Abstract: The invention relates to a method for filling a horizontal flue coking oven. According to the invention, spinning cells are introduced into the furnace chamber for filling, which comprise a discharge element rotating about a vertical axis. The bulk material is charged onto the spinning cells and the bulk material distributed in the furnace chamber as a result of the rotation of the discharge element. The surface of the bulk material is subjected to a subsequent raking process.

Abstract: Modular device and method for carrying out experiments in parallel on process substances to develop technical methods, comprising at least a multiplicity of individual reactors which are controllable independently of one another said reactors being comprised of pressure-tight chambers having separable sample vessels, and optionally, stirring devices, heating instruments, cooling instruments, or both, a monitoring unit for monitoring or controlling at least the pressure and the temperature in the individual reactors, pressure-tight lids having independent feed lines and optionally independent discharge lines for individual process substances; a plurality of the lids being simultaneously sealable upon the rectors by a common sealing means (11).

Abstract: A coke oven has a coke-oven chamber adapted to hold a mass of coke, defining above the mass of coke a gas-collecting chamber, and having a door opening. A door closes the door opening. A peripheral gas channel extends around the opening between the door and coke-oven chamber and has at least one outer and at least one inner door seal defining an annular space. The inner door seal is formed in both the coke-oven chamber and the gas-collecting chamber with a plurality of throughgoing holes forming fluid-communicating connections between the coke-oven chamber, the gas-collecting chamber, and the annular space at different heights of the coke-oven chamber and of the gas-collecting chamber. Thus regions of the coke-oven chamber with different gas pressures communicate with each other and with the annular space via the connections on the inner door seal to equalize pressure between the regions and the gas-collecting chamber.

Abstract: A table or counter mat having a composite sheet structure comprising a non-slip backing layer 3, a top liquid absorbent textile surface 1 for resting cups, mugs or glasses, and an intermediate stabilisation layer 2 joining the backing layer 3 to the textile surface 1 wherein the resultant mat is absorbent and readily able to be laundered. The invention also provides a method of forming the table or counter mat by curing and bonding of the nitrile rubber backing layer 3 to the intermediate layer 2 and upper polyester textile layer 1 at greater than 100° C. and preferably greater than 170° C. and a sublimation printing 4 for printing on the textile layer 1 occurs at greater that 100° C. and preferably greater than 170° C. such that the mat is able to be laundered in hot water.

Abstract: The compact chemical reactor with a central axis includes at least two unit reactors disposed adjacent to each other to form front and back sides of the compact chemical reactor; a front and back reactant plenum communicating with the front and back side respectively; at least one of the plenums comprises a reactant; and unit reactors comprising: a front cavity between front and back process layers; a back cavity between back and front process layers of adjacent unit reactors; the process layers facilitate transport processes between reactant plenums; each cavity communicates with one side of the compact chemical reactor; a front and back perimeter barrier on the back and front process layers respectfully, substantially surrounding respective cavities. At least one of the unit reactors comprise at least one frame formed from one of the process layers, at least one of the perimeter barriers, and at least one of the cavities.

Abstract: A distillation system is provided for batch thermolytic distillation of lump carbonaceous material, such as lump wood and shredded rubber tires. The system preferably includes multiple distillation units mounted side-by-side. Each unit includes a reactor bath for holding molten tin at approximately 455° C., a two-compartment reservoir for storing molten tin, and a porous basket pivotally mounted within the reactor bath for tipping motion. A process for batch thermolytic distillation of lump carbonaceous material includes rotating the porous basket into a reactor bath by rotating the basket about an axis passing through the reactor bath; putting a charge of wood into the basket; closing a retractable lid onto the reactor bath; filling the reactor bath with molten material to produce gas and char by thermolytic conversion of the charge, draining the reactor bath of molten material while the lid is closed; quenching the char in the reactor bath with steam; opening the lid; and tipping the char from the basket.

