Abstract: The invention relates to a method for determining the intrinsic viscosity [?] of an aqueous polymer solution at a temperature T, wherein the aqueous polymer solution comprises at least one acrylamide-based polymer in an aqueous solvent, the aqueous solvent having a salinity of from 6 to 250 g/L, the method comprising the steps of: —providing a single universal relation R1 between (i), the product of polymer concentration and intrinsic viscosity C·[?], and (ii) specific viscosity at zero shear rate ?sp; —performing a measurement of the dynamic viscosity of the aqueous polymer solution at one polymer concentration C1, at temperature T and at various shear rates; —determining from said measurement the zero-shear viscosity ?0 of the aqueous polymer solution at polymer concentration C1 and at temperature T; —calculating the specific viscosity at zero shear rate of the aqueous polymer solution at polymer concentration C and at temperature T as ?sp=(?0??s)/?s, where ?s is the zero-shear viscosity of the aqueous solv

Abstract: There are provided a viscometer that can accurately measure a bulk viscosity of a small amount of a liquid sample such as 100 ?L or less, and a method for measuring viscosity. A viscometer (1) comprises a fixing member (31), an upper unit (10), a lower unit (11), and an information processing unit (50). A method for measuring viscosity comprises measuring a viscosity of the sample by measuring a response voltage during resonance from a detecting means (19) that detects displacement of a leaf spring (17) in one direction due to vibration of the upper unit (10) through applying an AC voltage to a piezoelectric element (15) while changing a frequency by the information processing unit (50).

Abstract: Provided is an analysis apparatus configured to analyze characteristics of a viscoelastic material based on a viscoelastic material constitutive law in which an elastic element and a viscoelastic element are arranged in parallel with each other; calculate, in a viscoelastic material model divided into a finite number of elements each having a node, a displacement amount of the node; calculate a strain rate at the node through use of the displacement amount; calculate, as a relaxation time of the viscoelastic element, a value proportional to a value of a power using the strain rate as a base and a value of a power using a shift factor of a temperature-time conversion law as a base; and calculate a stress at the node through use of the relaxation time.

Abstract: The systems and methods described herein relate to a high-throughput flow apparatus. The apparatus is used with an array of wells, and is configured to impart a predetermined shear stress on cells cultured within each of the wells of the array of wells. The apparatus includes a plurality of mechanical tips. The plurality of mechanical tips each includes a head with a hemispheroid shape. The apparatus also includes a motor associated with at least one of plurality of mechanical tips. The motor is configured to drive the plurality of mechanical tips to impart the shear stress pattern in each of the wells.

Abstract: A method and a device determine tribological measured values of samples with a rheometer. Wherein the measuring parts of the rheometer are replaced by samples and the surfaces of the samples are moved into frictional contact relative to each other. Accordingly, it is provided that all parts of the rheometer holding the samples in frictional connection and frictional contact or forming the rheometer power circuit, including the spring unit pressing the samples against each other, are regarded as an oscillatory circuit. The oscillation properties of the spring unit are regarded as relevant to the oscillation properties of the oscillatory circuit, and that the oscillation properties of the spring unit are adjusted taking into consideration the resonance oscillations or effects produced by changing, different measurement conditions expected with the respective measurement.

Abstract: Disclosed is a sensor that can accurately detect displacement and prevents the phenomenon of a contact section between a shaft member and a sliding element receiver being shifted. The sensor comprising: a case having a through hole; a resistance substrate fixed at an inside of said case; a shaft member having a first end portion which is one end of the shaft member placed within said case and a second end portion which is other end of the shaft member exposed to an outside of said case from said through hole, said shaft member being placed at said through hole in a movable manner in an axial direction; and a sliding element receiver having a bearing end contacting with said second end portion of said shaft member, and attached with a brush sliding together with said resistance substrate, said sliding element receiver being capable of moving relatively against said resistance substrate with said shaft member. A hemispherical end face is formed at said first end portion.

