Patents Examined by John F Pettitt
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Patent number: 11965693Abstract: Disclosed are a helium gas liquefier and a method for liquefying a helium gas. The disclosed helium gas liquefier includes: a first cooling part including a first cooling column; a first cold head installed on the first cooling column, and a first cylinder in which the first cooling column and the first cold head are built; a second cooling part including a second cooling column, a second cold head installed on the second cooling column, and a second cylinder in which the second cooling column and the second cold head are built; and a liquid helium storage disposed under the second cooling part.Type: GrantFiled: December 18, 2020Date of Patent: April 23, 2024Assignee: KOREA BASIC SCIENCE INSTITUTEInventors: Yeon Suk Choi, Myung Su Kim
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Patent number: 11965694Abstract: In a process of the separation of a mixture of carbon monoxide, hydrogen and methane, the mixture is sent to a scrubbing column, a bottom liquid withdrawn at the bottom of the scrubbing column is depleted in hydrogen with respect to the mixture and is sent to a stripping column, a bottom liquid from the stripping column is sent to a separation column and a liquid enriched in methane withdrawn from the bottom of the separation column is vaporized in order to form a final product.Type: GrantFiled: July 24, 2019Date of Patent: April 23, 2024Assignee: L'Air Liquide, Societe Anonyme Pour L'Etude Et L'Exploitation Des Procedes Georges ClaudeInventors: Manon Cortale, Bertrand Demolliens, Antoine Hernandez, Guillaume Teixeira
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Patent number: 11933539Abstract: A system and method for improving the performance of an oxygen, nitrogen, and argon producing air separation unit configured to produce a gaseous nitrogen product stream is provided. By recycling the argon condenser boil-off vapor stream to the main air compression train, the argon recovery and oxygen recovery while maintaining the production level of a medium or high pressure gaseous nitrogen product stream. In addition, some operational cost savings in terms of lower power costs can also be realized compared to some prior art oxygen, nitrogen, and argon producing air separation units.Type: GrantFiled: August 11, 2021Date of Patent: March 19, 2024Assignee: Praxair Technology, Inc.Inventors: Zhengrong Xu, Neil M. Prosser
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Patent number: 11933541Abstract: A system and method for producing two or more nitrogen product streams and a crude argon stream from a nitrogen and argon producing air separation unit is provided. The disclosed embodiments of the cryogenic-based nitrogen and argon producing air separation units and associated air separation cycles include the means for directing a first portion of a boil-off stream from an argon condenser of the air separation unit to a waste expansion refrigeration circuit and concurrently recycling a second portion of the boil-off stream from the argon condenser to the main air compression system of the air separation unit to be mixed or blended with the incoming feed air. Optionally, a third portion of the boil-off stream from the argon condenser may be further compressed in a cold compressor and returned to the lower pressure column.Type: GrantFiled: August 11, 2021Date of Patent: March 19, 2024Assignee: Praxair Technology, Inc.Inventor: Zhengrong Xu
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Patent number: 11874055Abstract: An embodiment of a method for supplying refrigerants to a liquefied natural gas (LNG) facility includes: advancing a first refrigerant from a first storage device to a heat exchanger, the first refrigerant having a first temperature; advancing a second refrigerant from a second storage device to the heat exchanger, the second refrigerant having a second temperature different than the first temperature; flowing the first refrigerant and the second refrigerant through the heat exchanger; adjusting the second temperature based on at least a transfer of heat between the first refrigerant and the second refrigerant in the heat exchanger; and transferring the first refrigerant and the second refrigerant to the LNG facility.Type: GrantFiled: February 18, 2015Date of Patent: January 16, 2024Assignee: CONOCOPHILLIPS COMPANYInventors: Paul R. Davies, James L Harris
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Patent number: 11815308Abstract: A method and apparatus for producing liquefied natural gas. A portion of a natural gas stream is cooled in a first heat exchanger and re-combined with the natural gas stream, and heavy hydrocarbons are removed therefrom to generate a separated natural gas stream and a separator bottom stream. Liquids are separated from the separator bottom stream to form an overhead stream, which is cooled and separated to form a recycle gas stream. The recycle gas stream is compressed. A first portion of the compressed recycle gas stream is directed through the first heat exchanger and directed to the separator as a column reflux stream. The separated to natural gas stream is used as a coolant in the first heat exchanger to thereby generate a pretreated natural gas stream, which is compressed and liquefied.Type: GrantFiled: April 17, 2020Date of Patent: November 14, 2023Assignee: ExxonMobil Technology and Engineering CompanyInventors: Yijun Liu, Fritz Pierre, Jr.
