Marcel Schweiger, Elke Apel, Wolfram Höland, Volker Rheinberger
-
Publication number: 20120186300Abstract: A seed retaining member has a recessed portion for breaking and separating formed at an arbitrary location and thereby allows stress concentration to occur at the recessed portion when applying a breaking load, to enable the seed retaining member to break with a smaller load than conventional. So that the seed retaining member can prevent a crack from propagating in an unintended location in the seed retaining member by allowing the crack to propagate along the recessed portion, and also can reduce a workload in a separation work of the seed retaining member and polycrystalline silicon. The seed retaining member for retaining a lower end portion of a seed serving as a seed rod and disposed at a bottom portion of a furnace for producing polycrystalline silicon by a Siemens method. A groove for breaking and separating is formed in an outer peripheral surface of the seed retaining member.Type: ApplicationFiled: September 2, 2010Publication date: July 26, 2012Applicant: TOYO TANSO CO., LTD.Inventors: Jun Ishizaki, Masaki Izumiya
-
Patent number: 8211817Abstract: Fused silica glass having an internal transmittance of UV with 245 nm wavelength, being at least 95% at 10 mm thickness, a OH content of not larger than 5 ppm, and a content of Li, Na, K, Mg, Ca and Cu each being smaller than 0.1 ppm. Preferably the glass has a viscosity coefficient at 1215° C. of at least 1011.5 Pa·s; and a Cu ion diffusion coefficient of not larger than 1×10?10 cm2/sec in a depth range of greater than 20 ?m up to 100 ?m, from the surface, when leaving to stand at 1050° C. in air for 24 hours. The glass is made by cristobalitizing powdery silica raw material; then, fusing the cristobalitized silica material in a non-reducing atmosphere. The glass exhibits a high transmittance of ultraviolet, visible and infrared rays, has high purity and heat resistance, and exhibits a reduced diffusion rate of metal impurities, therefore, it is suitable for various optical goods, semiconductor-production apparatus members, and liquid crystal display production apparatus members.Type: GrantFiled: September 11, 2007Date of Patent: July 3, 2012Assignees: Tosoh Corporation, Tosoh SGM CorporationInventors: Kazuyoshi Arai, Tsutomu Takahata, Shinkichi Hasimoto, Masahito Uchida, Nobusuke Yamada, Yoshinori Harada, Hideharu Horikoshi
-
Publication number: 20110239706Abstract: The present invention relates to a method for production of a synthetic quartz glass having a fluorine concentration of 1,000 ppm by mass or higher, comprising the following processes steps (a) to (c): (a) depositing and growing quartz glass fine particles obtained by flame hydrolysis of a glass-forming material onto a substrate, to thereby form a porous glass body; (b) maintaining the porous glass body in a reaction vessel under an elemental fluorine (F2)-containing atmosphere of 400° C. or lower, to thereby obtain a fluorine-containing porous glass body; and (c) heating the fluorine-containing porous glass body in a vitrification furnace to a transparent vitrification temperature, to thereby obtain a fluorine-containing transparent glass body, wherein, in step (b), elemental fluorine (F2) is continuously or intermittently supplied to the reaction vessel and the gas in the reaction vessel is continuously or intermittently discharged from the reaction vessel.Type: ApplicationFiled: April 1, 2011Publication date: October 6, 2011Applicant: Asahi Glass Company, LimitedInventors: Chikaya Tamitsuji, Kunio Watanabe, Akio Koike
-
Publication number: 20110239707Abstract: The present invention relates to a method for production of a synthetic quartz glass having a fluorine concentration of 1,000 ppm by mass or higher, comprising the following steps (a) to (c): (a) depositing and growing quartz glass fine particles obtained by flame hydrolysis of a glass-forming material onto a substrate, to thereby form a porous glass body; (b) maintaining the porous glass body in a reaction vessel under an elemental fluorine (F2)-containing atmosphere of a pressure of Pb1 and a temperature of 400° C. or lower, and followed by maintaining in the reaction vessel under condition of a pressure Pb2 lower than the pressure Pb1 and a temperature of 400° C. or lower, to thereby obtain a fluorine-containing porous glass body; and (c) heating the fluorine-containing porous glass body in a vitrification furnace to a transparent vitrification temperature, to thereby obtain a fluorine-containing transparent glass body.Type: ApplicationFiled: April 1, 2011Publication date: October 6, 2011Applicant: Asahi Glass Company, LimitedInventors: Chikaya Tamitsuji, Kunio Watanabe, Akio Koike
-
