Abstract: A composition is disclosed of about 0.45 to about 5.5 percent of an organic water-soluble binder which has a thermal decomposition temperature of about 100 to about 500.degree. C. and a viscosity of less than about 10,000 poises at 20.degree. C., about 1.5 to about 4.0 percent of a starch which has a thermal decomposition temperature of about 250 to about 535.degree. C. where the thermal decomposition temperature of the binder and the starch are at least about 50.degree. C. apart, about 1.5 to about 3.5 percent cellulose, about 0.5 to about 2.0 percent of a dispersant, and about 7 to about 11 percent water, and about 75 to about 89 percent of a high temperature refractory material such as stabilized zirconia. The composition is de-aired, formed into a shape, and fired to produce a ceramic structure.

Abstract: Disclosed is a solventless UV dryable B-stageable epoxy adhesive which comprises about 40 to about 70 pbw of a solid thermally curable epoxy having a molecular weight between about 650 and about 4000, a thermal curing agent for the thermally curable epoxy which is stable at room temperature and soluble on the adhesive in an amount of about stoichiometric to about 50% by weight in excess of stoichiometric, up to about 2 pbw of an accelerator for the thermal curing agent which is soluble in the adhesive, about 25 to about 60 pbw of a liquid UV curable resin having a molecular weight of less than about 700 which is either an epoxy, an acrylic, or a mixture thereof and which is a diluent for the thermally curable epoxy, about 1 to about 10 pbw of a UV photoinitiator for the UV curable resin, up to about 20 pbw of a reactive diluent, up to about 5 pbw of a flow control agent, up to about 1 pbw of a surfactant, and up to about 10 pbw of a tri or higher functional epoxy.

Abstract: A method is disclosed for separating uranium from molybdenum in an aqueous solution. The pH of the solution is lowered to about 1 to about 4 using an inorganic acid such as hydrochloric acid. The carbon dioxide is then removed from the solution which can be done by aeration. The pH of the solution is raised to about 9 in the presence of ammonium ions which result in the precipitation of ammonium diuranate. The precipitated ammonium diuranate may then be filtered or otherwise separated from the molybdenum which remains in the solution.

Abstract: Disclosed is a high solids single-package air-dryable primer containing about 15 to about 30% by weight air-dryable synthetic alkyd resin, about 10 to about 30% by weight organic solvents for the resin, at least about 0.4% by weight of a suspending agent, at least about 1 pbw of a polar additive for every pbw of the suspending agent, at least about 3% by weight of a coloring pigment, at least about 15% by weight of a corrosion inhibitor, at least about 0.3% by weight of a dryer, and about 30 to about 40% by weight of an extender pigment. The primer is prepared by mixing enough of the alkyd resin to wet the coloring pigment with enough of the solvent to optimize sheer. The suspending agent and polar additive are then added followed by the corrosion inhibitor and wetting agent. The coloring pigment is then added and the composition is ground to satisfactory particle size. Finally, the remaining ingredients are mixed in.

Abstract: A substrate is made for silicon solar cells by heating a sheet of large-grained silicon steel at a temperature of at least about 1300.degree. C. in an atmosphere of hydrogen and tungsten hexafluoride (or hexachloride) at a partial pressure ratio of hydrogen to tungsten hexafluoride of about 3 to about 6 to deposit an epitaxial layer of tungsten on said sheet of silicon steel. Epitaxial silicon can then be deposited in a conventional manner on the layer of epitaxial tungsten.

Abstract: A continuous process is disclosed for precipitating uranium from an aqueous solution formed by the hydrolysis of uranium hexafluoride gas. Undersized ammonium diuranate particles are formed in a first container by mixing the aqueous solution and an ammonium hydroxide solution containing about 10 to about 30% by weight ammonium. The ratio of the two solutions should be such that there are about 20 to about 30 moles of ammonium per mole of uranium. The temperature is maintained at about 30.degree. to about 50.degree. C. and the residence time in the first container is about 14 to about 57 seconds. The slurry is then transported to a second container for further particle growth where it is agitated at a temperature of about 20.degree. to 40.degree. C. for a residence time of about 2 to about 9 minutes. The resulting ammonium diuranate precipitate has a surface area of about 10 to about 20 meters squared per gram. The precipitate can then be calcined and pressed into pellets.

