Spheroidizing Or Rounding Of Solid Particles Patents (Class 264/15)
  • Patent number: 11633785
    Abstract: Disclosed herein are embodiments of mechanically alloyed powder feedstock and methods for spheroidizing them using microwave plasma processing. The spheroidized powder can be used in metal injection molding processes, hot isostatic processing, and additive manufacturing. In some embodiments, mechanical milling, such as ball milling, can be used to prepare high entropy alloys for microwave plasma processing.
    Type: Grant
    Filed: March 23, 2022
    Date of Patent: April 25, 2023
    Assignee: 6K Inc.
    Inventors: Sunil Bhalchandra Badwe, Makhlouf Redjdal, Scott Joseph Turchetti
  • Patent number: 11266607
    Abstract: A process for manufacturing and using pancreatin micropellet cores and pancreatin micropellets which are substantially free of synthetic oils. In one embodiment, a pharmaceutical composition is provided comprising a pancreatin micropellet with the enteric coating being designed to deliver pancreatin to the upper portion of the intestine of a mammal for release.
    Type: Grant
    Filed: August 15, 2006
    Date of Patent: March 8, 2022
    Assignee: ABBVIE PHARMACEUTICALS GMBH
    Inventors: George Shlieout, Claus-Juergen Koelln, Frithjof Sczesny, Jens Onken, Guido Ruesing
  • Patent number: 10864492
    Abstract: A method for producing biochar aggregate particles that comprising the steps of (i) collecting or producing treated biochar fines less than 1 mm, (ii) adding a binding agent to the fines, (iii) forming the fines and binding agent into solid aggregate particles. The steps may further include, for example, adding additives to the fines, drying the solid aggregate particles, activing the binder after forming the solid aggregate particles with heat or cold temperatures and/or treating the biochar fines prior to forming the aggregate particles.
    Type: Grant
    Filed: May 24, 2019
    Date of Patent: December 15, 2020
    Assignee: Carbon Technology Holdings, LLC
    Inventors: Rajashekharam Malyala, Vern Traxler, Matthew William Smith, Han Suk Kim, Ranko Panayotov Bontchev, Richard Wilson Belcher
  • Patent number: 10806143
    Abstract: The present invention provides light weight, water dispersible, granular compositions containing a first herbicide and a second herbicide in which the first herbicide and the second herbicide have different physical characteristics. In particular, the present invention relates to granular herbicidal compositions comprising a low melting point herbicide, carfentrazone-ethyl, and a high melting point herbicide, sulfosulfuron, having excellent dispersibility in water and chemical and physical stability.
    Type: Grant
    Filed: October 11, 2010
    Date of Patent: October 20, 2020
    Assignee: FMC Corporation
    Inventor: Hong Liu
  • Patent number: 10792240
    Abstract: This invention discloses a novel class of skincare products to remove iron in the skin and its preparation method. The core active components, termed as de-ironizing inducers (DII), consist of a reducing agent and a precipitating agent. The reducing agent is selected from vitamin C, vitamin E, glutathione, vitamin A, vitamin D and their derivatives. The precipitating agent is chosen from calcium carbonate, pearl powder, magnesium carbonate, barium carbonate, calcium phosphate, magnesium phosphate, barium phosphate, calcium silicate, magnesium silicate, and barium silicate. Molar ratios of the reducing agent with the precipitating agent range from 1:3-6 and the core components in the skin care product range from 5% to 10% w/w. The PH value of the skincare product is between 6.6 and 7.4. The skin care products can safely and effectively remove iron in the skin, which has been shown to accelerate skin's natural aging and photoaging.
    Type: Grant
    Filed: February 22, 2013
    Date of Patent: October 6, 2020
    Assignee: Fe:I Beauty Tech, Inc.
    Inventor: Xi Huang
  • Patent number: 10633855
    Abstract: An insulative construction product includes a polyurethane foam core and a mixture of Aerogel and carbon black that is disposed within the polyurethane foam core. The mixture of Aerogel and carbon black includes between 90 and 99 weight percent Aerogel and between 1 and 10 weight percent carbon black. The polyurethane foam core includes between 10 and 90 percent by volume of the of Aerogel and carbon black mixture and the construction product has an R-value of at least 8.0 R/inch.
    Type: Grant
    Filed: December 1, 2017
    Date of Patent: April 28, 2020
    Assignee: Johns Manville
    Inventors: Guodong Zheng, Luke S Weith, Malay Nandi, Lance Wang, Jawed Asrar
  • Patent number: 10619013
    Abstract: A composite material includes a resinous particulate material, and an inorganic particulate material having a particle diameter being smaller than that of the resinous particulate material, fused welded onto a surface of the resinous particulate material, formed of an inorganic oxide, and including OH groups generated by fuse welding in the surface. The composite particulate material exhibits a degree of sphericity of 0.8 or more, and a has volumetric average particle diameter of from 0.1 to 100 ?m.