Abstract: The invention relates to a method for measuring the viscosity of a fluid, said method comprising the following steps: (a) providing a flow of said fluid in a laminar state inside a channel (14, 24) having a characteristic transverse dimension D, and in which an elongate member (12, 22) having a characteristic dimension d is placed substantially along the longitudinal direction of said channel and substantially at the center of the channel, and has a portion of the length l thereof submerged in said channel; (b) measuring the friction force (f) applied by said fluid on the walls of the elongate member; and (c) calculating the dynamic viscosity (?) of said fluid based on the equation (1) f=??lU where U is the average flow rate and ? is a geometric factor.

Abstract: A rheometer instrument including a stationary frame, a sleeve suspended from said frame, means for rotating the sleeve, a bob suspended within the sleeve, a cross-spring pivot suspending the bob from the stationary frame and a force rebalance system for effecting the rotational displacement of the bob with a torque. The force rebalance system includes an arm attached to the movable portion of the cross-spring pivot, a rotational position sensor in close proximity to the arm for measuring the rotational displacement and angular frequency of the arm, and a force actuator positioned to apply force to the arm. The rheometer instrument may be used to calculate the rheological properties of Newtonian and non-Newtonian fluids.

Abstract: A parallel-plate system collects data used to determine viscosity. A first plate is coupled to a translator so that the first plate can be moved along a first direction. A second plate has a pendulum device coupled thereto such that the second plate is suspended above and parallel to the first plate. The pendulum device constrains movement of the second plate to a second direction that is aligned with the first direction and is substantially parallel thereto. A force measuring device is coupled to the second plate for measuring force along the second direction caused by movement of the second plate.

Abstract: Methods and systems for characterizing drilling fluids laden with LCM (Lost Circulation Material) and other solid materials are disclosed. A test cell for analyzing a fluid is provided with a first conical inner portion and an axial positioning device positioned along an axis of the test cell. A first conical plug is coupled to the axial positioning device and is movable in and out of the first conical inner portion along the axis of the test cell. A fluid inlet is positioned at a first location on the test cell and a fluid outlet at a second location.

Abstract: A method is for connecting a tab pattern formed on a base sheet and a lead wire, wherein the tab pattern includes: a tab main portion; and a connecting portion formed to continue from one edge line of the tab main portion and to extend from the tab main portion along an extension line that is substantially orthogonal to the edge line, and wherein the method includes: connecting the lead wire on the tab main portion by bonding the lead wire at a position being displaced from the extension line of the connecting portion for more than a given offset amount where the extension line is identical to a center line of the connecting portion, the position being within a given distance from the edge line of the tab main portion.

Abstract: An apparatus and method for performing rheological measurements of interfaces located at the top of fluid sub-phases. In one configuration, a rotating rheometer is provided with a chamber wall whose inner surface defines an outer chamber radius and an inner cylinder disposed within the cylindrical chamber and having an inner chamber radius. The rotating rheometer is configured to hold a liquid sub-phase and interface layer that can be probed using a circular ribbon that is concentric with and suspended between the inner cylinder and chamber wall. The ratio of the ribbon radius, inner chamber radius, and outer chamber radius is designed to yield an average shear rate in the inner region that is the same as an average shear rate in the outer region. In one configuration, an interface-pinning feature is provided on at least one of the inner cylinder and the chamber wall.

Abstract: A method and device allow automatic trimming of samples for the measurement of the Theological properties of material samples by way of a plate/plate rheometer.

Abstract: An in-situ structuring rheometer provides a means to develop and measure the rheological properties of structured materials such as those having various polymer blend morphologies or particle networks. Chaotic advection of liquid contained within a cavity is instilled by controlled motions of boundary surfaces and, concomitantly, forces and displacements on the boundary surfaces are measured, indicating at least one of a flow- or a structure-related property.

Abstract: The present invention is generally directed to a method for measuring interfacial stick-slip transitions (SST) and an improved constant-force shear capable of measuring interfacial SST. Some embodiments are capable of measuring SST under simple shear conditions and/or in highly entangled polymer melts. Some embodiments include the application of a constant shearing force to a polymer sample.

