Abstract: A process directed to acetic acid production comprising providing a feed stream comprising methyl iodide, water, acetic acid, methyl acetate, and at least one PRC to a distillation column comprising a distillation zone and a bottom sump zone and distilling the feed stream at a pressure and a temperature sufficient to produce an overhead stream comprising methyl iodide and at least one PRC, and a residuum stream flowing from the bottom sump zone comprising water and greater than or equal to about 0.11 weight percent HI is disclosed herein.
Type:
Grant
Filed:
October 2, 2015
Date of Patent:
September 17, 2019
Assignee:
CELANESE INTERNATIONAL COPORATION
Inventors:
Mark O Scates, Ronald David Shaver, Yaw-Haw Liu