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Raw material gas liquefying device and method of controlling this raw material gas liquefying device
Patent number: 11808502Abstract: A raw material gas liquefying device includes a feed line which feeds a raw material gas, a refrigerant circulation line which circulates a refrigerant, the refrigerant circulation line including an expansion unit of a turbine type which expands the refrigerant to generate cryogenic energy, and an expansion unit entrance valve provided at an entrance side of the expansion unit, a heat exchanger which exchanges heat between the raw material gas and the refrigerant, a cooler which performs initial cooling of the raw material gas and the refrigerant by heat exchange with liquid nitrogen, and a controller which manipulates the opening rate of the expansion unit entrance value and performs a feedback control so that the rotation speed of the expansion unit reaches a predetermined target value, and outputs the opening rate command to the expansion unit entrance valve, at start-up and stop of the expansion unit.Type: GrantFiled: December 4, 2017Date of Patent: November 7, 2023Assignee: KAWASAKI JUKOGYO KABUSHIKI KAISHAInventors: Naotaka Yamazoe, Tomohiro Sakamoto, Hidetaka Miyazaki, Daisuke Kariya, Yasuo Miwa, Yuichi Saito, Yosuke Kimura -
Patent number: 11808518Abstract: A natural gas liquefaction system and method for effectively and efficiently removing heavy hydrocarbons and converting natural gas into liquefied natural gas. Natural gas streams entering the system may consist of varied gas compositions, pressures, and temperatures. In embodiments the system may comprise a natural gas (NG)-to-liquefied natural gas (LNG) portion and a closed-loop refrigeration portion comprising a closed-loop single mixed refrigerant system. In other embodiments the system may comprise an NG-to-LNG portion and a closed-loop refrigeration portion comprising a closed-loop gaseous nitrogen expansion refrigeration system. All embodiments utilize an integrated heat exchanger with cold-end and warm-end sections and integrated multi-stage compressor and expander configurations (e.g. compander) in order to increase overall operation flexibility and efficiency.Type: GrantFiled: May 21, 2020Date of Patent: November 7, 2023Assignee: EnFlex, Inc.Inventors: James Zhao, Shukui Zhao
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Patent number: 11774173Abstract: A technology liquefies natural gas. The natural gas liquefaction method pre-cools treated natural gas by ethane evaporation, sub-cools liquefied gas using cooled nitrogen as a refrigerant, reduces liquefied gas pressure, separates non-liquefied gas and diverts liquefied natural gas. Before pre-cooling the natural gas is compressed, ethane is evaporated during the multi-stage pre-cooling of liquefied gas with simultaneous evaporation of ethane using cooled ethane as a refrigerant. Ethane generated by evaporation is compressed, condensed and used as a refrigerant during the cooling of liquefied gas and nitrogen, with nitrogen being compressed, cooled, expanded and fed to the natural gas sub-cooling stage. The natural gas liquefaction unit contains a natural gas liquefaction circuit, an ethane circuit and a nitrogen circuit. The natural gas liquefaction circuit includes a natural gas compressor, a cooler unit, ethane vaporizers, a closed-end subcooling heat exchanger, and a separator, connected in series.Type: GrantFiled: September 8, 2022Date of Patent: October 3, 2023Assignee: Publichnoe Aktsionernoe Obshchestvo “NOVATEK”Inventors: Rafail Minigulovich Minigulov, Sergei Vladimirovich Rudenko, Oleg Evgenievich Vasin, Dmitriy Nikolaevich Gritsishin, Evgeniy Igorevich Sobolev
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Patent number: 11719387Abstract: A method for conditioning a liquid cryogen in a tank includes reducing a pressure of the liquid cryogen in the tank for reducing a temperature of the liquid cryogen and condensing any vapor boil-off in the tank for reclaiming the liquid cryogen in the tank. The liquid cryogen may be selected from the group consisting of liquid nitrogen (LIN), liquid oxygen (LOX), and liquid argon (LAR).Type: GrantFiled: December 5, 2018Date of Patent: August 8, 2023Assignee: Messer Industries USA, Inc.Inventors: Simon J. Shamoun, Isaiah Edmonds
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Patent number: 11713920Abstract: A process for cryogenic separation of a feed stream containing methane and air gases in which: the feed stream is cooled in order to produce a cooled stream, at least one portion of the cooled stream is sent to one level of a distillation column, a bottom stream is drawn off from the distillation column, the bottom stream being enriched in methane relative to the feed stream, a stream enriched in oxygen and in nitrogen relative to the feed stream is drawn off from the distillation column, at least one noncombustible dilution stream that is more volatile than oxygen is introduced into the distillation column at at least one level lower than the one at which the cooled stream is introduced. The dilution stream is extracted from the feed stream. Facility for producing biomethane by purification of biogases derived from non-hazardous waste storage facilities (NHWSF) implementing the process.Type: GrantFiled: March 20, 2017Date of Patent: August 1, 2023Assignee: WAGA ENERGYInventors: Guénaël Prince, Nicolas Paget, Jean-Yves Lehman
