Patents Examined by Katherine A. Bareford
  • Patent number: 10125053
    Abstract: A method of treating a ceramic surface containing zirconia, whereby the ceramic surface is ablated by directing a laser beam with a diameter of 200-400 ?m produced by a CO2 laser with a pulse frequency of 1200-1800 Hz onto the ceramic surface, and a N2 assist gas is concurrently applied with a pressure of 550-650 KPa co-axially with the laser beam to form an ablated ceramic surface comprising microgrooves with ZrN present on a surface of the microgrooves, wherein the ablated ceramic surface has a higher surface hydrophobicity than the ceramic surface prior to the ablating.
    Type: Grant
    Filed: May 19, 2017
    Date of Patent: November 13, 2018
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Bekir Sami Yilbas, Haider Ali
  • Patent number: 10128467
    Abstract: The invention relates to a method for depositing a target material onto an organic electrically functional material. The method includes the steps of: providing a substrate with an organic electrically functional material, like an emissive electroluminescent layer; creating a vapor plume of target material by pulsed laser deposition; depositing a first layer of target material on the organic electrically functional material, while maintaining the maximum particle velocity of the deposited particles below a preset value; and depositing a second layer of target material on the first layer of target material, while the maximum particle velocity of the deposited particles is above the preset value. The invention also relates to an intermediate product and to an organic light emitting diode.
    Type: Grant
    Filed: October 14, 2013
    Date of Patent: November 13, 2018
    Assignee: Solmates B.V.
    Inventors: Jan Matthijn Dekkers, Jan Arnaud Janssens
  • Patent number: 10072331
    Abstract: A formation method of a silicon film which contributes to improvements in cycle characteristics and an increase in charge/discharge capacity and can be used as an active material layer is provided. In addition, a manufacturing method of a power storage device including the silicon film is provided. The formation method is as follows. A crystalline silicon film is formed over a conductive layer by an LPCVD method. The supply of a source gas is stopped and heat treatment is performed on the silicon film while the source gas is exhausted. The silicon film is grown to have whisker-like portions by an LPCVD method while the source gas is supplied into the reaction space. A power storage device is manufactured using, as an active material layer included in a negative electrode, the silicon film grown to have whisker-like portions.
    Type: Grant
    Filed: June 29, 2012
    Date of Patent: September 11, 2018
    Assignee: Semiconductor Energy Laboratory Co., Ltd.
    Inventors: Toshihiko Takeuchi, Kazutaka Kuriki, Makoto Ishikawa
  • Patent number: 10060034
    Abstract: Electroless copper plating compositions including (a) copper ions, (b) a complexing agent for copper ions, (c) a reducing agent, (d) a pH adjustor and (e) a stabilizer is disclosed. The stabilizer has a specific chemical structure, and contributes to stable an electroless copper plating composition from decomposition.
    Type: Grant
    Filed: January 23, 2017
    Date of Patent: August 28, 2018
    Assignee: Rohm and Haas Electronic Materials LLC
    Inventors: Meng Qi, Sze Wei Chum, Ping Ling Li
  • Patent number: 9988713
    Abstract: A method for preparing a device having a film on a substrate is disclosed. In the method, a film is deposited on a polymeric substrate. The film includes at least one metal. A metal in the film is converted to a metal oxide using microwave radiation. One example device prepared by the method includes a polyethylene napthalate substrate and a film on the substrate, wherein the film includes a semiconducting copper oxide and silver as a dopant.
    Type: Grant
    Filed: March 12, 2014
    Date of Patent: June 5, 2018
    Assignee: Arizona Board of Regents on Behalf of Arizona State University
    Inventors: Terry Alford, Sayantan Das
  • Patent number: 9972415
    Abstract: Resin composition comprising a) the reaction product of a1) one or more epoxy compounds having at least 2 epoxy groups, and a2) sorbic acid as component A; b) a solvent containing vinyl groups as component B.