Publication number: 20110111944Abstract: The invention provides a crystallizable glass, a crystallized glass, and manufacturing methods thereof. The crystallizable glass can be crystallized in a short period of time, and can maintain its glass shape and its surface condition during a crystallization process. The crystallized glass has good mechanical strength, an adequate thermal expansion coefficient that allows the crystallized glass to be used as a construction material, less content of alkali-metal oxides, and good chemical durability. The MgO—Al2O3—SiO2-based crystallizable glass and crystallized glass contain, by mass percent, 55.0-65.0% SiO2, 8.0-14.0% Al2O3, 10.0-20.0% MgO, 1.5-6.0% CaO, 1.0-2.2% Li2O, 0.7-3.0% Na2O, 2.5-4.0% K2O, and 1.5-3.0% F.Type: ApplicationFiled: October 25, 2010Publication date: May 12, 2011Applicant: Huzhou Ta Hsiang Glass Products Co., Ltd.,Inventors: Kuo-Chuan Hsu, Chao Qu
-
Patent number: 7737062Abstract: The invention provides an opalescent forehearth color concentrate comprising a non-smelted agglomerated interspersion of particles for use in coloring glass, said concentrate comprising by weight from about 10% to about 70% of a glass component and from about 30% to about 90% of one or more opalescent pigments, the glass component comprising by weight from about 10% to about 50% ZnO and about 15 to about 60% SiO2. The invention also provides a method of using the color concentrate.Type: GrantFiled: June 5, 2007Date of Patent: June 15, 2010Assignee: Ferro CorporationInventors: George E. Sakoske, Kenneth R. Ackerman, John M. Bauer
-
Patent number: 7648656Abstract: The invention is directed to a silver-containing polarizing boroaluminosilicate glass composition that has been doped with a noble metal selected from the group consisting of Pt, Pd, Os, Ir, Rh and Ru, including mixtures thereof, to nucleate and precipitate silver ions to silver metal without the need for a reducing atmosphere step. The invention is further directed to a method for making the glass composition of the invention. Using the composition and method of the invention, one can prepare a glass having a selected null transmission range.Type: GrantFiled: November 6, 2008Date of Patent: January 19, 2010Assignee: Corning IncorporatedInventors: Nicholas Francis Borrelli, George Bigelow Hares, David John McEnroe, Joseph Francis Schroeder, III
-
Patent number: 7592063Abstract: For a substrate having fine convexoconcave patterns on its surface, the dimensions of the convexoconcave patterns in a vertical direction of a quartz glass substrate are controlled to be uniform with extreme accuracy and over the entire substrate surface. The quartz glass substrate is made to have a fictive temperature distribution of at most 40° C. and a halogen concentration of less than 400 ppm, and the etching rate of the surface of the quartz glass substrate is made uniform, whereby the dimensions of the convexoconcave patterns in a vertical direction of the quartz glass substrate are controlled to be uniform with good accuracy and over the entire substrate surface.Type: GrantFiled: September 5, 2006Date of Patent: September 22, 2009Assignee: Asahi Glass Company, LimitedInventors: Yoshiaki Ikuta, Shinya Kikugawa
-
Publication number: 20090223250Abstract: There is provided polarizing glass having a high extinction ratio in a broad band. A manufacturing method of the polarizing glass containing elongated metal particles dispersed and oriented within glass includes an elongation step of forming mother glass after heat-treatment into a preform, of heating the preform at such temperature that the viscosity of the glass becomes about 1×108 to 1×1014 poise, of applying stress of about 200 kg/cm2 to 500 kg/cm2 to the preform while moving the preform within an electric furnace with feeding speed of 10 mm/min. or less and of elongating the preform as an elongated sheet with pulling speed of 150 mm/min.Type: ApplicationFiled: December 12, 2007Publication date: September 10, 2009Applicant: ARISAWA MFG. CO., LTD.Inventors: Masahiro Ichimura, Yuichi Aoki
-
Patent number: 7371702Abstract: Radio-opaque glass ceramics are described which have high chemical durability and adjustable translucency, brightness and coefficient of thermal expansion.Type: GrantFiled: February 17, 2006Date of Patent: May 13, 2008Assignee: Ivoclar Vivadent AGInventors: Christian Ritzberger, Elke Apel, Wolfram Holand, Volker M. Rheinberger
-
Patent number: 7204942Abstract: The method of making a high quality fluoride crystalline optical microlithography lens element blank includes crystallizing a fluoride crystalline member with dimension ?200 mm from a melt, annealing the fluoride crystalline member and qualifying the resulting member for use as an optical microlithography lens element blank The fluoride crystalline optical lithography lens element blanks have multiple adjoining abutting crystalline subgrains with low boundary angles. The crystalline members made by the method are qualified for use as lens element blanks by a testing method including measuring their absorption spectra at 200 to 220 nm to determine absorbance at 205 nm and/or by making measurements of radiation diffracted by them.Type: GrantFiled: November 25, 2003Date of Patent: April 17, 2007Assignee: Schott AGInventors: Alexandre M. Mayolet, Michael A. Pell