Abstract: The present invention relates to an X-ray absorbing material that can be used in medicine as well as in the manufacture of special protective clothing, protective screens, housings, protective coatings and isolation materials. In a first embodiment, the material uses as a filler a poly-dispersed mixture, segregated by kneading and containing metallic particles having a size between 10?9 and 10?3 m, wherein the particles are bonded to the surface of a textile base. The density of the material is defined by the relation qN=(0.01–0.020) qP, where qN is filler. In a second embodiment, the invention uses as a filler the above mixture, although here the particles are surrounded by the volume of a matrix made of a compound that solidifies under atmospheric pressure. The total mass of the poly-dispersed and segregated mixture is defined by the relation M=(0.05–0.

Abstract: The compact chemical reactor includes one or more unit reactors, a front reactant plenum, and a back reactant plenum. Each unit reactor is made of a front and back process layer, a front and back cavity, and a front and back perimeter barrier. The resulting assemblage is configured so the front cavity is in communication with the front side of the compact chemical reactor and the back cavity is in communication with the back side of the compact chemical reactor. The process layers facilitate an exchange of reactants between the reactant plenums.

Abstract: Urea is prepared by reacting ammonia and carbon dioxide in an apparatus comprising a vertical condensation and synthesis column and a stripper, to provide a urea synthesis solution comprising urea, unreacted ammonia, unreacted carbon dioxide and water. The urea synthesis solution is transferred from the top of the vertical condensation and synthesis column to the top of a stripper. Carbon dioxide is introduced into the bottom of the stripper and contacted with the urea synthesis solution, thereby separating the unreacted ammonia and the unreacted carbon dioxide from the urea, and providing a mixed gas comprising ammonia, carbon dioxide and water. The mixed gas is transferred into the bottom of the vertical condensation and synthesis column, where it is reacted with liquid ammonia injected into the bottom and a middle of the vertical condensation and synthesis column. The mixed gas and liquid ammonia are condensed and react to form urea.

Abstract: A method and system for extracting hydrocarbon fuel products from plastic material provides extraction of usable fuel components from waste plastic materials. The materials (or hydrocarbon portion thereof) are liquified and introduced to a chamber where the liquid material is agitated and a negative relative pressure (vacuum) is applied. The liquid is maintained at a substantially constant temperature and the vacuum draws the off-gas hydrocarbon products out for condensation and further processing, while unconverted char is removed to an ash dump. An auger feed unit with agitator buckets is used to propel the char through a feed while agitating the liquid to enhance the rate of gas removal.

Abstract: An apparatus for parallel processing of reaction mixtures, including a reactor block including reaction chambers for containing reaction mixtures under pressure, the reactor block further including a first sidewall, a second sidewall, and a first plurality of fluid flow paths providing fluid communication with the first sidewall and respective reaction chambers and the second sidewall and respective reaction chambers; a stirring system including a base plate defining a second plurality of flow paths, wherein respective flow paths of said second plurality of flow paths are in fluid communication with respective reaction chambers and respective fluid flow paths of said first plurality of flow paths, and the base plate also supports a plurality of stirring blade assemblies for mixing the reaction mixtures; interchangeable manifolds supported by the first sidewall and the second sidewall, the interchangeable manifolds defining a plurality of manifold inlet/outlet ports, wherein respective inlet/outlet ports of sa

Abstract: New composite materials having a high density of small particles, such as hollow microspheres, in a matrix material are disclosed. The microspheres are densely packed in the matrix material such that adjacent microspheres are positioned in contact with each other or very close together. Fiber flanking may be provided on the opposite sides of a layer of a core of composite material having the small particles and matrix material. Also disclosed are methods of making and using the composite materials.