    Type: Grant
    Filed: November 5, 2019
    Date of Patent: April 14, 2020
    Assignee: ADMATECHS CO., LTD.
    Inventors: Hiroyuki Onda, Nobutaka Tomita, Yuki Arai
  • Patent number: 10545622
    Abstract: A recording layer is described that comprises a magnetizable material configured to store an image represented by magnetized regions of the magnetizable material. The magnetizable material may be brought into proximity with a magnetically responsive display layer, which may cause a change in an optical state of the display layer such that a facsimile of the image represented by the magnetized regions is produced within the display layer.
    Type: Grant
    Filed: May 20, 2017
    Date of Patent: January 28, 2020
    Assignee: E Ink Corporation
    Inventor: Richard J. Paolini, Jr.
  • Patent number: 10378111
    Abstract: Provided is a coated metal sheet for exterior use, having a metal sheet, and a top coat film situated on the metal sheet. The top coat film contains a resin, 0.2-15 volume percent of a gloss control agent composed of porous particles, and a delustering agent composed of primary particles. The coated metal sheet satisfies the following expressions in which, in the number-size distribution of the gloss control agent and the delustering agent, R is the number-average particle diameter (?m) of the gloss control agent, D197.5 and D297.5 are 97.5% particle diameter values (?m) of the gloss control agent and the delustering agent, Ru is the upper limit particle diameter (?m) of the gloss control agent, and T is the film thickness (?m) of the top coat film. D197.5/T?0.7 Ru?1.2T R?1.0 2.0?D297.5/T?7.0 13?T?20.
    Type: Grant
    Filed: December 16, 2014
    Date of Patent: August 13, 2019
    Assignee: NIPPON STEEL NISSHIN CO., LTD.
    Inventors: Taketo Hara, Koichiro Ueda, Kenji Sakato, Kazuhiko Takahashi
  • Patent number: 10319313
    Abstract: Video displays using relatively low frame rates of about 10 to about 20 frames per second, but having acceptable video quality are described. The displays may use bistable media, and may be driven such that the medium, when driven, changes its optical properties continuously during the driving of each frame. The displays may use an electro-optic medium such that the frame period is from about 50 to about 200 per cent of the switching time of the electro-optic medium at the driving voltage used.
    Type: Grant
    Filed: May 21, 2008
    Date of Patent: June 11, 2019
    Assignee: E Ink Corporation
    Inventors: George G. Harris, Shamus Ford Patry, Michael D. McCreary
  • Patent number: 10126678
    Abstract: A toner includes a binder resin. Particles of a metal complex or a salt of an aromatic carboxylic acid derivative having a number-average particle diameter of from 0.2 ?m to 1.0 ?m are present on the surface of the toner. A coverage of the particles of a metal complex or a salt of an aromatic carboxylic acid derivative over the surface of the toner is from 10% to 50%.
    Type: Grant
    Filed: September 27, 2016
    Date of Patent: November 13, 2018
    Assignee: Ricoh Company, Ltd.
    Inventors: Shizuka Hashida, Hiroshi Yamashita, Minoru Masuda, Hiroshi Yamada, Masanori Rimoto
  • Patent number: 10072213
    Abstract: A fireproof material incorporating aerogel with an organic foam material and a method for making the same are provided. The method is carried out as follows: A. a mixed solution of a precursor and an organic solvent is added with an acid catalyst and becomes an anhydrous aerogel solution through hydrolysis; B. the anhydrous aerogel solution is added with an aqueous alkali catalyst solution and forms an aerogel solution through condensation; C. an organic foam material is impregnated with the aerogel solution such that aerogel is generated by gelation and is incorporated with the organic foam material, forming a three-dimensional reticular structure; and D. the organic foam material incorporated with the aerogel is dried and then shaped to produce a fireproof material. The fireproof material is highly proof against fire and can pass the limiting oxygen index test.
    Type: Grant
    Filed: October 20, 2016
    Date of Patent: September 11, 2018
    Inventor: Jean-Hong Chen
  • Patent number: 9855605
    Abstract: In a method of manufacturing metal powders in a continuous type, metal is heated at a temperature greater than a melting point to form a liquid phase metal, and the liquid phase metal and an emulsion carrier, which is emulsified without reacting with the liquid phase metal, are supplied into a container, and the liquid phase metal and the emulsion carrier are emulsified through Taylor flow to form an emulsion solution. The emulsion solution is discharged from the container, and then, the emulsion solution is cooled at a temperature smaller than the melting point to selectively solidifying the liquid phase metal in the emulsion solution to form the metal powders.
