Patents Examined by Scott L. Hertzog
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Patent number: 5849074Abstract: A method for making magnetic ink compositions is disclosed. The magnetic particles used in the ink are prepared from an aqueous slurry. A surface derivatizing agent is added to the slurry to render the magnetic pigment particles hydrophobic. The particles then sink to the bottom of the slurry, and the bulk water is then removed. After air drying, dry magnetic pigment particles are provided. The particles will be hydrophobic, and thus will have superior resistance to water as compared to previously known magnetic pigment particles. Magnetic ink compositions are formulated from the magnetic particles.Type: GrantFiled: July 19, 1996Date of Patent: December 15, 1998Assignee: Videojet Systems International, Inc.Inventor: Wing Sum Vincent Kwan
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Patent number: 5849817Abstract: The present invention relates to a metal pigment, comprising a particle, preferably a flake, of iron or an alloy thereof, having on its surface a colored coating, formed by exposing the said particle to an elevated temperature in an oxygen-containing atmosphere. The product finds use in surface coatings and in the mass coloration of plastics, especially where a colored "glitter" effect is required.Type: GrantFiled: November 7, 1997Date of Patent: December 15, 1998Assignee: Silberline LimitedInventors: William Innes Green, Jonathan Joseph Whistler Knox
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Patent number: 5849073Abstract: A pigment for sensing gas leakage can be produced by adding at least one of salts of platinum group metals to a slurry of particulate substrate, neutralizing the resultant mixture to deposit at least one of oxides, hydroxides and hydrated oxides of platinum group metals on the surfaces of said particulate substrate, and if necessary, further adding to said slurry at least one of compounds of aluminum, silicon, titanium, zinc, zirconium, tin, antimony and cerium, neutralizing the resultant mixture to deposit at least one of compounds such as oxides, hydroxides and hydrated oxides of aluminum, silicon, titanium, zinc, zirconium, tin, antimony and cerium, on the particles.Type: GrantFiled: February 18, 1998Date of Patent: December 15, 1998Assignees: Ishihara Sangyo Kaisha, Ltd., Act Research, Inc.Inventors: Masashi Sakamoto, Haruo Okuda, Hideo Futamata
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Patent number: 5846309Abstract: A coarse particle kaolin clay is provided having an average Stokes equivalent particle diameter of about 4.5-6.0 microns, a BET surface area of about 8-11 m.sup.2 /g, and preferably having a median Malvern particle size of about 9.0-10.5 microns as determined by laser light-scattering measurement and a high aspect ratio preferably of about 12-14 as determined by Sphericity Model calculations. The coarse particle kaolin clay provides low viscosity build, good reinforcement properties and excellent surface finish qualities as a filler in thermoset composite materials, such as polyester molding compounds, and also provides excellent pigmenting properties in paints and industrial coatings.Type: GrantFiled: February 20, 1997Date of Patent: December 8, 1998Assignee: J. M. Huber CorporationInventors: Gary M. Freeman, John M. M. Harrison, Kenneth B. Files
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Patent number: 5843220Abstract: The present invention relates to a process for preparing a pigment composition whereby a mixture of an organic pigment and an inorganic filler is subjected to an air jet milling step. The inventive process is an environmentally friendly process which yields pigments having outstanding dispersibility and wetting characteristics when incorporated in plastics, aqueous or solvent based coatings and inks.Type: GrantFiled: December 1, 1997Date of Patent: December 1, 1998Assignee: Ciba Specialty Chemicals CorporationInventor: Fridolin Babler
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Patent number: 5840112Abstract: A process for reacting titanium tetrachloride vapors with oxygen including a first oxygen preheat assembly for preheating oxygen to a first predetermined temperature and a titanium tetrachloride preheat assembly for preheating titanium tetrachloride to a relatively low, temperature. The process includes adding a second oxygen preheat assembly for preheating oxygen to a second temperature substantially below the first temperature, and includes a second reaction zone adapted for receiving the mixture from the first reaction zone, the oxygen at the second temperature being reacted with the titanium tetrachloride in the mixture from the first reaction zone to produce titanium dioxide. Also provided is a process for the preparation of titanium dioxide comprising reacting titanium tetrachloride with oxygen at an elevated pressure and at a temperature above about 1750.degree. F.Type: GrantFiled: July 25, 1996Date of Patent: November 24, 1998Assignee: Kerr McGee Chemical CorporationInventors: A. J. Morris, J. C. Magyar, G. D. Wootten, W. A. Yuill
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Patent number: 5837045Abstract: A surface-modified colored pigment is disclosed which includes a colored pigment having no primary amines and at least one attached hydrophilic organic group, wherein said organic group comprises a) at least one aromatic group, and b) at least one ionic group or ionizable group, or a mixture of an ionic group or an ionizable group. The colored pigment may be blue, brown, cyan, green, violet, magenta, red, orange, yellow, mixtures thereof and the like. The surface-modified colored pigment, due to the hydrophilic groups on its surface, is readily dispersed in a liquid vehicle without the addition of a surfactant or other dispersing aid or additive. The surface-modified color pigment may be used in a variety of aqueous systems including, but not limited to, coatings, paints, papers, adhesives, latexes, inks, toners, textiles and fibers. In addition, an aqueous composition is disclosed including water-based liquid vehicle and the surface-modified colored pigment described above.Type: GrantFiled: June 17, 1996Date of Patent: November 17, 1998Assignee: Cabot CorporationInventors: Joseph E. Johnson, James A. Belmont