Abstract: A microscope rheometer for measuring shear and compression properties of biological samples is disclosed. The apparatus allows a sample of biological tissue to be strained controllably while fluorescently stained cells, or other markers, within the material are imaged with a fluorescence microscope and the applied forces are measured with a strain gauge. Using the rheometer, it is possible to obtain the shear and compression stiffness of a material as a function of position.

Abstract: Method of determining at least one dynamic characteristic of a sample of a deformable solid or fluid material, comprising: the contacting of said sample (24, 42) with at least one interaction surface (23, 25, 41a, 41b); the application of a relative movement between said sample (24, 42) and said interaction surface (23, 25, 41a, 41b); and the measurement (26) of at least one dynamic or kinematic quantity in respect of the sample (24, 42) and/or said interaction surface (23, 25, 41a, 41b), wherein said interaction surface (23, 25, 41a, 41b) has an intrinsic wettability with respect to the material that is higher than that of metals. Device for implementing this method. According to particular embodiments, said interaction surface (23, 25) is made of high-density sintered ceramic or made of single crystal silicon or germanium, preferably having a zero open porosity and an arithmetic mean roughness parameter of less than 12.5 ?m and preferably between 0.4 and 1.6 ?m.

Abstract: Device for measuring the rheological properties of a viscoelastic material, formed of an upper rotating plate (10) and of a lower rotating plate (20) which are able to press against the opposite faces of a sample S of the material to be measured. The axes of rotation (a1 a1? and a2 a2?) of said plates are arranged parallel to one another in a direction perpendicular to the plane formed by the plates, and offset from one another by a distance d. Two independent motors (12, 22) drive respectively the upper plate (10) and the lower plate (20) at the same speed of rotation ?, without giving rise to any angular displacement between the two plates.

Abstract: A rheometer has a measuring chamber which is delimited by a measuring chamber wall in which at least one measuring component is disposed for acceptance of a sample. The measuring chamber can have a gas flowing through it whose temperature is controlled in a desired fashion by a first temperature control device. A second temperature control device is also disposed in the measuring chamber wall by means of which the wall of the measuring chamber can be temperature controlled to a desired temperature. To temperature control the sample, the gas flow in the measuring chamber can be switched off or at least highly reduced prior to measurement of the reological characteristic quantities and further temperature control of the measuring chamber is effected by means of the temperature control of the measuring chamber wall.

Abstract: The present invention relates to a miniature rheometer, a parallel rheometer, and improved force sensor elements which may advantageously be used in combination with the miniature rheometer and the parallel rheometer. The miniature rheometer is adapted to determine rheological characteristics of materials which are provided in the form of small quantity samples. The miniature rheometer comprises an actuating element, a sensing element and a feedback circuit to provide rebalance of the shear force applied by the sample to the sensing element, which insures an exceptional stiffness in determining the shear strain so as to allow measurements of high accuracy. The parallel rheometer of the present invention allows simultaneous measurements of a plurality of samples so as to allow of a plurality of samples within a short time period. The force sensor element according to the present invention allows simultaneous measurement of a shear force and a normal force applied to the sensor element.

Abstract: A system that facilitates in situ determination of lubricity in a fluid comprises a multi-element sensor positioned within a machine, wherein the multi-element sensor obtains data regarding a plurality of parameters of a fluid. A component calculates lubricity of the fluid based at least in part upon the measured parameters.

Abstract: Viscometer (80) with a sample cup (42) rotatable by a pulley (26) and a timing belt (30) to shear a tested fluid thus imparting torque to a bob (44) mounted on a shaft (10) supported via a frictionless bearing (58), an optical distance sensor assembly (12) measures the distance to an arm (70) which is connected to the top of shaft (10). This distance information is further converted to the viscosity of the tested fluid.

Abstract: Viscometer (80) with a sample cup (42) rotatable by a pulley (26) and a timing belt (30) to shear a tested fluid thus imparting torque to a bob (44) mounted on a shaft (10) supported via a frictionless bearing (58), an optical distance sensor assembly (12) measures the distance to an arm (70) which is connected to the top of shaft (10). This distance information is further converted to the viscosity of the tested fluid.