    Type: Grant
    Filed: March 17, 2015
    Date of Patent: January 2, 2018
    Assignee: KOREA UNIVERSITY RESEARCH AND BUSINESS FOUNDATION
    Inventors: Woo Young Yoon, Jun Kyu Lee, Sung Man Cho
  • Patent number: 9745201
    Abstract: The purpose of the present invention is to provide: a synthetic amorphous silica powder which is suitable as a raw material for a synthetic silica glass product used in a high-temperature and reduced-pressure environment, which can yield a synthetic silica product such that the occurrence or expansion of air bubbles in the glass product is inhibited even in use in a high-temperature and reduced-pressure environment, and which can be obtained at a relatively low cost; and a process for manufacturing the same.
    Type: Grant
    Filed: December 10, 2014
    Date of Patent: August 29, 2017
    Assignee: MITSUBISHI MATERIALS CORPORATION
    Inventor: Toshiaki Ueda
  • Patent number: 9688832
    Abstract: A method for preparing macroporous polymethyl methacrylate (PMMA) particles includes the steps of: (a) dissolving a polymethyl methacrylate polymer and Pluronic polymer into an organic solvent; (b) introducing the mixed solution of step (a) to an aqueous solution containing a surfactant to carry out emulsion polymerization; (c) heating the resultant product of step (b) to allow evaporation of the organic solvent; and (d) washing and drying the porous polymethyl methacrylate particles remaining after the evaporation.
    Type: Grant
    Filed: March 18, 2014
    Date of Patent: June 27, 2017
    Assignee: COSMAX CO., LTD.
    Inventors: Jun Bae Lee, Chun Ho Park, Hee Chang Ryoo
  • Patent number: 9665021
    Abstract: A heat treating apparatus for powder particles including a cylindrical treating chamber; a powder particle-supplying unit; a hot air-supplying unit that supplies hot air for heat-treating powder particles; a cold air-supplying unit that supplies cold air for cooling the heat-treated powder particles; a regulating unit for regulating a flow of the supplied powder particles; and a recovering unit that recovers the heat-treated powder particles. The regulating unit is a substantially circular columnar member, the hot air-supplying unit has an outlet opposite to the upper end portion of the columnar member, and the regulating unit is equipped with a substantially conic distributing member for distributing the supplied hot air in a circumferential direction and a rotating member for rotating the distributed hot air in a spiral manner, on the center of the upper end portion.
    Type: Grant
    Filed: June 11, 2012
    Date of Patent: May 30, 2017
    Assignee: CANON KABUSHIKI KAISHA
    Inventors: Takeshi Ohtsu, Yuichi Mizo, Hironori Minagawa, Takakuni Kobori, Kohji Takenaka, Junichi Hagiwara, Daisuke Ito, Kunihiko Kawakita
  • Patent number: 9226874
    Abstract: Disclosed are methods for marking a pharmaceutical product, container or pharmaceutical packaging system with a scent to establish the identity and/or source of the pharmaceutical.
    Type: Grant
    Filed: September 14, 2010
    Date of Patent: January 5, 2016
    Assignee: Purdue Pharma L.P.
    Inventor: Sheryl E. Siegel
  • Patent number: 9023259
    Abstract: A method for processing feed material to produce dense and spheroidal products is described. The feed material is comprised of powder particles from the spray-drying technique or solution precursor droplets from ceramic or metallic materials. The feed material is processed using plasma generated from a microwave. The microwave plasma torch employed is capable of generating laminar flow during processing which allows for the production of spheroidal particles with a homogenous materials distribution. This results in products having improved thermal properties, improved corrosion and wear resistance and a higher tolerance to interface stresses.
    Type: Grant
    Filed: November 13, 2012
    Date of Patent: May 5, 2015
    Assignee: Amastan Technologies LLC
    Inventors: Kamal Hadidi, Makhlouf Redjdal
  • Patent number: 8986581
    Abstract: A method for producing biochar particles or pellets which use sulphur and other additives. The method includes producing a mixture with biochar and additives selected from sulphur, lignin, and gluten. The mixture is mixed with water and passed through an extruder to produce an extrudate. The extrudate is then cut into pellets. The pellets are then tumbled/spun with each other and heated to result in mostly spheroidal pellets whose mechanical characteristics allow them to be used with well-known agricultural equipment. The biochar can be produced with sulphur incorporated as an outer coating. To produce this sulphur coated biochar, the method includes feeding a biomass feedstock to a pyrolysis reactor, pyrolyzing the feedstock into biochar particles, size-sorting the biochar particles, and coating the biochar particles with the sulphur coating material.
    Type: Grant
    Filed: July 25, 2013
    Date of Patent: March 24, 2015
    Assignee: Carbron Basis Company Ltd.
