Abstract: A barrier coating resin formulation comprising at least one polycarbosilane preceramic polymer, at least one organically modified silicon dioxide preceramic polymer, at least one filler, and at least one solvent. A barrier coating comprising a reaction product of the at least one polycarbosilane preceramic polymer and the at least one organically modified silicon dioxide preceramic polymer and the at least one filler is also disclosed, as are articles comprising the barrier coating, rocket motors comprising the barrier coating, and methods of forming the articles.
Abstract: Ultra-high temperature carbide (UHTC) foams and methods of fabricating and using the same are provided. The UHTC foams are produced in a three-step process, including UHTC slurry preparation, freeze-drying, and spark plasma sintering (SPS). The fabrication methods allow for the production of any kind of single- or multi-component UHTC foam, while also providing flexibility in the shape and size of the UHTC foams to produce near-net-shape components.
Type:
Grant
Filed:
December 6, 2021
Date of Patent:
October 18, 2022
Assignee:
THE FLORIDA INTERNATIONAL UNIVERSITY BOARD OF TRUSTEES
Inventors:
Arvind Agarwal, Ambreen Nisar, Tony Thomas, Kazue Orikasa, Benjamin Peter Boesl
Abstract: A dielectric film may be exposed to an acid solution such as hydrochloric acid, nitric acid, or sulfuric acid during a wet process after film formation. The inventors have newly found that when a dielectric film includes Zr having a lower ionization tendency than Ti in a main component of a metal oxide expressed by a general formula (Ba, Ca)(Ti, Zr)O3 is provided and satisfies at least one between relationships such that degree of orientation of (100) plane is higher than degree of orientation of (110) plane, and degree of orientation of (111) plane is higher than degree of orientation of (110) plane in a film thickness direction, the dielectric film is less likely to be damaged during a wet process, and the resistance to a wet process is improved.
Abstract: A method for producing a glass article having high hydrolytic resistance is provided. A glass tube consisting of borosilicate glass and having an Al2O3 content of less than 1 weight-%, a ZrO2 content of 2-12 weight-%, and a glass transition temperature Tg is reshaped into a glass article and is subsequently subjected to a thermal post-treatment. To reduce the alkali release of the glass article, the glass article is subjected to a treatment temperature of TB?Tg+5° K over a treatment time of tB?5 min and is subsequently cooled during the thermal post-treatment.
Abstract: A method of treatment of bauxite residue resulting from a Bayer process of bauxite treatment in order to produce a solid product. The method comprises mixing a quantity of the bauxite residue (1) with a quantity of a glass material (2) to form a mixture. Then, compressing the mixture (4) to form a green body, and sintering (5) the green body. After cooling, the sintered green body thereby provides the solid product.
Type:
Grant
Filed:
December 15, 2016
Date of Patent:
September 20, 2022
Assignee:
PURGONPL GROUP LIMITED
Inventors:
James Patrick Sherry, John Bowles, David Shanahan, Stephen Jennings, Geoffrey Salt
Abstract: The present invention is a method for obtaining a ceramic slurry for the production of filaments for 3D FDM printing, comprising adding a polysaccharide, a glycol or an ethanolamine as a gelling agent to a suspension of ceramic material in order to produce said ceramic slurry. The invention also comprises the green body obtained from said slurry and the ceramic filament extruded from the green body.
Type:
Grant
Filed:
April 4, 2017
Date of Patent:
September 20, 2022
Assignee:
UNIVERSIDAD DE CASTILLA LA MANCHA
Inventors:
Jesús Canales Vázquez, Gloria Begoña Sánchez Bravo, Juan Ramón Marín Rueda, Vicente Yagüe Alcaraz, Juan José López López
Abstract: A method of making an ceramic article according to an exemplary embodiment of this disclosure, among other possible things includes arranging fiber plies into a preform, inserting one or more sacrificial springs to the preform, infiltrating the preform with a matrix material to form an article, and thermally degrading the one or more sacrificial springs to form cooling holes. A ceramic article and a gas turbine engine component are also disclosed.
