Abstract: This invention relates to metal-containing inserts, such as transformers, that are encapsulated, via compression molding processes, with at least one wet lay thermoplastic sheet material and that do not experience significant visible cracking during heat cycling.
Type:
Grant
Filed:
October 21, 1996
Date of Patent:
November 18, 1997
Assignee:
E. I. du Pont de Nemours and Company
Inventors:
M. Lana Sheer, Lloyd Fox, John Carl Solenberger
Abstract: An improved process for preparing thermoplastic polymer blends which contain at least 50% by weight of polyamide as a principal component with the remainder consisting essentially of an ionic polymer component which is derived from an olefin/acid copolymer in which the polyamide and the ionic polymer are combined into a uniform mixture via melt blending at high shear, and the improvement comprises simultaneously contacting the mixture while in the melt with one or more neutralizing basic metal compounds in an amount sufficient to neutralize from 100% up to 200% of the acid groups present in the ionic polymer component.
Abstract: An improved process for preparing high molecular weight polyester polymers, such as poly(butylene terephthalate), an alkylene glycol and a di- or tricarboxylic acid by first preparing a pre-polymer in the form of uniform solid particles having an intrinsic viscosity of from 0.1 to about 0.3 dL/gm and a chemical composition which contains greater than a 1% stoichiometric excess of the alkylene glycol above the amount required to produce a high molecular weight polymer, and polymerizing the pre-polymer in the solid state.
Abstract: An electroconductive powder composition of antimony-containing tin oxide with an outer layer of hydrous metal oxide having an isoelectric point in the range from about 5 to 9.
Abstract: An improved method and apparatus for preparing low-concentration polysilicate microgels from a water soluble silicate and a strong acid in which the silicate and acid are mixed at a rate to produce a Reynolds number of at least 4000, the mixture is aged and then diluted to a silica concentration of not more than 1.0 wt. %.
Abstract: Apparatus for shock-induced phase transformations in materials where two opposing shock waves pass coaxially through the material to be shocked from either end of its axial dimension on a converging path to a point where the shock waves collide.
Abstract: The manufacture of hydrogen cyanide by the catalytic reaction of air/oxygen, ammonia and a hydrocarbon gas employing an improved catalytic reaction zone comprising a sequential array of layers/piles in which the surface density of the catalyst in layers/piles decreases from the entrance to the exit of the catalytic reaction zone.
Abstract: An electroconductive composition comprising a two-dimensional network of antimony-containing tin oxide crystallites in association with amorphous silica, the composition according to one aspect of the invention comprising a powder of submicron to tens of micron size particles capable of forming a conductive network within a carrier matrix, such as a thin film matrix, and a process for preparing the composition.
Abstract: An improved process for preparing phenyl esters of alkanoyloxyacetic acids in which phenyl chloroacetate is reacted with the salt of a carboxylic acid.
Type:
Grant
Filed:
March 25, 1991
Date of Patent:
August 10, 1993
Assignee:
E. I. Du Pont de Nemours and Company
Inventors:
Bijan Amini, Donald J. Dumas, Ronald A. Fong, George C. Sonnichsen
Abstract: A process for using iron metal or an iron-containing sulfide reagent as a co-additive to extend the usefulness of sodium in refining crude lead bullion.
Type:
Grant
Filed:
February 13, 1992
Date of Patent:
June 29, 1993
Assignee:
E. I. Du Pont de Nemours and Company
Inventors:
Michael H. Blenk, Russell B. Diemer, Jr., John P. Hager
Abstract: A process is provided for separating high purity alkyl glycolate from a gaseous reaction mixture resulting from the catalyzed gas phase oxidation of alkyl glycolate. A hot solvent which is immiscible with water but selectively dissolves alkyl glycolate and alkyl glyoxylate is brought in contact with the gaseous reaction mixture, and water and alcohol vapors are removed from the hot solvent. The alkyl glyoxylate is removed from the solution by a first distillation and the alkyl glycolate and solvent are then separated in a second distillation.
