Abstract: A system and method for conditioning of very low pressure gas samples extracted from a source, heating the samples, boosting the pressure to a level appropriate for analysis, regulating the gas sample temperature and pressure to prevent dew-point dropout from Joules Thompson condensation, and passing the gas sample to an a remotely located analyzer or analyzer array where the electrical power for the pressurizing pump and heated regulator is provided by heat tracing.

Abstract: A heating and/or chilling bath with an internally illuminated specimen container receptacle for enhanced specimen examination or monitoring. Internal illumination provided either directly from light sources or redirected via light propagations rods. The enhanced illumination may include ultraviolet, visible light, infrared, and/or other electromagnetic ranges useful for illuminating specimens observation with the naked eye, microscopy, CCD, and/or other device assisted observation methods.

Abstract: A vial feed device is equipped with a feed arm, which is positioned between a vial tray and an oven and below either of them and having a feeding housing unit and a cooling housing unit, and a vial up-and-down moving mechanism for placing and removing vials in and from vial tray and oven. Feed arm is rotationally driven by a drive motor to move a feeding housing unit, a cooling housing unit and up-and-down moving mechanism toward vial tray or oven. High-temperature vials in oven are housed in cooling housing unit until cooling time T elapses. After cooling time T elapses, cooling housing unit is moved to a lower part of vial tray by feed arm, to be returned to vial tray by up-and-down moving mechanism.

Abstract: A system and method are provided for implementing an advanced monitoring scheme to detect a localized presence of particular target substances, including toxic chemical agents, in a space, and particularly for detecting and monitoring a presence of chemical agents that are absorbed into porous or semi-porous products and surfaces in the space when it is determined that potential chemical agent exposure has occurred. A heated vaporizer inlet apparatus provides a sensor source that is optimized for the detection of less volatile chemical agents, and particular less volatile chemical agents, that have been absorbed by materials with porous compositions or surfaces. The heated vaporizer inlet apparatus is used for heating architectural surfaces that were exposed to chemical agents in an effort to substantially increase a vapor pressure of a target substance disposed on or absorbed in a particular target surface.

Abstract: There is described a method for heating a sample material in a sample holder, the method comprising receiving the sample holder in a heating chamber of a heating system, the sample holder having at least one sample recipient with the sample material therein; dynamically forming an individual mini microwave cavity around the sample recipient; and applying microwaves generated by at least one microwave generator directly to the sample.

Abstract: The invention provides methods and devices for preparing frozen vitrified samples for transmission electron microscopy. By reducing the volume of sample from microliter scale to picoliter scale, the requirement for blotting of excess fluid is minimized or eliminated.

Abstract: A sampler has a sample chamber for a sample forming from a molten material, at least one lower cooling body, at least one upper cooling body, at least one inner cooling body, and at least one filling part. The sample chamber is surrounded jointly at least by the lower cooling body and the inner cooling body, such that at least the sample chamber can be cooled by at least the lower and inner cooling bodies. The filling part merges into the sample chamber by a filling opening. Between a region of the outer surface of the inner cooling body and a region of the outer surface of the upper cooling body opposite the outer surface of the inner cooling body, the sampler has at least one gap for conducting at least one gas. The volume of the respective cooling bodies is larger than the volume of the gap.

Abstract: The automated sample extraction device is a device for the automatic extraction of chemical samples. The device includes a housing defining an open interior region. A rotating carousel is disposed within the housing, and a plurality of sample holders are mounted thereon. A plurality of sample storage tanks each contain a unique chemical sample, and a desired volume of at least one chemical sample is drawn from a respective one of the sample storage tanks to a respective at least one of the plurality of sample holders. The carousel is rotated so that the desired volume of the at least one chemical sample may be dispensed into a receptacle positioned adjacent the carousel. The at least one chemical sample may then be mixed, heated, cooled, shaken and/or vibrated within the receptacle prior to dispensing.