Abstract: Methods and apparatus for measuring sag properties of a drilling fluid using a rotary viscometer. An insert, or shoe, is placed at the bottom of the heat cup containing the fluid to be tested. A rotating cylinder is disposed within the fluid and solid particles are allowed to settle toward the bottom of the heat cup. The shoe incorporates a curved and inclined upper surface that directs the settled particles toward a well non-centrally located in the shoe. As the test is performed, fluid samples can be withdrawn from the well and analyzed. The samples can then be returned to the well and the test continued. The insert concentrates the settled solids into a single location, which increases the sensitivity of the test and provides a location for sample acquisition that is easily and repeatedly located, which allows for improved correlation with laboratory and flow loop results.

Abstract: The present invention relates to a miniature rheometer, a parallel rheometer, and improved force sensor elements which may advantageously be used in combination with the miniature rheometer and the parallel rheometer. The miniature rheometer is adapted to determine rheological characteristics of materials which are provided in the form of small quantity samples. The miniature rheometer comprises an actuating element, a sensing element and a feedback circuit to provide rebalance of the shear force applied by the sample to the sensing element, which insures an exceptional stiffness in determining the shear strain so as to allow measurements of high accuracy. The parallel rheometer of the present invention allows simultaneous measurements of a plurality of samples so as to allow of a plurality of samples within a short time period. The force sensor element according to the present invention allows simultaneous measurement of a shear force and a normal force applied to the sensor element.

Abstract: The invention relates to an apparatus and method for testing the properties of chemicals in a reaction flow stream. In the method, chemicals from the reaction flow stream are directed to the apparatus for testing the physical properties of the chemicals, which is an indication of the state of the chemical reaction. Data measured by the apparatus is stored in a computer, and the computer may be used to analyze the data and to control the reaction parameters based on the analysis of the data. The apparatus used for the analysis comprises a rheometer having an actuated shaft and a concentric container, wherein the shear properties of the material sampled in the apparatus are measured when the actuator shaft is oscillated within the container. Various unique configurations of the apparatus are described.

Abstract: A viscometer for measuring liquid viscosities based upon rotational deflections of a suspended bob. The viscometer comprises a deflection indicator, a deflection reader located at a spaced relative position with respect to the indicator, a rotating element which rotates in unison with the bob and includes either the deflection indicator or the deflection reader, and a magnetic bearing assembly which prevents any substantial change in the spaced, relative position of the deflection reader with respect to the deflection indicator.

Abstract: The present invention relates to a miniature rheometer and improved force sensor elements which may advantageously be used in combination with the miniature rheometer. The miniature rheometer is adapted to determine rheological characteristics of materials which are provided in the form of small quantity samples. The force sensor element according to the present invention allows simultaneous measurement of a shear force and a normal force applied to the sensor element. Moreover, the force sensor may employ stress-optic material.

Abstract: The present invention relates to a miniature rheometer, a parallel rheometer, and improved force sensor elements which may advantageously be used in combination with the miniature rheometer and the parallel rheometer. The miniature rheometer is adapted to determine rheological characteristics of materials which are provided in the form of small quantity samples. The miniature rheometer comprises an actuating element, a sensing element and a feedback circuit to provide rebalance of the shear force applied by the sample to the sensing element, which insures an exceptional stiffness in determining the shear strain so as to allow measurements of high accuracy. The parallel rheometer of the present invention allows simultaneous measurements of a plurality of samples so as to allow of a plurality of samples within a short time period. The force sensor element according to the present invention allows simultaneous measurement of a shear force and a normal force applied to the sensor element.