    Inventors: Leonard Bruce Eddy, Jack Wolstenholme, Paul Byron Tiege, Nancy Yadira Meza Trevino, Jesus Josafath Quezada Rivera
  • Publication number: 20150057356
    Abstract: A melt-extruded polymer composition comprising a) at least one cellulose ether, b) one or more active ingredients and c) one or more optional additives, wherein said at least one cellulose ether has an MS (hydroxyalkyl) of 0.05 to 0.55 and hydroxyl groups of anhydroglucose units are substituted with methyl groups such that [s23/s26?0.2*MS(hydroxyalkyl)] is 0.32 or less, wherein s23 is the molar fraction of anhydroglucose units wherein only the two hydroxyl groups in the 2- and 3-positions of the anhydroglucose unit are substituted with a methyl group and wherein s26 is the molar fraction of anhydroglucose units wherein only the two hydroxyl groups in the 2- and 6-positions of the anhydroglucose unit are substituted with a methyl group.
    Type: Application
    Filed: April 8, 2013
    Publication date: February 26, 2015
    Inventors: Nicholas S. Grasman, True L. Rogers, Oliver Petermann, Meinolf Brackhagen, Roland Adden
  • Publication number: 20140348914
    Abstract: Improved oral dosage forms of methyl hydrogen fumarate and prodrugs thereof are disclosed. Methods of treating diseases such as multiple sclerosis and psoriasis using such dosage forms are also disclosed.
    Type: Application
    Filed: August 22, 2013
    Publication date: November 27, 2014
    Applicant: XenoPort, Inc.
    Inventors: Sami Karaborni, Sarina Grace Harris Ma, Chen Mao, Ching Wah Chong, Peter Robert Prinz Freed, Mesut Ciper, Stefanie Krenzlin, David J. Wustrow, Peter A. Virsik
  • Publication number: 20140342093
    Abstract: A method for processing feed material to produce dense and spheroidal products is described. The feed material is comprised of powder particles from the spray-drying technique or solution precursor droplets from ceramic or metallic materials. The feed material is processed using plasma generated from a microwave. The microwave plasma torch employed is capable of generating laminar flow during processing which allows for the production of spheroidal particles with a homogenous materials distribution. This results in products having improved thermal properties, improved corrosion and wear resistance and a higher tolerance to interface stresses.
    Type: Application
    Filed: May 19, 2014
    Publication date: November 20, 2014
    Applicant: Amastan LLC
    Inventors: Kamal Hadidi, Makhlouf Redjdal
  • Patent number: 8883110
    Abstract: The synthetic amorphous silica powder of the present invention is characterized in that it comprises a synthetic amorphous silica powder obtained by applying a spheroidizing treatment to a granulated silica powder, and by subsequently cleaning and drying it so that the synthetic amorphous silica powder has an average particle diameter D50 of 10 to 2,000 ?m; wherein the synthetic amorphous silica powder has: a quotient between 1.35 exclusive and 1.75 inclusive obtained by dividing a BET specific surface area of the powder by a theoretical specific surface area calculated from the average particle diameter D50; a real density of 2.10 to 2.20 g/cm3; an intra-particulate porosity of 0 to 0.05; a circularity between 0.50 inclusive and 0.75 inclusive; and a spheroidization ratio between 0.20 inclusive and 0.55 exclusive.
    Type: Grant
    Filed: December 27, 2010
    Date of Patent: November 11, 2014
    Assignee: Mitsubishi Materials Corporation
    Inventor: Toshiaki Ueda
  • Publication number: 20140272116
    Abstract: The invention relates to titanium diboride granules comprising aggregates of titanium diboride primary particles, wherein the titanium diboride granules have a rounded shape and are fracture-resistant. The invention further relates to a method for producing these titanium diboride granules, the use thereof for covering graphite cathodes in electrolytic cells in Al fused-salt electrolysis or for repairing holes in cathode bases of electrolytic cells and also a method for repairing holes in cathode bases of electrolytic cells.
    Type: Application
    Filed: August 2, 2012
    Publication date: September 18, 2014
    Applicant: ESK CERAMICS GMBH & CO. KG
    Inventors: Martin Engler, Georg Victor
  • Publication number: 20140264984
    Abstract: Speriodal polymer beads having a uniform size are prepared by polymerizing uniformly sized monomer droplets formed by dispersing a polymerizable monomer phase over double-walled cylindrical cross-flow membrane into an aqueous phase. A shear force is provided at a point of egression of the polymerizable monomer phase into the aqueous phase, the direction of shear substantially perpendicular to the direction of egression of the monomer phase. The polymer beads can be employed in applications where beads having uniform diameters of 10 to 200 ?m are useful.