Abstract: There is provided a monitoring apparatus including a gas sampling apparatus and a sensor that detects a chemical substance included in gas obtained by the gas sampling apparatus. The gas sampling apparatus includes: an air supplying unit that forms an air curtain to form a space that covers a region to which an object to be monitored is included and which is separated from the outside environment; a sampling unit that extracts the gas inside the separated space; and a diffusion gas supplying unit that supplies, into the separated space, an amount of diffusion gas that is at least equal to the sampled amount of the sampling unit, wherein the sampling unit includes a plurality of sampling nozzles disposed at three-dimensionally different positions inside the separated space.

Abstract: A method and system for controlled rate freezing and nucleation of materials is provided. The presently disclosed system and method provides the ability to rapidly cool the materials contained in vials or other containers within a cooling unit via forced convective cooling using a laminar and uniform flow of cryogen in proximity to the plurality of vials disposed within the cooling unit. The rapid cooling of the biological materials is achieved by precisely controlling and adjusting the temperature of the cryogen being introduced to the system as a function of time. The presently disclosed methods to systems also provide nucleation control via temperature quench and depressurized nucleation control.

Abstract: A method of monitoring a composition in transition from liquid to solid state includes the steps of providing an apparatus having a temperature pyrometer, a drying element, a laser displacement sensor, and an electronic balance; providing a composition in a liquid state; converting the composition to a solid state; and measuring the a process condition during said step of converting. The apparatus can include a drying element, a temperature pyrometer, a laser displacement sensor, a platform for holding a composition, an electronic balance, and a spectral birefringence measurement system.

Abstract: A headspace sample introduction device which collects a sample gas from a sample container and introduces the gas into a predetermined analyzer is provided. The device includes a sample tray 10 capable of holding at least one sample container 100 storing a liquid sample or a solid sample, a heating means 30 for heating at least one sample container 100 taken from the sample tray 10, a sample-gas collecting means 40 for collecting a sample gas from the upper space in the sample container 100 held in the heating means 30, and a cooling transfer means 20 for keeping and cooling at least one sample container 100 taken from the heating means 30 and returning the cooled sample container 100 to the sample tray 20. Since the headspace sample introduction device can return the heated sample containers 100 to the sample tray 10 after they are cooled with the cooling transfer means 20, the hot sample containers can be assuredly prevented from contacting the user.

Abstract: A transportable Sample Apparatus includes a vacuum flask (Dewar flask) and integral sample container. The Sample Apparatus may be used to capture a liquid phase LNG sample at a custody transfer point and to transport the sample to a laboratory for analysis. Vaporization of the liquid phase sample may take place at a variety of different locations. For example, vaporization may begin and/or be completed during transport from the collection point to the laboratory. In another example, vaporization may begin and be completed in the laboratory. In yet another example vaporization may begin during transport and be completed at the laboratory. The gas phase sample is typically analyzed by a gas chromatograph for Btu content, among other things. Prior to capture of the sample, the Sample Apparatus goes through a pre-cool cycle to chill a sample end cap and other components to a temperature compatible with capture of a cryogenic liquid sample which is about ?250° F.

Abstract: A method and system for controlled rate freezing and nucleation of materials is provided. The presently disclosed system and method provides the ability to rapidly cool the materials contained in vials or other containers within a cooling unit via forced convective cooling using a laminar and uniform flow of cryogen in proximity to the plurality of vials disposed within the cooling unit. The rapid cooling of the biological materials is achieved by precisely controlling and adjusting the temperature of the cryogen being introduced to the system as a function of time. The presently disclosed methods to systems also provide nucleation control via temperature quench and depressurized nucleation control.

Abstract: A method and system for controlled rate freezing of biological materials is provided. The presently disclosed system and method provides the ability to rapidly cool the biological materials contained in vials or other containers within a cooling unit via forced convective cooling using a laminar and uniform flow of cryogen in proximity to the plurality of vials disposed within the cooling unit. The rapid cooling of the biological materials is achieved by precisely controlling and adjusting the temperature of the cryogen being introduced to the system as a function of time.

Abstract: A gasoline blend spot sampling system and method including an adjustable volume mechanism for retaining an adjustable volume of gasoline for sampling, a coolant system integrated with the adjustable volume mechanism, and a sample collection assembly using a blunt-end tube for use with an open-mouthed bottle. Various three-way valves are actuated to route gasoline through various stages of a sampling process, from a gasoline fast loop to a purge loop to a gasoline capture stage to a sample bottling stage.