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Patent number: 11698225Abstract: A method is provided for determining a state of a distillation column having multiple column stages for separating a feed fluid stream into individual fluid components. The state is determined by means of a model in a manner dependent on pressure differences prevailing between adjacent column stages. In the model, both gaseous and liquid flows between adjacent column stages are brought about by the pressure differences prevailing between adjacent column stages. A substance quantity flow characterizing gaseous flow between two column stages is given by {dot over (N)}V·RV=CV·?pV. A substance quantity flow characterizing liquid flow between two column stages is given by {dot over (N)}L·RL=CL·?pL. ?pV,L is a total pressure difference between two adjacent column stages. RV,L is a coefficient of resistance between two adjacent column stages and CV,L is a conductance value of flow between two adjacent column stages.Type: GrantFiled: October 17, 2018Date of Patent: July 11, 2023Assignee: LINDE AKTIENGESELLSCHAFTInventors: Ingo Thomas, Bernd Wunderlich
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Patent number: 11680747Abstract: In a process for the combined production of a) a hydrogen-enriched gas and a carbon monoxide-enriched gas and/or b) a mixture of hydrogen and carbon monoxide by cryogenic distillation and scrubbing, a still liquor is extracted from a scrubbing column and sent to a stripping column, a still liquor is extracted from the stripping column and sent to a separating column for carbon monoxide and methane and a cooling fluid is used at a pressure greater than that of the head of the separating column for cooling at least one fluid extracted at an intermediate level from the scrubbing column.Type: GrantFiled: November 16, 2017Date of Patent: June 20, 2023Assignee: L'Air Liquide, Societe Anonyme Pour L'Etude Et L'Exploitation Des Procedes Georges ClaudeInventors: Jean Billy, Axelle Gaertner, Antoine Hernandez, Jean-Marc Tsevery, Marie-Pascal Victor
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Patent number: 11680746Abstract: Process and plant for the production of liquid hydrogen with a liquefier that has a variable cooling power dependent on the electrical power consumed. The liquefier is supplied with electricity by a first source of electricity at least one additional source of electricity that provides an intermittent or variable amount of electricity over time. Liquid hydrogen is produced at first thermodynamic conditions when the liquefier is supplied with a predetermined nominal electrical energy level and produced at subcooled conditions, with respect to the first thermodynamic conditions, when electricity supplied to the liquefier exceeds the nominal level.Type: GrantFiled: July 8, 2020Date of Patent: June 20, 2023Assignee: L'Air Liquide, Societe Anonyme Pour L'Etude Et L'Exploitation Des Procedes Georges ClaudeInventors: Laurent Allidieres, Gregoire Rigout, Pierre Barjhoux, Pierre-Germain Marlier
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Raw material gas liquefying device and method of controlling this raw material gas liquefying device
Patent number: 11662140Abstract: A raw material gas liquefying device includes a feed line; a refrigerant circulation line; and a controller. In a refrigerant liquefaction route, a refrigerant flows through a compressor, a heat exchanger, a circulation system JT valve, a liquefied refrigerant storage tank, and the heat exchanger, and returns to the compressor. In a cryogenic energy generation route, the refrigerant flows through the compressor, the heat exchanger, an expansion unit, and the heat exchanger, and returns to the compressor. The controller determines if a refrigerant storage tank liquid level is within an allowable range, manipulates a feed system JT valve opening rate to control refrigerant temperature at the high-temperature-side refrigerant flow path exit side of the heat exchanger, and manipulates the opening rate of the feed system JT valve to control the refrigerant storage tank liquid level so that the refrigerant storage tank liquid level falls into the predetermined allowable range.Type: GrantFiled: December 4, 2017Date of Patent: May 30, 2023Assignee: KAWASAKI JUKOGYO KABUSHIKI KAISHAInventors: Tomohiro Sakamoto, Hidetaka Miyazaki, Naotaka Yamazoe, Daisuke Kariya, Yasuo Miwa, Yuichi Saitou, Yosuke Kimura, Toshihiro Komiya, Yoshihiro Matsuda, Keisuke Nakagawa -
