Abstract: The instant invention relates to an apparatus for contacting solids in the form of flowable lumps with liquids and, optionally, gases, particularly for producing aluminum alcoholates by reacting aluminum with an excess of an aliphatic C3 to C10 alcohol, wherein solids charged to a reactor from the top are contacted in a spouted bed with liquid or a mixture of liquids and a rotary grate is provided for holding at least temporarily the aluminum lumps in the form of ingot off-cuts.
Abstract: There is provided a process for producing Guerbet alcohols not containing any heavy metals or soaps, wherein primary and/or secondary alcohols having 2 to 30 carbon atoms are condensed at elevated temperature in the presence of alkaline catalysts and/or heavy metal catalysts while eliminating the reaction water, and the reaction product is immediately separated by distillation without any additional purification.
Type:
Grant
Filed:
February 11, 2000
Date of Patent:
July 16, 2002
Assignee:
Sasöl Germany GmbH
Inventors:
Erich Scherf, Hans-Jürgen Letsch, Clemens Schröder, Albert Thomas Herrmann