Abstract: An isothermal reaction and analysis system may include a receiver to receive sample holders, a thermal control subsystem to control a temperature of the receiver, an excitation subsystem, a detection subsystem and an analysis subsystem. Excitation sources and/or detectors are positioned to enhance data collection. Sample holders may include filters, selectively blocking and passing wavelengths or bands of electromagnetic radiation.

Abstract: A test apparatus includes a test site, a buffer carrying device, a transport carrying device, a handling mechanism and a dry air flow guide mechanism. The test site performs a test procedure on the objects. The buffer carrying device is disposed close to a side of the test site, holds the objects and performs a temperature conditioning process. The transport carrying device is disposed close to another side of the test site, moves back and forth along a transporting direction, transports the objects into and out of the test site, and heats up the objects. The handling mechanism carries the objects among the buffer carrying device, the test site and the transport carrying device. The dry air flow guide mechanism guides a dry air to surround the test site, the buffer carrying device, the transport carrying device and the handling mechanism and generates a dry environment to prevent dew condensation.

Abstract: The invention provides a method for detaching and/or isolating a histological sample that is adhering to another sample and/or to the inside of a cassette, for example as a result of solidification of an embedding medium within a cassette. The sample is immobilized in a sample receiving chamber above a first fill level of a liquid that is suitable for counteracting the adhesion; and that the fill level of the liquid is then elevated at least until said level reaches the sample. An apparatus according to the present invention that can be used for carrying out the method comprises a sample receiving chamber and an adjusting chamber, the adjusting chamber being connected to the sample receiving chamber in such a way that a change in the fill level height of the liquid in the sample receiving chamber is producible by changing the pressure existing in the adjusting chamber.

Abstract: In a first mode, a monitoring system inputs humidified gas through at least a portion of a conduit. At least a portion of the water in the humidified gas adheres to the inner surface of the conduit, inhibiting contaminants in the gas sample from adhering to the inner surface. The water in the humidified gas may also push any contaminants adhered to the surface of the sample line back out the sample line. In a second mode, after previously passing the humidified gas through the conduit, the monitoring system controls a flow of a gas sample including the contaminants through the conduit to a gas analyzer. The one or more layer of water on the inner surface of the conduit prevents or reduces a buildup of undesirable contaminants on an inner surface of a conduit that conveys gas samples.

Abstract: System and method for natural gas liquid sample pressure regulating vaporizer system including a vented cabinet having a gas sample input, a pressure regulator, a single path vaporizer, a liquid block, a heated regulator and a gas sample outlet, and a communications assembly including a temperature controller, a communication outlet, and a power input electrically connected via appropriate secure feedthroughs to the cabinet.

Abstract: A method, apparatus and system for obtaining a sample of a fluid solids, such as a coke and hydrocarbon mixture, from a fluid solids process is provided. A sample vessel is provided that contains a first end, a second end, an aperture in the first end and an interior cavity. A cooling device can be provided for cooling material in the interior cavity of the sampling vessel. In operation, fluid solids can be routed through the aperture and collected in the interior cavity. The collected sample material can then be cooled by the cooling device and used for testing.

Abstract: The present disclosure describes a method and apparatus for detecting particles in a gas by saturating the gas with vapor and causing the gas to flow through a chamber with walls that are at a temperature different than the temperature of the entering gas creating a gas turbulence within the chamber resulting in the gas becoming super-saturated with vapor and causing said super-saturated vapor to condense on said particles and form droplets, which are then detected and counted by an optical light-scattering detector.

Abstract: A groundwater sampling tool that includes an elongated hollow coring tube having a proximal end and a distal end for collecting groundwater and sediment; a Peltier element located in close proximity to a wall of the elongated hollow coring tube adapted to freeze groundwater and sediment collected by the elongated hollow coring tube.