Type:
Grant
Filed:
February 7, 1992
Date of Patent:
June 8, 1993
Assignee:
E. I. Du Pont de Nemours and Company
Inventors:
George E. Heinsohn, John F. Kook, John R. Kosak, Rudolf E. Svadlenak
Abstract: A process and apparatus for the production of hydrogen peroxide directly from hydrogen and oxygen utilizing a pipeline reactor for establishing a reaction zone for the reaction of these gases within an acidic aqueous solution, is disclosed. The reaction zone is completely filled with the solution and a reaction mixture is formed by dispersing hydrogen gas and oxygen gas in the solution in proportions above the lower flammability limit under control conditions resulting in the formation of hydrogen peroxide. This reaction mixture is maintained until the proportion of hydrogen has decreased to below the lower flammability limit for the gas mixture. The hydrogen peroxide is then removed from the reaction zone. The reaction of the hydrogen and oxygen in the solution is conducted under plug-flow conditions.
Abstract: An insensitive gel propellant composition based on a fine-particle detonating high explosive which contains from about 10 to 15 wt. % water, and which will not ignite until subjected to a temperature of about 900 psi.
Type:
Grant
Filed:
November 14, 1991
Date of Patent:
February 23, 1993
Assignee:
E. I. Du Pont de Nemours and Company
Inventors:
William C. Burkhardt, Michael W. Diehl, Wesley F. Spence
Abstract: In the catalyzed gas phase oxidative dehydrogenation of alkyl glycolate with an oxygen source in the presence of a metallic silver catalyst, the selectivity of from 500 to about 5000 ppm the reaction is increased at high conversion rates by the addition of methylene chloride to the reactants.
Abstract: An improved plastic-bonded explosive composition which includes from 2 wt. % up to 30 wt. % of a nitrocellulose binder and comprises incorporating into the composition during preparation from about 0.0025 wt. % up to a value less than 2 wt. % of fibrillatable polytetrafluoroethylene (PTFE) and mixing the composition thoroughly and with sufficient shearing action whereby the PTFE fibrillates and becomes substantially uniformly distributed throughout the finished composition.
Abstract: The use of anionic polysilicate microgels with an organic polymer to flocculate pulp and filler fines, such that water removal is easier and fines retention is greater and a new silicated cationic starch composition.
Abstract: Previously formed copper speiss in an amount of about 6.5% by weight is a co-additive which extends the usefulness of sodium in refining crude lead bullion, which has a sulfur content generally less than about 1.3% by weight.
Type:
Grant
Filed:
February 13, 1992
Date of Patent:
February 2, 1993
Assignee:
E. I. Du Pont de Nemours and Company
Inventors:
Michael H. Blenk, Russell B. Diemer, Jr., John P. Hager
Abstract: A process for using an iron-containing sulfide reagent and a previously formed copper speiss as joint co-additives to extend the usefulness of the sodium in refining crude bullion which has less than about 1.3 wt. % sulfur.
Type:
Grant
Filed:
February 13, 1992
Date of Patent:
February 2, 1993
Assignee:
E. I. Du Pont de Nemours and Company
Inventors:
Michael H. Blenk, Russell B. Diemer, Jr., John P. Hager
Abstract: An improved process for preparing alkanoyloxyacetyloxybenzenesulfonate salts in which phenyl esters of alkanoyloxyacetic acids (alkanoyloxyacetyloxybenzenes) are sulfonated to yield novel alkanoyloxyacetyloxybenzenesulfonic acids which, on neutralization, yield the corresponding alkanoyloxyacetyloxybenzenesulfonate salts.
Type:
Grant
Filed:
March 25, 1991
Date of Patent:
October 6, 1992
Assignee:
E. I. Du Pont de Nemours and Company
Inventors:
Bijan Amini, Donald J. Dumas, George C. Sonnichsen
Abstract: A continuous catalyzed vapor phase process for the production of dimeric cyclic esters which comprises converting the corresponding alpha-hydroxy-carboxylic acid or ester in the vapor phase over a solid catalyst, such as a silica-alumina, preferably a silica-alumina having a high silica content, in the presence of a carrier of gas.