    Type: Grant
    Filed: April 4, 2012
    Date of Patent: May 15, 2018
    Assignee: ELANTAS GMBH
    Inventors: Majdi Al Masri, Anne-Gönke Huesmann, Klaus-Wilhelm Lienert, Hans-Ulrich Moritz
  • Patent number: 9950451
    Abstract: A method of manufacture of products from geopolymer composite shaped in a mold which is filled by casting of geopolymer composite in form of a precursor and after its hardening the casting is taken out from the mold and the casting surface is provided with a metallic layer. Before metal-plating casting surface with absorption capacity greater than 5% is treated to make it chemically stable so that pH of a leachate from 100 g of the bulk product in 1000 g distilled water after 24 hours does not exceed 9. In order to reduce the absorption capacity of the casting surface it is penetrated with polymer substances or particles of a non-porous filler are added into the geopolymer composite in the precursor state.
    Type: Grant
    Filed: August 29, 2012
    Date of Patent: April 24, 2018
    Assignee: IQ STRUCTURES S.R.O.
    Inventors: Tomas Tethal, Michaela Steinerova, Jiri Houfek
  • Patent number: 9920431
    Abstract: A method of preparing a substrate to receive a metal coating deposited by thermal spraying, the method including the following steps: a) depositing a layer of adhesive on the zone to be coated, the layer having a uniform thickness greater than 10 ?m and less than 100 ?m; b) before the adhesive dries, cold spraying a metal powder onto the zone to be coated, so that powder particles become embedded at least in part in the layer of adhesive; and c) drying the adhesive in which the powder particles remain held captive, thereby forming an undercoat suitable for receiving a metal coating deposited by thermal spraying. The method is applicable to protecting the leading edges of fan blades.
    Type: Grant
    Filed: July 3, 2014
    Date of Patent: March 20, 2018
    Assignee: SNECMA
    Inventors: Laurent Paul Dudon, Antonio Cremildo Arantes
  • Patent number: 9920414
    Abstract: A method for producing a ceramic layer on a surface formed from a Ni base alloy, includes the following steps: producing on the surface a ceramic layer containing ZrO2 as a main constituent; producing a gas phase having a temperature in the range from 400 to 900° C., in which a vapor formed from a salt melt with the components alkali chloride, alkali sulphate and ZnCl2 is contained in a carrier gas formed from an inert gas with an addition from 0.5 to 10% by weight HCl; and bringing the ceramic layer into contact with the gas phase for a period of time that is sufficient for an intermediate layer having a thickness of at least 0.1 ?m to form between the ceramic layer and the surface.
    Type: Grant
    Filed: January 14, 2013
    Date of Patent: March 20, 2018
    Assignee: FRAUNHOFER-GESELLSCHAFT ZUR FÖRDERUNG DER ANGEWANDTEN FORSCHUNG E. V.
    Inventors: Karl Thomas Fehr, Yaping Ye, Gerhard Wolf
  • Patent number: 9845703
    Abstract: A turbine component surface treatment process includes passing a UV-curable maskant through one or more fluid flow passages, wherein at least a portion of the UV-curable maskant exits the one or more fluid flow passages at an exterior surface of the turbine component, applying a UV light to the exterior surface of the turbine component, wherein the UV light cures at least a portion of the UV-curable maskant exiting the one or more fluid flow passages, and, treating the exterior surface with a treatment material, wherein the portion of the UV-curable maskant cured by the UV light substantially blocks the treatment material from entering the one or more fluid flow passages.
    Type: Grant
    Filed: December 12, 2014
    Date of Patent: December 19, 2017
    Assignee: General Electric Company
    Inventors: James Carroll Baummer, Thomas Robert Reid
  • Patent number: 9808885
    Abstract: A method for forming three-dimensional anchoring structures on a surface is provided. This may result in a thermal barrier coating system exhibiting enhanced adherence for its constituent coatings. The method involves applying a laser beam (10) to a surface (12) of a solid material (14) to form a liquefied bed (16) on the surface of the solid material, then applying a pulse of laser energy (18) to a portion of the liquefied bed to cause a disturbance, such as a splash (20) or a wave (25) of liquefied material outside the liquefied bed. A three-dimensional anchoring structure (22) may thus be formed on the surface upon solidification of the splash or wave of liquefied material.