    Type: Application
    Filed: March 15, 2013
    Publication date: September 18, 2014
    Applicant: PUROLITE CORPORATION
    Inventor: Serguei Rudolfovich Kosvintsev
  • Publication number: 20140248493
    Abstract: The present invention provides a spherical carbon material in the form of isotropic particles which undergoes a considerably less change in shape even after subjected to carbonization or graphitization, and has a good crystal growth property. The present invention relates to a raw coke spherical carbon material in which an average of a plane-direction sphericity and an elevation-direction sphericity of particles of the spherical carbon material as measured in plane and elevation directions of particles of the spherical carbon material, respectively, by observation using a scanning electron microscope is not less than 60%, and a shape retention rate of the spherical carbon material after being heated at 1200° C. for 5 hr and then at 2800° C.
    Type: Application
    Filed: October 2, 2012
    Publication date: September 4, 2014
    Applicant: Toda Kogyo Corp.
    Inventors: Seiji Okazaki, Wataru Oda, Tomoaki Urai, Akio Sakamoto
  • Publication number: 20140227600
    Abstract: The purpose of the present invention is to provide: a composite active material for lithium secondary batteries, which is capable of providing a lithium secondary battery that has large charge and discharge capacity, high-rate charge and discharge characteristics and good cycle characteristics at the same time; and a method for producing the composite active material for lithium secondary batteries.
    Type: Application
    Filed: August 10, 2012
    Publication date: August 14, 2014
    Inventor: Naoyoshi Kachi
  • Patent number: 8790440
    Abstract: In certain embodiments, a material comprising one or more semiconductive substances is vaporized to generate a vapor phase condensate. The vapor phase condensate is allowed to form nanoparticles. The nanoparticles are annealed to yield substantially spherical nanoparticles.
    Type: Grant
    Filed: November 8, 2010
    Date of Patent: July 29, 2014
    Assignee: Raytheon Company
    Inventor: Kalin Spariosu
  • Patent number: 8771455
    Abstract: Provided is a process for production of composite fine particles with heterogeneous surfaces. The process ensures a high productivity and enables a voluntary control of particle diameters. Further, the process imposes no restrictions on heterogeneous substances added for functional expression, and allows a heterogeneous substance to be encapsulated in central portions of composite fine particle spheres. A composite film obtained by laminating two or more kinds of films is cut into minute pieces, followed by melting the same to obtain spherical minute pieces. Particularly, liquid films are separately formed with two or more kinds of liquids containing polymerizable monomers. Further, two or more kinds of films can thereby be obtained through polymerization. The two or more kinds of films thus obtained are then laminated to further allow polymerization to take place, thus obtaining the composite film.
    Type: Grant
    Filed: December 13, 2010
    Date of Patent: July 8, 2014
    Assignees: Niigata University, Sekisui Chemical Co., Ltd
    Inventor: Masato Tanaka
  • Publication number: 20140138862
    Abstract: A highly efficient process is disclosed for making proppants from generally non-spherical or discretized raw material, such as naturally occurring sand or pelletized refractory material. In one embodiment of the process, the discretized material is heated by a counter-current flow of hot gas in a first Moving Bed Gas-Solids Direct Contact Heat Exchanger (MBGSDCHX). The heated discretized material is then further heated to a transformative temperature by a raw material transformation means to a partially or fully melted state in which the discretized raw material assumes generally spherical shapes. The spheres are then cooled by a counter-current flow of cold gas in a second MBGSDCHX. The cooled spheres are then size-classified for use as proppants. In an alternate embodiment, refractory raw material is melted and then discretized into molten drops. The molten drops are cooled and frozen into generally spherical shapes. The cooled spheres are used as proppants.
    Type: Application
    Filed: June 19, 2012
    Publication date: May 22, 2014
    Inventor: Daniel Mark St. Louis
  • Publication number: 20140131906
    Abstract: A method for processing feed material to produce dense and spheroidal products is described. The feed material is comprised of powder particles from the spray-drying technique or solution precursor droplets from ceramic or metallic materials. The feed material is processed using plasma generated from a microwave. The microwave plasma torch employed is capable of generating laminar flow during processing which allows for the production of spheroidal particles with a homogenous materials distribution. This results in products having improved thermal properties, improved corrosion and wear resistance and a higher tolerance to interface stresses.
    Type: Application
    Filed: November 13, 2012
    Publication date: May 15, 2014
    Inventors: Kamal Hadidi, Makhlouf Redjdal
  • Publication number: 20140065211
    Abstract: Improved oral dosage forms of methyl hydrogen fumarate and prodrugs thereof are disclosed. Methods of treating diseases such as multiple sclerosis and psoriasis using such dosage forms are also disclosed.
    Type: Application
    Filed: August 22, 2013
    Publication date: March 6, 2014
    Applicant: XenoPort, Inc.
