Abstract: A crosslinkable acrylic copolymer sealant composition has a stabilized viscosity in that the viscosity does not unduly increase nor does the material gel on storage for periods of time up to and including one year. The stabilized viscosity is unexpectedly achieved by adding moisture scavengers either before and/or during the polymerization of the various monomers. The sealant composition is suitable for use in high movement applications as well as to metal and glass substrates.

Abstract: An expansion joint sytem (10) spans a slot (12) of adjacent concrete slabs (14, 16). The system includes a boxed out area (22) adjacent the slot. A plate member (32) extends across the slot. A preformed resilient pad (42) is positioned above the plate member. Nosings (64) of resilient material are bonded to the pad and to the surfaces bounding the boxed out area. The pad has a cross sectional configuration that achieves enhanced bonding to the nosings, greater flexibility and resistance to failure in cold weather, and greater elongation without failure.

Abstract: The present invention relates to a one-part, self-leveling urethane sealant composition for substantially horizontal surfaces, wherein the sealant will flow within a crack, joint or the like and quickly cure to provide an elastomeric seal having a smooth, substantially horizontal surface. The cured sealant provides a surface and volume cure time superior to many known systems, and once cured, provides an elastomeric seal having a superior void volume and void distribution than many known self-leveling sealant systems.

Abstract: An FT-IR spectrometer (10) operated for analysis by reflectance spectroscopy, has a window (56) having a body (58) which generally transmits radiation in the visible range there through. The window has a surface (60) for supporting a sample (72) of material to be analyzed. The surface of the window has a coating (62) that generally transmits visible radiation while generally reflecting radiation across the infrared range. The window provides for fast and reliable set up of sample and background scans through use of a visual microscope portion of the spectrometer. The window also has a long life, is durable and is low in cost.

Abstract: A caulking gun with the open supporting framework that has a forwardly disposed ring member and a rearwardly disposed trigger actuating mechanism that is cooperative with a rod member with teeth thereon to advance the piston on the one end of the rod member which in turn operates on a moveable member in a disposable cartridge that is received by the supporting framework. A nozzle is removably connectable with the cartridge and is also removably connectable with the ring member of the gun to provide selective detachment.

Abstract: A non-sag agent useful in providing non-sag properties to many conventional curable, polymeric adhesives and sealants, said agent comprising:a first component comprising crush resistant coated particles wherein the first component particles are less than about 1 and 1/2 microns in size and have a coating of about 0.1% to about 10% by weight of the particle and wherein said coating substantially comprises a first surface modifying agent,a second component comprising crush resistant coated particles wherein the second component particles are about 1 and 1/2 to about 3 microns in size and have a coating of about 0.

Abstract: The present invention relates generally to the re-utilization of silicone scrap material. More specifically, the process of the present invention is directed to dissolving silicone scrap in an appropriate solvent and chemically converting the scrap into dimethyl silicone cyclic trimer, tetramer, pentamer and/or the like by means of a two step acid/base catalyzed cracking process.

Abstract: The present invention relates generally to multi-paned window systems and to the manufacture of such systems. More specifically, the present invention is directed to an improved window system having an innovative seal comprising crush resistant beads or the like wherein the seal can be compressed only to a substantially uniform and substantially predefined thickness and wherein the seal provides exceptional insulation, weather resistance and adhesion characteristics.

Abstract: The present invention relates to a compatibalizing agent useful in compatibalizing a substantially non-polar compound, such as asphalt, with a substantially polar organic compound, such as an isocyanate prepolymer. The compatibalizing agent consisting of a polymer unit, or of two such units being either identical or different linked together by an ester, carbon or ether bond, said unit having the following formula:CH.sub.3 --(C.sub.n H.sub.2n)--R.sub.1wherein:n is 4 or more, andR.sub.1 is COOH, COO.sup.- M.sup.+, COOR.sub.2 or R.sub.2,wherein:M is a metal, andR.sub.2 is a substantially saturated organic chain having a backbone substantially comprising carbon-carbon, carbon-oxygen, or carbon-nitrogen linkages, or combinations thereof, wherein the backbone's pendent constituents are either --H or --OH and wherein at least one pendent constitutent is --OH.