Abstract: The invention relates to an apparatus and method for testing the properties of chemicals in a reaction flow stream. In the method, chemicals from the reaction flow stream are directed to the apparatus for testing the physical properties of the chemicals, which is an indication of the state of the chemical reaction. Data measured by the apparatus is stored in a computer, and the computer may be used to analyze the data and to control the reaction parameters based on the analysis of the data. The apparatus used for the analysis comprises a rheometer having an actuated shaft and a concentric container, wherein the shear properties of the material sampled in the apparatus are measured when the actuator shaft is oscillated within the container. Various unique configurations of the apparatus are described.

Abstract: The present invention relates to a miniature rheometer, a parallel rheometer, and improved force sensor elements which may advantageously be used in combination with the miniature rheometer and the parallel rheometer. The miniature rheometer is adapted to determine rheological characteristics of materials which are provided in the form of small quantity samples. The miniature rheometer comprises an actuating element, a sensing element and a feedback circuit to provide rebalance of the shear force applied by the sample to the sensing element, which insures an exceptional stiffness in determining the shear strain so as to allow measurements of high accuracy. The parallel rheometer of the present invention allows simultaneous measurements of a plurality of samples so as to allow of a plurality of samples within a short time period. The force sensor element according to the present invention allows simultaneous measurement of a shear force and a normal force applied to the sensor element.

Abstract: The present invention relates to a miniature rheometer, a parallel rheometer, and improved force sensor elements which may advantageously be used in combination with the miniature rheometer and the parallel rheometer. The miniature rheometer is adapted to determine rheological characteristics of materials which are provided in the form of small quantity samples. The miniature rheometer comprises an actuating element, a sensing element and a feedback circuit to provide rebalance of the shear force applied by the sample to the sensing element, which insures an exceptional stiffness in determining the shear strain so as to allow measurements of high accuracy. The parallel rheometer of the present invention allows simultaneous measurements of a plurality of samples so as to allow of a plurality of samples within a short time period. The force sensor element according to the present invention allows simultaneous measurement of a shear force and a normal force applied to the sensor element.

Abstract: A viscosity and viscoelasticity measuring instrument has a cam, a follower arm, a flat spring, a plate fixture, and a removable plate assembly. The cam is a rotating circular disk with a spiral slot. A cam follower on the follower arm resides in the spiral slot so that the follower arm pivots about its fixed end as the cam rotates. The spring is attached to and collinear with the fixed end of the follower arm so that the spring pivots in the opposite direction as the follower arm. The removable plate assembly has a lower plate and an upper plate with mating sample surfaces on which test fluid is placed. The lower plate fits into a lower jaw of the plate fixture that is attached to the instrument base. The upper plate fits into an upper jaw of the plate fixture attached to the free end of the spring. A fluid is placed on the lower sample surface. The cam rotates, pushing the follower arm up, causing the spring to pivot down, and pressing the sample surfaces together.

Abstract: An apparatus and method are disclosed for measuring or analyzing dynamic and static sag caused by settling of weighting materials in drilling fluids or other solids bearing fluid. The apparatus comprises a tube and shear shaft assembly that allows for a controlled rate of shear to be applied to a sample of the fluid for testing. During a test, the assembly is placed on a pivotal holder at an angle. The assembly has pistons at the pivot center of the assembly which accommodate expansion and contraction of the test fluid due to changes in temperature and pressure, thereby allowing the test fluid to be heated, cooled and pressurized to simulate subterranean wellbore conditions without changing the center of mass of the test fluid. When weight material settles down the inclined assembly, the center of mass of the assembly changes resulting in changing torque or moment about the pivotal holder. The resultant moment is measured by energizing external coils arranged to provide a uniform magnetic field.

Abstract: A sample surface component for an instrument the measures viscosity and viscoelasticity. The instrument has a cam, a follower arm, a flat spring, a plate fixture, and a removable plate assembly. The cam is a rotating circular disk with a spiral slot. A cam follower on the follower arm resides in the spiral slot so that the follower arm pivots about its fixed end as the cam rotates. The spring is attached to and collinear with the fixed end of the follower arm so that the spring pivots in the opposite direction as the follower arm. The sample surface component include a removable plate assembly with a lower plate and an upper plate with mating sample surfaces on which test fluid is placed. The lower plate fits into a lower jaw of the plate fixture that is attached to the instrument base. The upper plate fits into an upper jaw of the plate fixture attached to the free end of the spring. A fluid is placed on the lower sample surface.