    Inventors: Sami Karaborni, Sarina Grace Harris Ma, Chen Mao, Ching Wah Chong, Peter Robert Prinz Freed, Mesut Ciper, Stefanie Krenzlin, David J. Wustrow, Peter A. Virsik
  • Publication number: 20140044787
    Abstract: The present application discloses a sustained release composition in pellet form, wherein the core of the pellet comprises: (a) a therapeutically effective amount of a medicament; (b) 0.5 to 50% by weight of a water-soluble polymer; and (c) 1 to 25% by weight of a water-insoluble polymer applied as an aqueous latex dispersion and subsequently the water is removed, wherein the sum of the percentages of the medicament, the water-insoluble polymer and the water-soluble polymer is equal to or less than 100%. It also discloses methods of making this composition.
    Type: Application
    Filed: October 18, 2013
    Publication date: February 13, 2014
    Applicant: NOSTRUM PHARMACEUTICALS, LLC
    Inventor: Nirmal MULYE
  • Publication number: 20140042654
    Abstract: Fulvestrant nanosphere/microsphere and preparation method and use thereof are provided in the present invention. The carrier material of the fulvestrant nanosphere/microsphere is methoxy ended polyethylene glycol-polylactic acid block copolymer. The nanosphere/microsphere is prepared by solvent-nonsolvent method, in-liquid drying method and/or spray drying method, and has the features of high drug loading and high encapsulation efficiency, controllable release of medicine and no irritant to application site or blood vessel. The fulvestrant nanosphere/microsphere can be used to treat metastatic advanced breast cancer in post-menopausal woman.
    Type: Application
    Filed: October 17, 2013
    Publication date: February 13, 2014
    Applicant: Xi'an Libang Pharmaceutical Technology Co., Ltd.
    Inventors: Renle Hu, Jiucheng Wang, Yaqi Jiao, Hua Liang, Duohao Ding
  • Publication number: 20140035180
    Abstract: A single stage straight forward process for extraction and isolation of lutein ester from the dried petals of marigold flowers Tagetes species using the carbondioxide as the supercritical fluid was developed. The pressure maintained for the extraction was up to 625 bar and at temperature up to 750 Centigrade. Lutein ester of high strength and purity up to 70% was achieved for the first time in single stage from the dried petals of marigold flowers-Tagetes species while enrichment of the lutein ester content up to 98% was achieved by crystallization of the lutein ester obtained from supercritical carbon dioxide extract (SCFE). The high strength and purified lutein ester isolated by supercritical fluid-single stage extraction process are free from saturated fat, oil, waxy impurities and serve as a safe source of nutritional supplement for human consumption and color additive for human foods.
    Type: Application
    Filed: January 12, 2012
    Publication date: February 6, 2014
    Applicant: India Glycols Limited
    Inventors: Uma Shankar Bhartia, Gopu Bala Show Reddy
  • Publication number: 20140030250
    Abstract: A method for producing biochar particles or pellets which use sulphur and other additives. The method includes producing a mixture with biochar and additives selected from sulphur, lignin, and gluten. The mixture is mixed with water and passed through an extruder to produce an extrudate. The extrudate is then cut into pellets. The pellets are then tumbled/spun with each other and heated to result in mostly spheroidal pellets whose mechanical characteristics allow them to be used with well-known agricultural equipment. The biochar can be produced with sulphur incorporated as an outer coating. To produce this sulphur coated biochar, the method includes feeding a biomass feedstock to a pyrolysis reactor, pyrolyzing the feedstock into biochar particles, size-sorting the biochar particles, and coating the biochar particles with the sulphur coating material.
    Type: Application
    Filed: July 25, 2013
    Publication date: January 30, 2014
    Applicant: Carbon Basis Company Ltd.
    Inventors: Leonard Bruce EDDY, Jack WOLSTENHOLME, Paul Byron TIEGE, Nancy Yadira MEZA TREVINO, Jesus Josafath QUEZADA RIVERA
  • Patent number: 8632709
    Abstract: A process for efficiently producing a water-dispersible particulate agricultural-chemical composition having improved disintegrability/dispersibility in water, the composition having a particular size in the range of 50-1,000 ?m. The process is characterized by comprising the following steps (a) to (e): (a) a step of kneading an agricultural-chemical active ingredient, a surfactant, and water; (b) a step of extruding the resultant mixture through a screen having pores 600-2,000 ?m in diameter to form granules; (c) a step of drying the granules; (d) a step of rotating two toothed rolls with irregularities on the surface arranged in parallel to each other, and leading the dried granules to pass between the toothed rolls thereby pulverizing the granules; and (e) a step of sieving the pulverized granules.
    Type: Grant
    Filed: November 4, 2009
    Date of Patent: January 21, 2014
    Assignees: Kumiai Chemical Industry Co., Ltd., Nippon Soda Co., Ltd.