Abstract: A biocidal additive formulation comprises a silver containing glass particle, and a combination of at least two metal based compounds. A metal in each of the metal based compounds is selected from the group consisting of silver, copper, zinc, mercury, tin, lead, bismuth, barium, cadmium, chromium, titanium, and a combination thereof. Another biocidal additive formulation comprises a silver containing glass particle, ZnO, and Bi2O3. A glass substrate possessing a durable biocidal property and an article possessing a durable biocidal property are also provided.
Abstract: An electrophoretic deposition method of forming a boron nitride (BN) nanotube interface coating on ceramic fibers has been developed. The method comprises immersing first and second electrodes in a suspension including surface-modified BN nanotubes, where the first electrode includes ceramic fibers positioned on a surface thereof. The surface-modified BN nanotubes comprise BN nanotubes with an electrically charged polymer adsorbed on surfaces thereof. A voltage is applied to the first and second electrodes, and the surface-modified BN nanotubes move toward the first electrode and deposit on the ceramic fibers. After the deposition of the surface-modified BN nanotubes, the ceramic fibers are removed from the suspension and heat treated. Accordingly, a BN nanotube interface coating is formed on the ceramic fibers.
Type:
Grant
Filed:
June 2, 2020
Date of Patent:
September 6, 2022
Assignees:
ROLLS-ROYCE CORPORATION, ROLLS-ROYCE HIGH TEMPERATURE COMPOSITES INC.
Abstract: There are provided a cubic boron nitride sintered body having a surface also excellent in adhesiveness to a ceramic coating film, while having excellent wear resistance and defect resistance, and a manufacturing method thereof, and a tool. The cubic boron nitride sintered body of the present invention includes 60.0 to 90.0% by volume of cubic boron nitride, the remainder being a binder phase, wherein the binder phase contains: at least any of a nitride, a boride, and an oxide of Al; at least any of a carbide, a nitride, a carbonitride, and a boride of Ti; and a compound represented by the following formula (1): W2NixCo(1-x)B2(0.40?x<1)??(1).
Abstract: A glass composition comprising: Al2O3, ZnO, and SiO2; TiO2, in the amount of at least 10 mol % and not greater than 20 mol %; and alkaline metal oxide selected from the group consisting of MgO, CaO, SrO, BaO, or any combination thereof, such that the molar sum of MgO, CaO, SrO, BaO, and ZnO, in the amount in the glass composition is least 20 mol % and not greater than 35 mol %, and such that: the amount of BaO is 0 to 10 mol %; the amount of MgO is 0 to 10 mol % the amount of CaO is 0 to 10 mol %, and the molar sum of CaO and MgO in the glass composition is less than 12.5 mol %; and rare earth metal oxides (?REmOn), in the amount of at least 1.5 mol % and not greater than 10 mol %; alkali metal oxides (?Alk2O), in the amount of greater than or equal to 0 mol % and less than or equal to 5 mol %; and not greater than 5 mol % of other components; and wherein ?5 mol %?Al2O3 (mol %)?1.5 ?REmOn (mol %)??Alk2O (mol %)?+5 mol %.
Abstract: A variable-temperature and fast-sintering process for an alumina-doped zinc oxide target material is provided. Integrated degreasing and sintering processes are carried out on an alumina-doped zinc oxide biscuit, The degreasing process is carried out in air atmosphere, and a high-density alumina-doped zinc oxide target material is produced by a variable-temperature treatment during the sintering process under a state of circulating controllable mixed atmosphere. The mixed atmosphere is air and oxygen. As a result, a sintering time is greatly reduced, so that a fast-activated sintering is realized to inhibit grain growth.