Abstract: A method and apparatus for treating the surface of an insulating strip for use in the manufacture of multi-pane windows. The apparatus and methods of one embodiment of the invention includes a texturing roller which leaves a textured impression in a surface of the insulating strip, thereby improving the desiccating and altering the sheen and otherwise affecting the appearance of the insulating strip. According to an alternative embodiment of the invention, method and apparatus are provided for laminating a moisture vapor permeable layer onto a surface of the insulating strip. The apparatus of the invention also includes forming rollers for restoring the profile of the insulating strip.

Abstract: A protective cap for fastener heads includes a preformed member formed of a naturally tacky compound of unvulcanized butyl rubber, a reinforcing layer of a non-woven polyester fabric, and a silicone-coated polyethylene release liner. The preformed member has a dome-shaped central portion and a surrounding generally flat annular flange. The reinforcing layer of the polyester fabric is disposed over a top surface of the preformed member to form a homogeneous cap construction, and the release liner covers the tacky bottom surface of the preformed member to prevent the cap from adhering to surfaces until ready for use. A plurality of the protective caps are formed in a manipulatable sheet unit and are maintained thereon by the natural tackiness of the unvulcanized butyl rubber compound.

Abstract: A concrete and masonry waterproofing composition comprises a major amount of a polyurethane and a minor amount of a penetrant. The polyurethane is desirably made from a polyether polyol or a polyester polyol intermediate, wherein the polyol is a diol or a triol. Such intermediates are reacted with a polyisocyanate. Cure, that is, chain extension occurs upon contact with moisture in the air. The penetrant is an organosilane having the formula: ##STR1## where R.sup.1 is an aliphatic having from 1 to 18 carbon atoms and wherein R.sup.2, R.sup.3, and R.sup.4, independently, is an alkyl having from 1 to 6 carbon atoms, or an organosiloxane having the formula: ##STR2## wherein R.sup.7 is an aliphatic having from 1 to 18 carbon atoms and R.sup.5 and R.sup.6, independently, is an alkyl having from 1 to 6 carbon atoms, and wherein n is 2 to 20.

Abstract: A high performance urethane sealant or coating composition is made from a physical blend of a polypropyleneoxide polyol intermediate and a high molecular weight polybutyleneoxide polyol intermediate or copolymers thereof wherein the comonomer is preferably ethyleneoxide. The urethane prepolymer is made by reacting the physical intermediate blend with a polyisocyanate and preferably blocking the same with blocking agents such as phenols to prevent reaction with moisture in the air. Alternatively, the prepolymer can be end capped with an epoxy. Cure is effected through the utilization of curing agents such as polyamines or polyimines, e.g., diamines, amine terminated polyethers, ketimines, aldimines, and the like. The sealant composition can contain various fillers, organosilanes, and the like. The prepolymers as well as the sealants of the present invention have improved physical rubbery type properties such as higher elongation, lower modulus, and generally improved tensile strength.

Abstract: The invention relates to an improved adsorbent, essentially impermeable to oxygen and nitrogen but permeable to water vapor, and to sealants incorporating said adsorbent. The adsorbent comprises outgassed zeolite having pores with apertures large enough to permit entry of gases such as oxygen and nitrogen into the pore spaces and having on its surface, covering the pore apertures, a fluid which is essentially impermeable to nitrogen and oxygen molecules and yet permeable to water vapor. The zeolite adsorbent, and sealants prepared from the zeolite, are particularly useful in the fabrication of thermal insulating glazed windows having a sealed air pocket.