    Inventors: Shigeki Fujita, Kazunori Kurita
  • Publication number: 20130345100
    Abstract: A ceramic propping agent, in the form of a spherical pellet, and containing common mineral particulate. The desired propping agent is defined as a particulate ceramic made from raw materials which may be comprised of about: 10%-90% parts by weight of a naturally occurring mineral particulate, 30%-70% parts by weight aluminosilicate network modifier, 0.25-20% parts by weight strength enhancer, and at least one part, typically less than 10% by weight, binder. For use in oil and/or natural gas wells as a hydraulic fracturing proppant.
    Type: Application
    Filed: June 21, 2013
    Publication date: December 26, 2013
    Applicant: Brownwood Clay Holdongs, LLC
    Inventors: Bryan Dell Geary, David Glenn Hall, Carlton Frazier Sorrell, Gary J. Davis, Richard F. Watkins
  • Patent number: 8603930
    Abstract: The present invention provides a high-purity fused and crushed stabilized zirconia powder. The powder—with or without further processing, such as plasma spheroidization—is used in thermal spray applications of thermal barrier coatings (TBCs) and high-temperature abradables. The resulting coatings have a significantly improved high temperature sintering resistance, which will enhance the durability and thermal insulation effect of the coating.
    Type: Grant
    Filed: April 25, 2007
    Date of Patent: December 10, 2013
    Assignee: Sulzer Metco (US), Inc.
    Inventors: Jacobus C. Doesburg, Mitchell R. Dorfman, Liangde Xie
  • Patent number: 8563460
    Abstract: A catalyst unit is described comprising a cylinder with a length C and a diameter D, wherein said unit has five holes arranged in a pentagonal pattern extending longitudinally therethrough, with five flutes running along the length of the unit, said flutes positioned equidistant adjacent holes of said pentagonal pattern. The catalyst may be used particularly in steam reforming reactors.
    Type: Grant
    Filed: August 24, 2009
    Date of Patent: October 22, 2013
    Assignee: Johnson Matthey PLC
    Inventors: David James Birdsall, Mileta Babovic, Mikael Per Uno Carlsson, Samuel Arthur French, Michiel Nijemeisland, William Maurice Sengelow, Edmund Hugh Stitt
  • Patent number: 8557729
    Abstract: A catalyst unit is described in the form of a cylinder having a length C and diameter D, which has two or more flutes running along its length, wherein said cylinder has domed ends of lengths A and B, such that (A+B+C)/D is in the range 0.50 to 2.00, and (A+B)/C is in the range 0.40 to 5.00. The catalyst may be used particularly in reactions where hydrogen is a reactant such as hydroprocessing, hydrogenation, water-gas shift reactions, methanation, hydrocarbon synthesis by the Fischer-Tropsch reaction, methanol synthesis and ammonia synthesis.
    Type: Grant
    Filed: August 24, 2009
    Date of Patent: October 15, 2013
    Assignee: Johnson Matthey PLC
    Inventors: Daniel Lee Cairns, Mileta Babovic, Terence James Fitzpatrick, Elizabeth Margaret Holt, Colin William Park, William Maurice Sengelow, Edmund Hugh Stitt
  • Patent number: 8557728
    Abstract: A catalyst unit is described in the form of a cylinder having a length C and diameter D, which has one or more holes extending therethrough, wherein said cylinder has domed ends of lengths A and B, such that (A+B+C)/D is in the range 0.50 to 2.00, and (A+B)/C is in the range 0.40 to 5.00. The catalyst or catalyst unit preferably has one or more flutes miming along its length. The catalyst may be used particularly in steam reforming reactors.
    Type: Grant
    Filed: August 24, 2009
    Date of Patent: October 15, 2013
    Assignee: Johnson Matthey PLC
    Inventors: David James Birdsall, Mileta Babovic, Mikael Per Uno Carlsson, Samuel Arthur French, Michiel Nijemeisland, William Maurice Sengelow, Edmund Hugh Stitt
  • Publication number: 20130241094
    Abstract: The present invention is a preparation method for asphalt-based spherical activated carbon which requires no infusibilization process. Placing coal tar asphalt into a melting device; introducing compressed air of 0.1 MPa-0.5 MPa into the device and stirring until a melting temperature of 280° C.-350° C. is reached; continuing for 2-8 hours until the base material has a softening point of 200° C.-260° C.; after cooling down, pulverizing the base material to obtain asphalt powder. Obtaining 34%-79% by mass of carbon powder, 1%-10% by mass of binder, and 20%-65% by mass of the asphalt powder and then forming spherical particles with a diameter of 0.5 mm-5 mm with the carbon powder, the binder and the asphalt powder at room temperature. Introducing the spherical particles of asphalt directly into an asphalt carbonization furnace for carbonization at a temperature of 600° C.-900° C. under protection of an inert gas to obtain asphalt spherical carbon.
    Type: Application
    Filed: February 20, 2012
    Publication date: September 19, 2013
    Applicants: SHENZHEN BATIAN ECOTYPIC ENGINEERING CO.,LTD.