Type:
Grant
Filed:
September 29, 2021
Date of Patent:
August 2, 2022
Assignee:
ZHENGZHOU UNIVERSITY
Inventors:
Benshuang Sun, Yang Liu, Jilin He, Xueyun Zeng, Yongchun Shu, Jie Chen, Zhenhua Hao
Abstract: Setter plates are fabricated from Li-stuffed garnet materials having the same, or substantially similar, compositions as a garnet Li-stuffed solid electrolyte. The Li-stuffed garnet setter plates, set forth herein, reduce the evaporation of Li during a sintering treatment step and/or reduce the loss of Li caused by diffusion out of the sintering electrolyte. Li-stuffed garnet setter plates, set forth herein, maintain compositional control over the solid electrolyte during sintering when, upon heating, lithium is prone to diffuse out of the solid electrolyte.
Abstract: A ceramic slurry for forming a ceramic article includes a binder, a first plurality of ceramic particles having a first morphology, a second plurality of ceramic particles having a second morphology that is different from the first morphology; and a photoinitiator. A method for using this slurry for fabricating ceramic articles is presented as well.
Type:
Grant
Filed:
December 12, 2019
Date of Patent:
July 19, 2022
Assignee:
General Electric Company
Inventors:
Cathleen Ann Hoel, Xi Yang, Michael Joseph O'Brien
Abstract: A diffuser material of synthetically produced, pore-containing quartz glass and a method for the manufacture of a molded body consisting fully or in part thereof. The diffuser material has a chemical purity of at least 99.9% SiO2, a cristobalite content of not more than 1%, and a density in the range of 2.0 to 2.18 g/cm3. Starting therefrom, to indicate a diffuser material which is improved with respect to diffuse reflectivity with Lambertian behavior over a wide wavelength range, high material homogeneity and UV radiation resistance, the quartz glass has a hydroxyl group content in the range of at least 200 wt. ppm and at least 80% of the pores have a maximum pore dimension of less than 20 ?m.
Type:
Grant
Filed:
February 13, 2017
Date of Patent:
July 19, 2022
Assignee:
HERAEUS QUARZGLAS GMBH & CO. KG
Inventors:
Gerrit Scheich, Frank Nuernberg, Andreas Goetzendorfer, Nadine Tscholitsch, Bernhard Franz, Ursula Klett, Matthew Donelon
Abstract: In embodiments, a precursor glass comprising from about 55 wt. % to about 80 wt. % SiO2; from about 5 wt. % to about 20 wt. % Al2O3; from about 5 wt. % to about 20 wt. % Li2O; from about 2 wt. % to about 4 wt. % P2O5; and from about 0.2 wt. % to about 15 wt. % ZrO2.
Type:
Grant
Filed:
December 11, 2020
Date of Patent:
July 12, 2022
Assignee:
Corning Incorporated
Inventors:
George Halsey Beall, Qiang Fu, Charlene Marie Smith
Abstract: A cubic boron nitride sintered material includes: more than 80 volume % and less than 100 volume % of cubic boron nitride grains; and more than 0 volume % and less than 20 volume % of a binder phase. The binder phase includes: at least one selected from a group consisting of a simple substance, an alloy, and an intermetallic compound selected from a group consisting of a group 4 element, a group 5 element, a group 6 element in a periodic table, aluminum, silicon, cobalt, and nickel. A dislocation density of the cubic boron nitride grains is more than or equal to 3×1017/m2 and less than or equal to 1×1020/m2.
Type:
Grant
Filed:
December 16, 2019
Date of Patent:
July 5, 2022
Assignees:
Sumitomo Electric Industries, Ltd., SUMITOMO ELECTRIC HARDMETAL CORP.
Abstract: The invention relates to a sliding member having a first sliding surface, wherein the first sliding surface (29) comprises a particulate support material (6) and a graphene-containing material (7), wherein the particulate support material (6) is at least partially coated with the graphene-containing material (7), and wherein a material bond (14) is present between the particulate support material (6) and the graphene-containing material (7).
Type:
Grant
Filed:
July 5, 2018
Date of Patent:
June 21, 2022
Assignee:
EagleBurgmann Germany GmbH & Co. KG
Inventors:
Rolf Mulhaupt, Jorg Thomas Thelke, Wenli Zhang