Abstract: The invention relates to different designs of a microelectronic device comprising an array of heating elements (HE) with local driving units (CU2) and optionally with an array of sensor elements (SE) adjacent to a sample chamber (SC). By applying appropriate currents to the heating elements (HE), the sample chamber can be heated according to a desired temperature profile. The local driving units comprise means for compensating variations of their individual characteristics.

Abstract: Disclosed is an integrated measurement apparatus that may perform measurement of various material characteristics (e.g., thermal conductivity, electrical conductivity, magnetic inductivity, etc.) and defects of a composite material in a non-destructive manner. The apparatus may include: a jig chamber having a door; a first jig device for measuring electrical characteristics, a second jig device for measuring magnetic characteristics, and a third jig device for measuring magnetic characteristics, the three jig devices interchangeably mounted in the jig chamber so that either the first, second, or third jig device may be used to measure a composite material sample.

Abstract: A system and method for concurrently and uniformly removing thermal energy from clustered specimen samples.

Abstract: An adapter device includes a receptacle including at least one receiving element that detachably secures a sample chamber for cryoconservation of a biological sample, and a coupling device that connects the receptacle to a base section which can be secured in a cooling device, wherein the receiving element is 1) immobile in a holding state at a cryoconservation temperature and secures the sample chamber and 2) at least one of deformable and movable in a release state at a temperature above the cryoconservation temperature so that the sample chamber is detachable from the adapter device or can be inserted into the adapter device.

Abstract: The present invention is intended to improve response property and accuracy of temperature control of a liquid sample, and is provided with a vaporization tank that retains the liquid sample, one or more heaters that are provided in the vaporization tank and respectively have heating parts that come into contact with the liquid sample to heat the liquid sample, a temperature detection part that is provided in contact with an outer surface including the heating part of any of the heaters and detects a temperature of the outer surface, and a control part that receives a temperature detection signal from the temperature detection part to control electric power supplied to the heaters.

Abstract: The invention relates to a sensor system (100) comprising a reader (150) with a sensor unit (155, 156) and an accommodation Space (151) for an exchangeable cartridge (110). The cartridge (110) is held in said accommodation space (151) by at least one contact element (111) which has an increased thermal resistance and/or a contact area of reduced size. Thus a more homogenous temperature distribution can be achieved within the cartridge (110), reducing distortions which might adversely affect optical measurements.

Abstract: Disclosed is a sampling method which comprises the steps of: blowing airflow towards a center portion of a sampling surface through a blowing port; and sucking the blown airflow from periphery of the sampling surface through a sucking port, or a sampling method which comprises the steps of: providing a sampling device on a sampling surface, the sampling device being shaped to form a sampling space together with the sampling surface, and the sampling device including a blowing port arranged at the center portion of the sampling device and a sucking port arranged at periphery of the sampling device; blowing airflow towards the sampling surface through the blowing port; and sucking the airflow blown towards the sampling surface through the sucking port so as to collect samples.

Abstract: Instruments, devices and methods of analysis are provided which fully integrate a significant number of process steps in a continuous operation. Accurate positioning and full contact between components is also provided by the relative movement the designs allow. An effect interface between a low cost disposable cartridge or device and the instrument to process it is also detailed.

Abstract: In a sampling head (1) of an analysis arrangement (31), provision is made that a sample stream delivered via a sampling line (2) and a dilution air stream delivered through a dilution air inlet (4) are mixed together in a dilution unit (3) in such a way that a volumetric quantity entrained in at least one receiving space moved along by a movable element (8) between the sampling stream and the dilution air stream are exchanged with each other, wherein the analysis arrangement (31) has a gas analyzer (35) for the analysis of the slightly diluted sample stream and a particle determination unit (32) for the analysis of the enriched dilution air stream.

Abstract: A sampler for an elemental analyzer comprises a sample housing suitable to accommodate one or more samples, sealed in tin or silver capsules, to be analyzed, a closure mechanism suitable to reversibly seal the sample housing, a sample passage having a connection opening for the passage by gravity of the one or more samples from the sampler into the analyzer through the connection opening. The sampler further comprises a heater for heating the sample housing and a vacuum system or other means for pumping out environmental gases and vapors from the sample housing.