    Type: Grant
    Filed: September 4, 2013
    Date of Patent: November 7, 2017
    Assignee: SIEMENS ENERGY, INC.
    Inventors: Gerald J. Bruck, Ahmed Kamel
  • Patent number: 9803271
    Abstract: A thermal coating method for applying a functional layer to a workpiece surface, particularly for applying a running surface coating to a cylinder running surface of a crankcase of an internal-combustion engine, includes the steps of: melting a coating material by use of a melting device, applying coating material droplets to the workpiece surface by use of a gas jet aimed at the workpiece surface, which gas jet blows coating material droplets from a melting location of the melting device onto the workpiece surface, and cooling or rapidly freezing the coating material droplets during their transport from the melting location to the workpiece surface.
    Type: Grant
    Filed: March 13, 2013
    Date of Patent: October 31, 2017
    Assignee: Bayerische Motoren Werke Aktiengesellschaft
    Inventors: Wolfgang Bluemlhuber, Wolfram Wagener
  • Patent number: 9786435
    Abstract: A method for producing a multilayer ceramic capacitor that includes preparing a dielectric ceramic material by mixing a perovskite compound, a Re compound, a Mn compound, a Mg compound, and a Si compound. The perovskite compound contains Ba and Ti and has 1.2×1015 or more and 4.5×1015 or less Ba vacancies per gram. Re in the Re compound is at least one element selected from Y, Gd, Tb, Dy, Ho, Er, and Yb. Green sheets containing the dielectric ceramic material are then formed. Inner electrode patterns are then formed on some of the green sheets. An unsintered capacitor body is then formed by stacking the green sheets, some of which have the inner electrode patterns formed thereon. Sintering of the unsintered capacitor body is then conducted.
    Type: Grant
    Filed: May 27, 2016
    Date of Patent: October 10, 2017
    Assignee: MURATA MANUFACTURING CO., LTD.
    Inventor: Toshimi Oguni
  • Patent number: 9765421
    Abstract: A method is described that can be used in electrodes for electrochemical devices and includes disposing a precious metal on a top surface of a corrosion-resistant metal substrate. The precious metal can be thermally sprayed onto the surface of the corrosion-resistant metal substrate to produce multiple metal splats. The thermal spraying can be based on a salt solution or on a metal particle suspension. A separate bonding process can be used after the metal splats are deposited to enhance the adhesion of the metal splats to the corrosion-resistant metal substrate. The surface area associated with the splats of the precious metal is less than the surface area associated with the top surface of the corrosion-resistant metal substrate. The thermal spraying rate can be controlled to achieve a desired ratio of the surface area of the metal splats to the surface area of the corrosion-resistant metal substrate.
    Type: Grant
    Filed: January 8, 2009
    Date of Patent: September 19, 2017
    Assignee: TREADSTONE TECHNOLOGIES, INC.
    Inventor: Conghua Wang
  • Patent number: 9743516
    Abstract: A method for forming thin film conductors is disclosed. A thin film precursor material is initially deposited onto a porous substrate. The thin film precursor material is then irradiated with a light pulse in order to transform the thin film precursor material to a thin film such that the thin film is more electrically conductive than the thin film precursor material. Finally, compressive stress is applied to the thin film and the porous substrate to further increase the thin film's electrical conductivity.
