Abstract: A method of synthesizing a 2-hydroxyphenyl-5-pyrimide ketone represented by the following chemical formula (I), including: weighing 0.048 g of a palladium complex, 0.8413 g of chromone-3-formaldehyde and 2.5719 g of ammonium formate into a 100 mL round bottom flask, then adding 50 mL of anhydrous methanol to dissolve, heating to reflux for 36 h, then stopping the reaction, performing column chromatography with petroleum ether and dichloromethane in a volume ratio of 1:1, and then naturally volatilizing the first component to obtain a light yellow crystal, namely the 2-hydroxyphenyl-5-pyrimidine ketone; wherein the chemical formula of the compound (I) is as follows: and an use of compound (I) as a catalyst in the reaction of benzophenone imine and trimethylsilyl nitrile showing a good catalytic performance, with a conversion rate of 69.1%.

Abstract: A dedicated device for shattering phenolics with mechanochemical synthesis and a shattering method thereof. The dedicated device includes a supporting frame, a primary shattering device, a secondary shattering device, a three-stage shattering device and an automatic regulating device. The primary shattering device includes a shattering box, a first motor, a first transmission rod, a plurality of tool frames, a plurality of blades, at least one screen mesh, a plurality of fixed cutters and a guide hopper. The secondary shattering device includes a first roller, a second roller, a second transmission rod and a set of helical gears. The three-stage shattering device includes a second motor, a set of tapered blade sets and a plurality of strain sensors. This realizes the regeneration of new mixed materials and the chemical properties of materials control of some micro changes such as material morphology.