-
Publication number: 20040167006Abstract: The invention relates to a bioactive rhenanite glass ceramic which is characterized by a high content of P2O5, CaO and Na2O and is particularly suitable as bone replacement material in dentistry.Type: ApplicationFiled: February 12, 2004Publication date: August 26, 2004Inventors: Elke Apel, Wolfram Holand, Volker Rheinberger
-
Patent number: 6772608Abstract: The invention relates to a method for producing UV polarizers, according to which spheroid particles situated near the surface of the glass are incorporated into the support material (primarily standard float glass) in a novel arrangement. According to the method for producing UV polarizers, after the introduction of metal ions (e.g., silver ions) into the glass surface, a large size distribution of particles is achieved by multiple alternation of a heat treatment for separating out spherical metal particles, followed by the renewed introduction of metal ions and a subsequent heat treatment. A deformation of the glass produces spheroid particles of various sizes and different semi-axis relationships. The particles are characterized by their large size distribution and are deformed differently in relation to their spheroid shape. In this way UV polarizers are produced which have a wide absorption range since the absorption bands having different maximum positions overlap.Type: GrantFiled: January 3, 2001Date of Patent: August 10, 2004Assignee: F.O.B. GmbH Gesellschaft Zur Fertigung Farbiger Optoelektronischer BauelementeInventors: Wolf-Gernot Drost, Andreas Berger
-
Patent number: 6767854Abstract: The invention refers to a material which is chemically long-term stable in a neutral or slightly acid environment and which can be used both as bioactive bone replacement material, e.g. in the form of a coating applied onto metallic prosthesis sticks by thermal spraying, and as substrate material in biotechnology, e.g. in the form of a ceramic sheet. According to the invention, said material comprises 15-45% by weight CaO, 40-45% by weight P2O5, 10-40% by weight ZrO2 and fluoride, said material further comprises two crystalline phases being apatite and calcium zirconium phosphate, and a secondary glass phase. Said material has a very high chemical long-term stability, compared to known materials which can also be produced by means of a melting process.Type: GrantFiled: June 13, 2002Date of Patent: July 27, 2004Assignee: Bam Bundesanstalt fuer Materialforschung und PrufungInventors: Georg Berger, Ute Ploska
-
Publication number: 20030230113Abstract: Methods of forming glass articles sensitive to aggressive heat treatment are disclosed. Glass preforms have sections of glass fusion bonded to the preforms, and the preforms are subsequently drawn into glass articles.Type: ApplicationFiled: June 12, 2002Publication date: December 18, 2003Inventors: Patrick Gedeon, Michael D. Harris, Robert Sabia
-
Patent number: 6645893Abstract: A glass includes (a) a matrix containing a compound of at least one nonmetallic element; and (b) a particle selectively formed in the matrix. This particle is made of the at least one nonmetallic element. A process for producing such glass includes (a) providing a blank glass containing a compound of at least one nonmetallic element; (b) condensing a pulsed laser beam to a focal point in the blank glass such that a particle is selectively formed in the blank glass at a position corresponding to the focal point, the particle being made of the at least one nonmetallic element dissociated from the compound; and (c) moving the focal point in the blank glass to produce a pattern of the particle. The glass is suitable for optical functional elements.Type: GrantFiled: February 21, 2001Date of Patent: November 11, 2003Assignee: Central Glass Company, LimitedInventors: Kiyotaka Miura, Seiji Fujiwara, Takuya Teshima, Natsuya Nishimura, Yoshinori Kubota
-
Publication number: 20030195107Abstract: A synthetic quartz glass for optical use, to be used by irradiation with light within a range of from the ultraviolet region to the vacuum ultraviolet region, which contains fluorine, which has a ratio of the scattering peak intensity of 2250 cm−1 (I2250) to the scattering peak intensity of 800 cm−1 (I800), i.e. I2250/I800, of at most 1×10−4 in the laser Raman spectrum, and which has an absorption coefficient of light of 245 nm of at most 2×10−3 cm−1.Type: ApplicationFiled: December 12, 2002Publication date: October 16, 2003Applicant: ASAHI GLASS COMPANY LIMITEDInventors: Yoshiaki Ikuta, Shinya Kikugawa, Noriaki Shimodaira, Akio Masui, Shuhei Yoshizawa
-