    Type: Grant
    Filed: December 3, 2012
    Date of Patent: August 22, 2017
    Assignee: NCC NANO, LLC
    Inventors: Andrew E. Edd, Charles C. Munson
  • Patent number: 9725797
    Abstract: A process for forming a ceramic coating on a substrate, such as a turbine engine component includes the steps of providing a substrate, creating a plasma which preheats the substrate, and forming a ceramic coating by injecting a powder feedstock into the plasma. The ceramic coating forming step comprises depositing ceramic particles having a mean size in the range of from 100 to 150 microns at constant particle morphology.
    Type: Grant
    Filed: April 30, 2008
    Date of Patent: August 8, 2017
    Assignee: United Technologies Corporation
    Inventors: Christopher W. Strock, Charles R. Beaudoin
  • Patent number: 9708225
    Abstract: A method of treating a ceramic surface containing zirconia, whereby the ceramic surface is ablated by directing a laser beam with a diameter of 200-400 ?m produced by a CO2 laser with a pulse frequency of 1200-1800 Hz onto the ceramic surface, and a N2 assist gas is concurrently applied with a pressure of 550-650 KPa co-axially with the laser beam to form an ablated ceramic surface comprising microgrooves with ZrN present on a surface of the microgrooves, wherein the ablated ceramic surface has a higher surface hydrophobicity than the ceramic surface prior to the ablating.
    Type: Grant
    Filed: November 17, 2015
    Date of Patent: July 18, 2017
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Bekir Sami Yilbas, Haider Ali
  • Patent number: 9689072
    Abstract: A method of depositing a thin film includes: supplying a first source gas to a reactor during a first time period; supplying a purge gas to the reactor during a second time period; supplying a second source gas to the reactor during a third time period; and supplying the purge gas to the reactor during a fourth time period, wherein the first source gas and the second source gas comprise polymer precursors, and wherein the first source gas and the second source gas are supplied at a temperature that is less than 100° C. or about 100° C. According to the method, uniformity and step coverage of a thin film can be improved by depositing an amorphous carbon layer using polymer precursors according to an Atomic layer deposition (ALD) method.
    Type: Grant
    Filed: August 31, 2015
    Date of Patent: June 27, 2017
    Assignee: ASM IP HOLDING B.V.
    Inventors: Hyung Wook Noh, Seung Woo Choi, Dong Seok Kang
  • Patent number: 9691526
    Abstract: A method for making carbon nanotube composite film is provided. An original carbon nanotube film includes carbon nanotubes joined end to end by van der Waals attractive force. The carbon nanotubes substantially extend along a first direction. A patterned carbon nanotube film is formed by patterning the original carbon nanotube film to define at least one row of through holes arranged in the original carbon nanotube film along the first direction. Each row of through holes includes at least two spaced through holes. The patterned carbon nanotube film is treated with a polymer solution. The patterned carbon nanotube film is shrunk into the carbon nanotube composite film.
    Type: Grant
    Filed: April 15, 2013
    Date of Patent: June 27, 2017
    Assignee: Beijing FUNATE Innovation Technology Co., LTD.
    Inventors: Chen Feng, Li Qian, Yu-Quan Wang
  • Patent number: 9682403
    Abstract: A spot repair method of scratch-resistant paint film: (a) sanding a part to be repaired having a scratch-resistant clear paint film thereon, (b) sanding a part to be clear gradation painted outside the part to be repaired with an abrasive material, (c) painting the part to be repaired with a color base-paint, (d) applying a clear paint wet-on-wet without curing the color base-paint, (e) applying a clear paint diluted with a gradation agent to the part to be gradation painted, (f) drying the applied paints, and (g) polishing the dried parts, wherein (1) the clear paint is a two-liquid type having an isocyanate curing agent and (2) the gradation agent comprises from 5 to 50 mass % ethyl ethoxypropionate, from 1 to 5 mass % of an acrylic resin as solid fraction, a surfactant and a curing catalyst.
    Type: Grant
    Filed: August 2, 2010
    Date of Patent: June 20, 2017
    Assignee: BASF Japan Ltd.
    Inventors: Takehito Ito, Tsutomu Shimamura, Makito Monden