Abstract: The invention relates to an improved adsorbent, essentially impermeable to oxygen and nitrogen but permeable to water vapor, and to sealants incorporating said adsorbent. The adsorbent comprises outgassed zeolite having pores with apertures large enough to permit entry of gases such as oxygen and nitrogen into the pore spaces and having on its surface, covering the pore apertures, a fluid which is essentially impermeable to nitrogen and oxygen molecules and yet permeable to water vapor. The zeolite adsorbent, and sealants prepared from the zeolite, are particularly useful in the fabrication of thermal insulating glazed windows having a sealed air pocket.

Abstract: A dimensionally stable sealant and spacer strip comprising an elongated ribbon of deformable sealant enveloping and having embedded therein spacer means extending longitudinally of the ribbon of sealant. The thickness of the enveloping sealant extends beyond the spacer means in an amount sufficient to maintain a continuous sealing interface under applied compressive forces but insufficient to permit substantial distortion of the strip under such applied compressive forces.

Abstract: The method of making a deformable sealant strip having a continuous strip of rigid corrugated material embedded longitudinally within mastic material wherein a continuous linear-rigid spacer is first corrugated and then fed in this condition into an extruder cross head wherein such rigid corrugated spacer is encompassed by a mastic. The strip is coiled for subsequent use in retrofitting double pane windows as well as making dual insulated windows. The extruder that receives the rigid corrugated spacer in its crosshead provides a mastic that surrounds and encompasses the spacer without deforming it.

Abstract: A waterproofing sheet material useful for example as a free floating membrane or flashing material in roofing applications, a pond liner, or a gasketing material, composed of from about 15 wt. % to about 80 wt. % of an ingredient selected from the group consisting of:(a) homopolymers of alkadienes and substituted alkadienes(b) addition copolymers of alkadienes with unsaturated monomers(c) homopolymers of alkenes and substituted alkenes selected from the group consisting of polyethylene, chlorosulfonated polyethylene and polyisobutylene(d) resin acids and resin acid derivatives(e) highly aromatic bituminous materials, and(f) pine oiland from about 85 wt. % to about 20 wt. % of a plasticized polyvinyl butyral resin. Minor amounts of fatty acids and paraffin wax may be added to improve low temperature properties and to facilitate processing a hot melt admixture of the ingredients into a sheet.

Abstract: A waterproofing sheet material useful for example as a free floating membrane or flashing material in roofing applications, a pond liner, or a gasketing material, composed of from about 15 wt. % to about 80 wt. % of an ingredient selected from the group consisting of:(a) homopolymers of alkaldienes and substituted alkadienes(b) addition copolymers of alkadienes with unsaturated monomers(c) homopolymers of alkenes and substituted alkenes selected from the group consisting of polyethylene, chlorosulfonated polyethylene and polyisobutylene(d) resin acids and resin acid derivatives(e) highly aromatic bituminous materials, and(f) pine oiland from about 85 wt. % to about 20 wt. % of a plasticized polyvinyl butyral resin. Minor amounts of fatty acids and paraffin wax may be added to improve low temperature properties and to facilitate processing a hot melt admixture of the ingredients into a sheet.

Abstract: A waterproofing sheet material useful for example as a free floating membrane or flashing material in roofing applications, a pond liner, or a gasketing material, composed of from about 15 wt. % to about 80 wt. % of an ingredient selected from the group consisting of:(a) homopolymers of alkadienes and substituted alkadienes(b) addition copolymers of alkadienes with unsaturated monomers(c) homopolymers of alkenes and substituted alkenes selected from the group consisting of polyethylene, chlorosulfonated polyethylene and polyisobutylene(d) resin acids and resin acid derivatives(e) highly aromatic bituminous materials, and(f) pine oiland from about 85 wt. % to about 20 wt. % of a plasticized polyvinyl butyral resin. Minor amounts of fatty acids and paraffin wax may be added to improve low temperature properties and to facilitate processing a hot melt admixture of the ingredients into a sheet.