Abstract: Provided herein are systems and methods for storage, retrieval and sampling of materials.

Abstract: The invention provides a planar coil (1) of a tube (2), wherein the planar coil (1) has an overall planar shape. The cross-section of the tube (2) can be oval. The invention further provides a heating device comprising one or more of the planar coil (1). The invention further provides a method for heating a sample comprising the step of heating the sample in the heating device of the invention.

Abstract: The present invention relates to a distributable sampling and sensing instrument for chemical analysis of consumable foods and other agricultural products. The distributed sampling system is used to separate and concentrate the chemicals of interest obtained from samples at remote locations via thermal desorption onto a detachable target substrate that can be analyzed on-site or off-site. The volatile components adsorbed onto the target substrate can be analyzed with specific sensors (e.g., electrochemical sensors) or the assembly can be sent to a central lab and analyzed with conventional chemical instrumentation (e.g., GC-MS). This instrument provides the capability to enable chemical analysis of a wide range of chemical species of interest in a wide range of environments and conditions.

Abstract: An apparatus for handling a liquid sample, especially for automatic removal of a liquid sample from a sample-taking location, comprising: a control unit; a sample collecting unit; a supply and metering system, which is embodied to convey a liquid sample from the sample-taking location and to meter the sample into a liquid receptacle of the sample collecting unit; a housing with a first housing part, which at least partially surrounds at least the sample collecting unit, and a second housing part, which is separated from the first housing part, and which at least partially surrounds a metering space; wherein at least parts of the supply and metering system are arranged in the metering space; and wherein the apparatus furthermore includes a plate, which is releasably connected with the second housing part surrounding the metering space, and which divides the metering space into a first metering space part and a second metering space part.

Abstract: Heat sinks for use in assemblies for preheating liquid samples prior to their introduction into an analytical stream. The heater assemblies have a heat sink having a metallic heater block and a heating element for heating the block. The block has a basin for receiving a liquid sample and allowing heat to be transmitted from the block to the sample. A drain at the lower end of the basin allows sample in the basin to flow out of the basin. A passageway extends through the block from the drain to an exterior surface of the block and provides a conduit for sample flowing from the drain, A temperature sensor is mounted in a cavity in the block and extends into the basin to measure the temperature of sample in the basin. A temperature sensor is mounted in a cavity in the block and measures the temperature of the block.

Abstract: Systems and methods are described for laser ablation of an analyte from a specimen and capturing of the analyte in a dispensed solvent to form a testing solution. A solvent dispensing and extraction system can form a liquid microjunction with the specimen. The solvent dispensing and extraction system can include a surface sampling probe. The laser beam can be directed through the surface sampling probe. The surface sampling probe can also serve as an atomic force microscopy probe. The surface sampling probe can form a seal with the specimen. The testing solution including the analyte can then be analyzed using an analytical instrument or undergo further processing.

Abstract: A device for sampling surfaces for the presence of compounds is provided, including a housing having a proximal end adapted to receive it negative pressure gradient and a distal end adapted to contact the surfaces; a heating element spaced from the distal end; a primary filter spaced from the heating element; and a secondary filter spaced from the primary filter, the secondary filter removably received by the housing. Also provided is as method for sampling a surface for the presence of compounds, the method including contacting the surface to dislodge the compounds from the surface; capturing first fractions of the compounds with a primary filter while allowing second fractions of the compounds to pass through the primary filter; heating the primary filter to volatilize the first fractions; capturing the volatized first fractions and the second fractions with a secondary filter; and analyzing the secondary filter to identify the compounds.

Abstract: An apparatus for processing a liquid sample in a sample tube. The apparatus includes a base, a receptacle for receiving a sample tube, and a heating portion coupled to the base to selectively apply heat to the receptacle. A shaking portion is coupled to the base and supports the receptacle. The shaking portion agitates the receptacle with respect to the base. A magnetizing portion is coupled to the base and movable to selectively change a magnetic field with respect to the receptacle.