Patent number: 6519975Abstract: The present invention is directed to a fluorinated rare earth doped glass composition and method for making a glass-ceramic optical article therefrom, e.g. optical fiber waveguides, fiber lasers and active fiber amplifiers, having application in the 1300 nm and 1550 nm telecommunications windows. The inventive compositions include Pr3+ and/or Dy3+ in a concentration range of between 300-2,000 ppmw and Ag+ in a concentration range of between 500-2000 ppmw; or Er3+ in a concentration range of between 500-5,000 ppmw and Ag+ in a concentration range of between 0-2,000 ppmw. The monovalent silver ion provides an ionic charge balanced glass-ceramic crystal. These compositions exhibit reduced or absent rare earth ion clustering and fluorescence quenching effects in the presence of high concentrations of rare earth ion dopants.Type: GrantFiled: August 22, 2000Date of Patent: February 18, 2003Assignee: Corning IncorporatedInventors: James Crawford Bange, Nicholas Francis Borrelli, Lauren Kay Cornelius, John White O'Connell, Paul Arthur Tick
-
Publication number: 20020062662Abstract: The invention relates to a method for ceramizing starting glass of glass-ceramics into glass-ceramics, comprising at least the following steps:Type: ApplicationFiled: August 23, 2001Publication date: May 30, 2002Inventors: Ulrich Fotheringham, Hauke Esemann, Bernd Hoppe, Rudiger Sprengard, Michael Kluge, Falk Gabel
-
Publication number: 20020064493Abstract: This invention relates to bioactive sol-gel derived silica fibers, methods for their preparation, an implantable device comprising said fibers and the use of said device for tissue guiding or bone repair.Type: ApplicationFiled: December 1, 1999Publication date: May 30, 2002Inventors: TIMO PELTOLA, Mika Jokinen, Sinikka Veittola, Antti Yli-urpo
-
Patent number: 6352949Abstract: A glass ceramic material for storing energy of X-rays and releasing said energy by photo-stimulation comprising a fluoride glass matrix containing micro-crystalline particles, said particles having an average particle size, d, so that d<2 &mgr;m and said glass ceramic shows in a XRD spectrum a continuous spectrum of said glass matrix and discrete peaks superimposed on said continuous spectrum. Said glass matrix contains preferably zirconium ions and ions selected from the group consisting of alkali ions and alkaline earth ions, at least 5 mole % of the fluoride ions is replaced by bromide and/or chloride ions and at least 0.01 mole % of cations selected from the group consisting of transition metal ions, rare earth metal ions, In+, Ga+, Tl+, and Pb2+ is present.Type: GrantFiled: June 15, 2000Date of Patent: March 5, 2002Inventors: Peter Willems, Johann-Martin Spaeth, Stefan Schweizer, Andrew Edgar, Luc Struye, Paul Leblans
-
Publication number: 20010045106Abstract: The present invention provides a two stage process of thermal separation of CFCs and HCFCs followed by vitrification of the waste into a commercially viable glass. In the first stage, the hydrogenated compounds are reacted at elevated temperature with water and a metal oxide such as calcium oxide to form a halide salt and carbon dioxide. In the second stage of the process, the brine slag is reacted at elevated temperature with the carbon dioxide from stage one and glass-forming raw materials such as silicon dioxide to produce a glass. The final glass product incorporates the halide into the glass.Type: ApplicationFiled: March 20, 2001Publication date: November 29, 2001Inventors: Christopher J. Ludwig, Frederic M. Schwartz
-
Patent number: 6281151Abstract: The present invention relates to a transparent glass-ceramic material which includes a glass matrix and a crystalline phase of lanthanum fluoride crystals in the glass matrix, where the transparent glass-ceramic material contains no silica. The present invention further relates to a method of producing the transparent glass-ceramic material.Type: GrantFiled: January 24, 2000Date of Patent: August 28, 2001Assignee: Corning IncorporatedInventor: Paul A. Tick
-
Patent number: 6167727Abstract: A process for producing a polarizing glass containing shape-anisotropic metallic particles dispersed in an oriented state therein, which comprises drawing a glass preform containing metallic halide particles dispersed therein while its viscosity being held above 2×106, but below 7×107 poises; and subjecting the drawn glass to a reducing treatment so that a part or all of the metallic halide particles are reduced to metallic particles, which process enables it to produce a polarizing glass with a high yield from a starting material of a glass containing metallic halide particles, while avoiding glass breakage or fracture during elongation as well as preventing the elongated metallic halide particles from returning to a spherical shape.Type: GrantFiled: August 19, 1998Date of Patent: January 2, 2001Assignee: Hoya CorporationInventors: Hidemi Tajima, Takeshi Takahashi, Yukari Miyashita, Yoshihiko Matsuoka