Abstract: A method and apparatus for determining the total amount of organic carbon in a sample comprising the successive steps of: (a) heating the sample in an inert atmosphere to a first temperature capable of cracking at least a fraction of the organic material contained in the sample; (b) measuring the amount of organic carbon contained in at least a fraction of the effluent resulting from this cracking; (c) heating the sample in an oxidizing atmosphere to a second temperature at most equal to the first temperature; (d) measuring the amount of organic carbon in the effluent produced by the oxidation of the organic material, and (e) deriving from the above measurements the total organic carbon content of the sample. In order to perform the method of the invention, there is also provided means for performing each of the successive steps. In a further refinement, the method also includes steps for determining the mineral carbon content so that the total carbon content of the sample can be determined.
Type:
Grant
Filed:
July 26, 1982
Date of Patent:
May 28, 1985
Assignees:
Institut Francais du Petrole, Societe Labofina S.A.
Inventors:
Jean Espitalie, Marcel Madec, Paul Leplat, Jacques Paulet
Abstract: The method of the invention comprises the successive steps of: (a) heating the sample in an inert atmosphere to a first temperature capable of cracking at least a fraction of the organic material contained in the sample; (b) measuring the amount of organic carbon contained in at least a fraction of the effluent resulting from this cracking; (c) heating the sample in an oxidizing atmosphere to a second temperature at most equal to the first temperature; (d) measuring the amount of organic carbon in the effluent produced by the oxidation of the organic material, and (e) deriving from the above measurements the total organic carbon content of the sample. In order to perform the method of the invention, there is also provided means for performing each of the successive steps. In a further refinement, the method also includes steps for determining the mineral carbon content so that the total carbon content of the sample can be determined.
Type:
Grant
Filed:
December 24, 1980
Date of Patent:
October 5, 1982
Assignees:
Institut Francais du Petrole, Societe Labofina S.A.
Inventors:
Jean Espitalie, Marcel Madec, Paul Leplat, Jacques Paulet