Abstract: A system for preparing a refrigerant sample for analysis including a pressure regulator assembly including a pressure regulator and provisions for heating a refrigerant sample contained within an interior region of the pressure regulator. The pressure regulator defines an inlet through which the refrigerant sample is delivered and an outlet through which the refrigerant sample is expelled. The system also includes a filter assembly having an inlet that is fluidly connected to the outlet of the pressure regulator to receive the vaporized refrigerant sample from the pressure regulator, at least one filter for removing contaminants from the refrigerant sample, and an outlet that is configured to be coupled to a refrigerant analysis system for analyzing a composition of the refrigerant sample.

Abstract: The present disclosure relates to a method for sampling rock mass, especially jointed rock mass. The present disclosure provides a simple and convenient method for sampling jointed rock mass to prevent the rock sample from being disturbed and damaged during sampling and accordingly resulting in opening of the weak structural planes, to therefore obtain rock specimen correctly reflecting the basic physical and mechanical characteristics of rock mass comprising integral fissure network. The method for sampling jointed rock mass of the present disclosure comprises the following steps: Step a: Siting; Step b: Drilling; Step c: Protecting; and Step d: Sampling. The method is suitable for determining the basic mechanical properties of the rock mass and for assessing the stability of caverns in jointed rock mass.

Abstract: A sampling component including a sampling body that can be electrically heated and an outer surface of which has a wiping sampling area to receive a sample; and an insulated handle that is connected to one longitudinal end of the sampling body. The sampling component contacts directly electrical contacts of an external power supply after being positioned in a analysis chamber, the power supply is turned on to vaporize the sample, and the power is turned off immediately after the sampling component removed from the chamber. The power consumption and a malfunction caused by long-term use of the sampling device under a high temperature can be avoided. A sampling device having the sampling component and an ion mobility spectrometer having the sampling device are also provided.

Abstract: The present invention relates to a cryopreparation chamber (100) for preparing and manipulating a sample for electron microscopy, the cryopreparation chamber (100) being cooled by a primary cryogen, the cryopreparation chamber (100) including a first and a second chamber portion (101,102), the second chamber portion (102) being detachably placeable (101) on the first chamber portion (101), and moreover, the second chamber portion (102) being provided, in its outer wall (106), with an access port (107) through which a specimen holder (108) for an electron microscope can be inserted into the cryopreparation chamber (100). The present invention also relates to a cryopreparation device (200) which is suitable for cryopreparing a sample for an electron microscope and includes such a cryopreparation chamber (100).

Abstract: A system and method for collecting a selected phase of a representative sample from a multiphase fluid flowing through a flowline, preferably located subsea. The system includes a multiphase sampling apparatus attachable to the flowline for sampling the representative sample; a vehicle sampling apparatus (e.g., ROV) locatable proximate the flowline having a power supply and a fluid sample collector for storing at least one selected phase of the representative sample; an interface for connecting the multiphase sampling apparatus and the vehicle sampling apparatus; and a temperature control arrangement disposed between the multiphase sampling apparatus and the vehicle sampling apparatus configured to minimize the temperature difference between the representative sample and the multiphase fluid flowing through the flowline.

Abstract: The present invention includes a heat sealable capsule adapted for use in analysis devices such as GCs, and methods for using the capsules to perform analysis in such devices. The capsules include a tube having an end that is heat-sealed to contain a sample that is to be analyzed at an injection temperature. The tube includes a heat sealable medium having a heat seal that closes the end, the tube having an inner and outer surface, both of the surfaces being substantially chemically inert with respect to the sample. The tube is substantially free of any material that outgases at the injection temperature. The tube is openable without breaking into pieces, and remains intact at the injection temperature. The capsule can include a programmable tag that stores information related to the sample contained therein.

Abstract: An apparatus can include ablation chamber body having a transmission window and defining an accommodation region configured to accommodate a target that is movable relative to the transmission window. An aerosol transmission conduit is configured to transport an aerosol produced within the accommodation region to a sample receiving region of an analysis system along a substantially straight transport path.

Abstract: A sample plate for a biochemical analyzer is provided, which includes a main shaft, an inner plate, an outer plate, a refrigeration bin, a tubing portion, a cooling fluid inlet and a cooling fluid outlet.