Abstract: Disclosed is a method of coating a substrate with .beta.-alumina, a compound of alumina and an alkali metal oxide, while maintaining its electrically conductive properties. A powdered mixture is formed of the .beta.-alumina and a carbonate of the alkali metal. The mixture is sprayed through a source of heat sufficient to melt it onto the substrate. A plasma spray torch can be used to melt spray the mixture.

Abstract: Disclosed is a method of making an .alpha.-hematite catalyst comprising condensing a ferric halide gas such as ferric chloride onto an inert metal oxide support such as alumina in the presence of moisture. The ferric chloride gas could be formed by reacting in iron source such as hematite with hydrogen chloride gas. The catalyst formed is less subject to erosion and is useful in the reduction of sulfur trioxide to sulfur dioxide.

Abstract: Disclosed is a method of removing uranium from a slurry containing a water-insoluble molybdate and a Group II element, usually calcium. The pH of the slurry is raised with an alkali metal hydroxide and maintained at a level sufficiently high to solubilize insoluble molybdenum compounds. This will generally require a pH of at least 10 which can be achieved by adding sodium hydroxide. Carbonate ion is then added to the slurry in an amount at least sufficient to precipitate the cation of the insoluble molybdenum compound. And finally, the solid portion of a slurry, which now contains calcium carbonate and sodium uranate, is separated from the liquid portion, which contains a soluble molybdenum compound.

Abstract: An emulsion is prepared which comprises about 8 to about 20 percent of a solvent, about 0.5 to 5 percent of an epoxy resin dissolved in the solvent to form a discontinuous phase, about 75 to about 90 percent of a precipitant as the continuous phase, and an emulsifier in an amount sufficient to react stoichiometrically with the epoxy and hydroxyl groups on the epoxy resin up to about 900% in excess of stoichiometric. A conductive workpiece is placed in the emulsion about 1/2 to about 2 inches from an electrode which is also immersed in the emulsion. A direct electric current potential is applied between the workpiece and the electrode with the workpiece as the anode. About 50 to about 400 volts and about 2 to about 50 milliamperes are used until a coating of the desired thickness has been deposited on the workpiece. The solvent and precipitant are preferably ketones such as cyclohexanone, and methylethylketone or isobutylketone, respectively.

Abstract: Disclosed is a method of altering the zirconium 91 isotopic content of zirconium by raising a zirconium chelate ligand from a ground state to an activated state in the presence of a scavenger which reacts with the activated state but not with the ground state, and permitting about 25 to about 75% of the zirconium chelate to react with the scavenger. The reaction may be performed in a solution of the zirconium chelate ligand using water as a solvent. Activation of the zirconium chelate may be accomplished by using light and having a wavelength of about 220 to about 350 nm or by heating to about 80 to about 100.degree. C.

Abstract: A method is disclosed for stabilizing glass which contains nuclear waste by coating the glass with synthetic monazite. The synthetic monazite has a composition of about 30 to about 35% Ce.sub.2 O.sub.3, about 31 to about 36% La.sub.2 O.sub.3, about 27 to about 35% P.sub.2 O.sub.5, and about 2 to about 5% Nd.sub.2 O.sub.3, where the percentage of La.sub.2 O.sub.3 is about 0.5 to about 1.5 percentage points greater than the percentage of Ce.sub.2 O.sub.3. The coating can be applied by detonation gun or by chemical vapor deposition. Chemical vapor deposition can be accomplished by heating halides of La, Ce, Nd, and P or PO and bringing the vapors by carrier gas to the glass where they are contacted by an oxidizing gas such as carbon dioxide, oxygen, steam, or air.

Abstract: Disclosed is a method of immobilizing nuclear waste in glass. A composition is prepared of 60 to 100% of a hydrolyzed glass-forming silicon compound and up to about 40% of a glass-forming aluminum compound. About 1 to about 50% liquid nuclear waste and up to about 10% solid nuclear waste is mixed into the composition. The composition is heated at about 200.degree. to about 500.degree. C. to drive off water and organics, with the resulting vitreous product totally containing the nuclear waste. Finally, this product can be sintered at about 800.degree. to about 900.degree. C. to reduce porosity, or warm pressed into block form.