Abstract: The present invention relates to a miniature rheometer, a parallel rheometer, and improved force sensor elements which may advantageously be used in combination with the miniature rheometer and the parallel rheometer. The miniature rheometer is adapted to determine rheological characteristics of materials which are provided in the form of small quantity samples. The miniature rheometer comprises an actuating element, a sensing element and a feedback circuit to provide rebalance of the shear force applied by the sample to the sensing element, which insures an exceptional stiffness in determining the shear strain so as to allow measurements of high accuracy. The parallel rheometer of the present invention allows simultaneous measurements of a plurality of samples so as to allow of a plurality of samples within a short time period. The force sensor element according to the present invention allows simultaneous measurement of a shear force and a normal force applied to the sensor element.

Abstract: The present invention relates to a miniature rheometer, a parallel rheometer, and improved force sensor elements which may advantageously be used in combination with the miniature rheometer and the parallel rheometer. The miniature rheometer is adapted to determine Theological characteristics of materials which are provided in the form of small quantity samples. The miniature rheometer comprises an actuating element, a sensing element and a feedback circuit to provide rebalance of the shear force applied by the sample to the sensing element, which insures an exceptional stiffness in determining the shear strain so as to allow measurements of high accuracy. The parallel rheometer of the present invention allows simultaneous measurements of a plurality of samples so as to allow of a plurality of samples within a short time period. The force sensor element according to the present invention allows simultaneous measurement of a shear force and a normal force applied to the sensor element.

Abstract: The present invention relates to a miniature rheometer, a parallel rheometer, and improved force sensor elements which may advantageously be used in combination with the miniature rheometer and the parallel rheometer. The miniature rheometer is adapted to determine rheological characteristics of materials which are provided in the form of small quantity samples. The miniature rheometer comprises an actuating element, a sensing element and a feedback circuit to provide rebalance of the shear force applied by the sample to the sensing element, which insures an exceptional stiffness in determining the shear strain so as to allow measurements of high accuracy. The parallel rheometer of the present invention allows simultaneous measurements of a plurality of samples so as to allow of a plurality of samples within a short time period. The force sensor element according to the present invention allows simultaneous measurement of a shear force and a normal force applied to the sensor element.

Abstract: The present invention relates to a parallel rheometer and improved force sensor elements, which may advantageously be used in combination with the parallel rheometer. The parallel rheometer of the present invention allows simultaneous measurements of a plurality of samples so as to allow characterization of a plurality of samples within a short time period. The force sensor element according to the present invention allows simultaneous measurement of a shear force and a normal force applied to the sensor element. Moreover, the force sensor may employ stress-optic material.

Abstract: An asphalt stability testing vessel includes a container, an external heater, an internal heater, an agitator assembly, a temperature controller, and at least one sampling tube. The external heater is disposed on the outside surface area of the container. The external heater is surrounded by a thermal insulator. The internal heater is located inside the container and at substantially the bottom thereof. The agitator includes a motor, a shaft, and at least one propeller. The top of the container has at least one opening for the insertion of a sampling tube. The asphalt stability testing vessel is used to prepare modified asphalt binder for numerous stability tests. The tests include external heat without agitation, internal heat with high agitation, and internal heat without agitation. The values of complex shear modulus and phase angle obtained from the modified asphalt binder are analyzed for separation and degradation.

Abstract: To detect rheological material properties of a fluid, flowable or elastic material, the material is exposed to harmonic excitation with at least one fundamental and at least one parameter F is measured that is variable in response to the harmonic excitation and suitable for determining a new material parameter, whereby measurement of the parameter F comprises recording of a time function F(t) of the parameter and the time function F(t) is subjected to Fourier transformation to form a shear spectrum in which the rheological material properties can be detected from the position of the frequency components, their intensity and/or their dependence on the fundamental.