Abstract: An improved process and apparatus for the destructive distillation or pyrolysis of rubber, such as used rubber tires, to produce liquid and gaseous hydrocarbons and a solid carbonaceous char. A heat transfer gas circulating in a circulation loop is used to cool the hot char produced in the distillation chamber of a distillation oven, the circulation loop having some means for removing the heat transferred to the heat transfer gas from the hot char. In one embodiment, two distillation ovens are operated in off-set, batchwise distillation cycles. The distillation cycles in the two ovens are coordinated so that a fresh charge of rubber feed is introduced into the distillation chamber of one of the ovens as the distillation of rubber in the other oven is concluded.

Abstract: A safe, efficient and repetitively operable coke vessel decoking system is disclosed. In a preferred embodiment the closed system comprises a coker vessel pressure-tightly sealed to a top head system, which includes a closure housing with a laterally moveable horizontal closure member therein and a cutting head enclosure, which further comprises a drill stem guide, an access door, and a cutting assembly mounted therein. A novel feature of the invention is a steam purge/blocking system whereby steam pressure is maintained in the closure housing during the coking cycle to maintain seal integrity. Personnel safety during decoking operations is greatly enhanced by eliminating dangerous manual tasks associated with the prior art such as unbolting and removing top head devices. The system can be remotely and repetitively operated through numerous coking/decoking cycles without removal of any system element.

Abstract: A method and a device for the hot-repairing of the heating flues of a coke-oven battery according to which the completed sections of a heating flue still under construction are heated by means of a heated gas. The heated gas comprises the air usually provided for combustion in the heating flues during coking operations. The air is guided through the flow paths provided for in the coke-oven battery for combustion air and waste gases as well as through the regenerator, heated as it passes through the flow paths and then guided through the heating flues to be repaired. The completed section of the heating flue is separated from the non-completed portion by an air-reversion device that also directs the heated air.

Abstract: A coke drum bottom de-heading system having an internal shroud enclosure and a shroud end cap opened by a flange to a coke bottom de-heading valve capable of accepting the end of a gate valve upon actuation. Acting in coordination with the shroud enclosure to prevent the escape of steam is a gate seal assembly having a gate seal slidably engaged against the sliding gate to prevent the passage of steam thereby.

Abstract: A conventional method of pyrolytically decomposing plastic to make low-molecular compounds is poor in efficiency of use of energy due to high heating temperatures (at least 600° C. and 800° C. at maximum). The invention provides that a functional powder is heated to a predetermined temperature and pieces of plastic to be disposed are caused to be contacted with the heated powder, the functional powder including a powder which does in an aqueous solution state show alkalinity, and a photo-catalyst effect powder.

Abstract: A reactor system for reacting a hydrocarbon or hydrocarbon derivative charging material comprises a catalyst-coated reaction chamber, to which a reaction educt stream can be fed through a reaction chamber inlet, and electric heating means. The reaction chamber inlet has a flat, electrically heatable, catalyst-coated, and reaction educt stream-permeable heater, which covers at least partially the inlet cross section of the reaction chamber inlet and through which the educts for reacting the charging material can be fed at least in a start operating phase of the reactor system. An electric heater may be provided in front of the reaction chamber inlet, for the purpose of heating at least one reaction educt in a start operating phase and there are means for point-by-point injection of at least one reaction educt, heated in the heater, into the reaction chamber.

Abstract: An injection and solidification operation as well as a kneading and solidification operation can be performed by a single facility. A decreased amount of radioactive secondary waste is generated. A solidifying agent paste is prepared by kneading a solidifying agent and additive water. The solidifying agent paste is injected into a solidifying container. The radioactive waste is charged into the solidifying container and kneaded.

Abstract: A vapor-phase tubular reactor in a shell heat exchanger for removal of the heat of reaction at essentially isothermal conditions has porous wicking surface applied to the external surface of reactor tubes. The porous wicking surface on the reactor tubes draws liquid heat transfer fluid from a reservoir at the bottom of the wicked tube section and provides enhanced evaporative cooling. The invention is particularly useful for highly exothermic reactions or when reaction selectivity is negatively affected by high temperature excursions.