Patent number: 11639815Abstract: A portable refrigeration system for use in transport of medicines or other valuable, temperature sensitive materials is disclosed. The system can use GPS positioning technology to provide absolute global location along with internet connection through a cellular modem on board which allows for communication to the cloud of temperature and transit data during device use. The refrigerator 10 can be powered by a rechargeable battery back that may be recharged through connection to AC mains supply or connection to the photovoltaic panel 26 included with the device 10. The insulated container can be held at a constant temperature through the use of vacuum insulated panel construction. The device 10 can be cooled through the use of thermoelectric cooling modules 68 coupled to the insulated chamber 74 and paired with a heat exchanger 56 with heat pipes 60 and a system fan 54.Type: GrantFiled: May 14, 2016Date of Patent: May 2, 2023Assignee: Stone Cold Systems, Inc.Inventors: Robert H. J. Miros, Keith B. Payea, James A. McCrea
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Patent number: 11635254Abstract: An air separation apparatus and process, which produces gaseous oxygen and/or nitrogen products at an elevated pressure through internal compression of respective liquid products, are disclosed. Split-core main heat exchangers are employed to warm up product streams generated in an air rectification unit against 1) a main feed air stream in the low-pressure heat exchanger and 2) at least one boosted pressure air stream in the high-pressure exchanger. Because the boosted pressure air stream is at a higher pressure and temperature than the main feed air stream, after separate heat exchange in the split main heat exchangers, the subsidiary waste nitrogen stream exiting the high-pressure heat exchanger is also warmer than the subsidiary waste nitrogen stream exiting the low-pressure heat exchanger. The warmer waste nitrogen stream is fed into the air purification unit for regeneration purposes and the cooler waste nitrogen stream is introduced into the nitrogen water tower to perform cooling duty.Type: GrantFiled: December 28, 2017Date of Patent: April 25, 2023Assignee: L'Air Liquide, Societe Anonyme Pour L'Etude Et L'Exploitation Des Procedes Georges ClaudeInventors: Bowei Zhao, Alain Briglia
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Patent number: 11635255Abstract: Carbon dioxide is recovered from an exhaust gas in the form of liquid carbon dioxide or supercritical carbon dioxide utilizing a rotary separator. Nitrogen gas recovered from the rotary separator can be expanded to provide cooling for carbon dioxide in a closed-loop CO2 power cycle that is used to cool the exhaust gas upstream of the rotary separator. The recovery can power itself and can produce excess electricity from waste heat.Type: GrantFiled: April 8, 2022Date of Patent: April 25, 2023Assignee: AXIP ENERGY SERVICES, LPInventors: Robert Stiles, David Thomas Stiles, Christopher Cory Vail, John Guoynes, Robert Earl Ashley
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Patent number: 11629914Abstract: The present disclosure provides an energy-efficient process for preparing nitrogen and oxygen for a glass melting furnace. A device required by the process includes a filter, a turbine air compressor, an air pre-cooling unit, alternately used molecular sieve adsorbers, an electric heater, a main heat exchanger, a rectifying tower I, a main condenser-evaporator I, a rectifying tower II, a main condenser-evaporator II, a rectifying tower III, a main condenser-evaporator III, a supercooler, an expander I and an expander II. The three rectifying towers are used to prepare a low-pressure nitrogen product and an oxygen product with a certain pressure at the same time. The oxygen product with a certain pressure is used for oxygen-enriched combustion for the glass melting furnace, and the low-pressure nitrogen product is used as shielding gas of a tin bath.Type: GrantFiled: June 13, 2022Date of Patent: April 18, 2023Assignee: Hangzhou Turning Energy Technology Development Co., Ltd.Inventors: Senlin He, Ting Wei, Lei Guo, Youzhen Zhou, Zhengjun Yang, Hang Zhu, Yunfeng Zhang
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Patent number: 11566840Abstract: A technology liquefies natural gas. The natural gas liquefaction method pre-cools treated natural gas by ethane evaporation, sub-cools liquefied gas using cooled nitrogen as a refrigerant, reduces liquefied gas pressure, separates non-liquefied gas and diverts liquefied natural gas. Before pre-cooling the natural gas is compressed, ethane is evaporated during the multi-stage pre-cooling of liquefied gas with simultaneous evaporation of ethane using cooled ethane as a refrigerant. Ethane generated by evaporation is compressed, condensed and used as a refrigerant during the cooling of liquefied gas and nitrogen, with nitrogen being compressed, cooled, expanded and fed to the natural gas sub-cooling stage. The natural gas liquefaction unit contains a natural gas liquefaction circuit, an ethane circuit and a nitrogen circuit. The natural gas liquefaction circuit includes a natural gas compressor, a cooler unit, ethane vaporizers, a closed-end subcooling heat exchanger, and a separator, connected in series.Type: GrantFiled: August 10, 2017Date of Patent: January 31, 2023Assignee: Publichnoe Aktsionernoe Obshchestvo “NOVATEK”Inventors: Rafail Minigulovich Minigulov, Sergei Vladimirovich Rudenko, Oleg Evgenievich Vasin, Dmitriy Nikolaevich Gritsishin, Evgeniy Igorevich Sobolev