    Inventors: Xiangmin Yu, Yizhou Kong
  • Patent number: 8501056
    Abstract: The invention relates to a method for the solvent-free preparation of a homogenizate, especially for implants or microparticles, wherein one or more polymers and one or more active constituents, as raw materials, are homogenized together below the glass transition temperature of the polymer(s) and, when homogenization is complete, brought to room temperature.
    Type: Grant
    Filed: May 23, 2002
    Date of Patent: August 6, 2013
    Assignee: Hexal AG
    Inventors: Gregor Schütz, Brigitte Freudensprung
  • Publication number: 20130172617
    Abstract: The invention concerns a method for preparing a complex of an acid chosen from among methionine, 2-hydroxy-4-methylthiobutanoic acid (HMTBA) and lactic acid, and of at least one metal, starting from said acid and a mineral metal source, wherein the acid is caused to react with the mineral metal source in an extruder.
    Type: Application
    Filed: September 21, 2011
    Publication date: July 4, 2013
    Applicant: ADISSEO IRELAND LIMITED
    Inventors: Jean-Claude Le Thiesse, Patrick Rey, Vivien Henryon
  • Patent number: 8455402
    Abstract: Fluid systems may contain elements to provide changes in bulk fluid density in response to various environmental conditions. One environmental driver to the variable density is pressure; other environmental drivers include, but are not limited to, temperature or changes in chemistry. The variable density of the fluid is beneficial for controlling sub-surface pressures within desirable pore pressure and fracture gradient envelopes. The variability of fluid density permits construction and operation of a wellbore with much longer hole sections than when using conventional single gradient fluids.
    Type: Grant
    Filed: November 29, 2012
    Date of Patent: June 4, 2013
    Assignee: Baker Hughes Incorporated
    Inventors: Larry A. Watkins, Roger W. Fincher
  • Publication number: 20130113129
    Abstract: This invention relates to coated digestive enzyme preparations and enzyme delivery systems and pharmaceutical compositions comprising the preparations. This invention further relates to methods of preparation and use of the systems, pharmaceutical compositions and preparations to treat persons having ADD, ADHD, autism, cystic fibrosis and other behavioral and neurological disorders.
    Type: Application
    Filed: October 25, 2012
    Publication date: May 9, 2013
    Inventors: Joan M. Fallon, Matthew Heil
  • Patent number: 8420578
    Abstract: A low-density ceramic proppant is formed from a light aggregate of a natural mineral and a ceramic binding material in the form of a proppant granule. The light aggregate expands in volume when burnt so that the density of the aggregate is changed. A method of preparing a proppant material is carried out by pre-crushing and pre-mixing of raw components. This is followed by their granulation into proppant granules, drying and screening of the granules to a selected size. The raw components include at least a ceramic binding material and a light aggregate of a natural mineral that, when burnt, expands in volume so that the specific volume of the aggregate is changed. The burning of the light aggregate may be accomplished before or after the aggregate is mixed with the binding material.
    Type: Grant
    Filed: April 10, 2008
    Date of Patent: April 16, 2013
    Assignee: Schlumberger Technology Corporation
    Inventors: Zinaida Yurievna Usova, Elena Mikhailovna Pershikova
  • Publication number: 20130064896
    Abstract: The disclosure provides multiparticulate systems that give release of active agents with a narrow window of absorption such that there is bioavailability to a patient. The disclosure provides a composition comprising microparticulates comprising a swellable hydrophilic polymer and an active agent, wherein the swellable hydrophilic polymer is substantially non-crosslinked intramolecularly, and the size of the microparticulates is about 500 ?m or less.
    Type: Application
    Filed: December 28, 2010
    Publication date: March 14, 2013
    Inventors: Laman Lynn Alani, Jim H. Kou, Shook-Fong Chin, Guangbin Ding, Natasha G. Masand
  • Patent number: 8393892
    Abstract: A burner for production of inorganic spheroidized particles according to the present invention includes a raw material powder supply path that supplies raw material powder by using oxygen or an oxygen-enriched air as a carrier gas; a powder diffusion plate having a plurality of fine holes, which is provided at a downstream end of the raw material powder supply path; a raw material diffusion chamber that is formed in a diffusion pipe provided at a downstream end of the powder diffusion plate; a fuel supply path disposed around the outer circumference of the raw material powder supply path; an oxygen supply path disposed around the outer circumference of the fuel supply path; and a combustion chamber disposed at a downstream side of the raw material diffusion chamber, which has an inside diameter increasing along the downstream direction and communicates with the fuel supply path and the oxygen supply path.
    Type: Grant
    Filed: May 30, 2007
    Date of Patent: March 12, 2013
    Assignee: Taiyo Nippon Sanso Corporation
    Inventors: Yoshiyuki Hagihara, Kazuro Suzuki, Shinichi Miyake, Yasuyuki Yamamoto