Abstract: Disclosed is a method of immobilizing nuclear waste in glass. A composition is prepared of about 30 to about 85% of a hydrolyzed glass-forming silicon compound, about 5 to about 30% of a glass-forming sodium compound, up to about 30% of a glass-forming aluminum compound, and about 5 to about 30% of a glass-forming boron, calcium, or magnesium compound. Up to an equal amount of nuclear waste is mixed into the composition and the mixture is heated at up to 500.degree. C. until dry. The mixture is then melted at 800.degree. to 1300.degree. C., and can be poured into ingots and cooled. The mixture can also be melted in situ with a laser.

Abstract: Disclosed is a method of forming a deposit, such as silicon, by the reaction of a reactant, such as lithium, with a gas containing the element or compound to be deposited, such as silicon tetrachloride. One reactant diffuses through the growing scale on a heated inert substrate to react with the gas on the other side of the scale and lead to further scale growth.

Abstract: A solderable solventless UV curable enamel is disclosed which comprises a totally saturated compound having at least two rings each containing an epoxy group and a UV curative which generates a cation in the presence of UV light. The enamel contains no Lewis base but may contain up to 35% by weight based on total solids of a modifying resin which is co-reactive with the totally saturated compound and which does not char or prevent UV cure. The enamel is suitable for coating wires which must be soldered because the enamel melts away from the solder instead of charring.

Abstract: A clear solution is prepared by reacting metal alkoxide with a mixture of critical amounts of water and/or acid in an alcohol diluted medium. Alkoxides may be Ti(OR).sub.4 or Ta(OR).sub.5, or another metal alkoxide such as Si(OR).sub.4 in admixture with these alkoxides. Acids may be HCl or HNO.sub.3. Quarter wave inorganic optical coatings are deposited by applying the alkoxide solution to a substrate then heating the coating at over 350.degree. C. The coatings reduce reflectivity on silicon solar cells. The index of refraction of the coating can be varied by several techniques, including altering the proportion of titanium and silicon in the coating firing temperature, firing atmosphere. Thicknesses of the coating can be controlled by varying the rpm in spin application, withdrawal rate in dipping application, by concentration of the solution, by the type of solvent or the degree of polymerization of the titanium complexes.

Abstract: Disclosed is a solvent-free wire enamel cement coat which is curable to the B-stage with ultraviolet light. The wire can then be formed into a coil and cured with heat to the C-stage. The cement coat composition comprises a mixture of a UV photosensitizer and a curing agent with either an acrylated epoxy or an amine terminated acrylated epoxy or an acrylated urethane, or mixtures thereof, all dissolved in a monoacrylate. The composition can also include an end-blocked urethane, an acrylated hexamethoxymethyl melamine, or a low molecular weight cresol formaldehyde resin.

Abstract: Disclosed is an energy efficient electrolyzer for the production of hydrogen. The electrolyzer consists of an inner container, a plurality of electrolytic cells within the container and means for passing electric current in series through the electrolytic cells. Each cell consists of the anode half of one inert impervious conducting bipolar plate, in contact with an inert conductive anode bed of large surface area separated from the facing cathode half of another inert impervious conducting bipolar plate by a porous insulating separator. The anode is impregnated with an anolyte of about 10 to about 60% aqueous sulfuric acid saturated with sulfur dioxide and the cathode is bathed in a catholyte of about 10 to about 60% aqueous sulfuric acid. The anode is preferably carbon pellets which have been obtained from vegetable matter and which contain about 1 to about 5% platinum.

Abstract: A flexible mica tape having a low gel time is prepared from a composition of an epoxy resin, an organotin salt, and catechol or pyrogallol. A mica sheet is immersed in the composition and the solvent is evaporated to form a tack-free A-staged resin. A conductor is wound with the tape and is impregnated with an impregnating resin using vacuum-pressure impregnation.