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Patent number: 5837041Abstract: Ink cartridges containing ink compositions containing nanometer scale pigment particles are produced by preparing a pigment solution including a solubilized pigment-Lewis acid complex and an aprotic solvent system, separating the pigment from the pigment solution to form pigmented particles either by precipitating pigment nanoparticles or by dyeing colloidal particles with the solubilized pigment-Lewis acid complex, concentrating the pigmented particles, then dispersing the pigmented particles in a formulating solvent to form an ink composition, and finally introducing the ink composition into an ink cartridge. The ink compositions are particularly suitable for use in ink jet ink cartridges.Type: GrantFiled: April 15, 1997Date of Patent: November 17, 1998Assignee: Xerox CorporationInventors: Lloyd F. Bean, Bing R. Hsieh, Leonard M. Carreira
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Patent number: 5837051Abstract: The present invention relates to a process for the production of iron oxide brown, red and black pigments and to the use thereof.Type: GrantFiled: December 13, 1995Date of Patent: November 17, 1998Assignee: Bayer AGInventors: Jorg Krekel, Berndt-Ullrich Kohler, Horst Brunn
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Patent number: 5833747Abstract: There is disclosed a method for the preparation of a precipitated calcium carbonate (PCC) for use as a pigment in paper coating compositions, the method comprising the steps of (a) carbonating an aqueous lime-containing medium to produce an aqueous suspension of a PCC predominantly in a selected crystal form, (b) at least partially dewatering the PCC-containing suspension; and (c) subjecting the PCC-containing suspension to comminution by high shear attrition grinding with an attrition grinding medium. Steps (b) and (c) may be applied in either order, ie. (b) followed by (c) or alternatively (c) followed by (b). The dewatering step (b) is preferably carried out using a pressure filter device operating at a pressure of at least 5 MPa, preferably at least 10 MPa. A pH reduction step may be applied after steps (b) and (c). Also disclosed are pigments produced by the method and pigment and paper coating compositions including such pigments.Type: GrantFiled: October 9, 1996Date of Patent: November 10, 1998Assignee: ECC International Ltd.Inventors: Ian Stuart Bleakley, Philip Martin McGenity, Christopher Nutbeem
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Patent number: 5830267Abstract: The invention relates to the coloration of high molecular weight organic materials in the mass with soluble phthalocyanine precursors of structure ##STR1## or isomers thereof, to the soluble phthalocyanine precursors as such wherein M is Zn, Ti or V or wherein L.sub.1 is morpholino, pyrrolidino or with C.sub.1 -C.sub.12 alkyl substituted piperidino, to compositions containing high molecular weight organic materials and the above soluble phthalocyanine precursors, and to a process for making structured color images and applications thereof.Type: GrantFiled: May 6, 1996Date of Patent: November 3, 1998Assignee: Ciba Specialty Chemicals CorporationInventors: John Zambounis, Heinz Wolleb
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Patent number: 5827363Abstract: A method for preparing precipitated silicates and silicas having good high shear rheology in high solids aqueous slurries. Destructuring of aluminum silicate and silica via dry milling results in decreasing DBP oil absorption. The destructured materials are useful for ink jet coating formulations.Type: GrantFiled: December 17, 1996Date of Patent: October 27, 1998Assignee: Degussa CorporationInventors: Michael S. Darsillo, Sturgis Gregg Allen
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Patent number: 5827364Abstract: Pigment compositions comprising a pigment and both a phthalimidomethylquinacridone and a pyrazolylmethylquinacridone as additives are disclosed. The disclosed pigment compositions are useful for coloring coating compositions. Coating composition colored with the inventive pigment compositions have excellent rheological characteristics and which yield coatings having excellent saturation.Type: GrantFiled: February 21, 1997Date of Patent: October 27, 1998Assignee: Ciba Specialty Chemicals CorporationInventor: Shivakumar Basalingappa Hendi
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Patent number: 5824144Abstract: A pigment in the form of metallic platelets is mixed with a sticky viscous liquid. The resulting pigment can be combined with a powdery film-forming polymer to produce a film-forming composition which can be applied by electrostatic coating.Type: GrantFiled: April 11, 1997Date of Patent: October 20, 1998Assignee: Engelhard CorporationInventors: Mingbo He, Michael T. Venturini
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Patent number: 5824146Abstract: This invention relates to a new method for making a photodurable, aqueous titanium dioxide (TiO.sub.2) pigment slurry. This method involves reacting titanium tetrachloride, aluminum chloride and an oxygen-containing gas in the presence of a nucleant in the vapor phase to produce TiO.sub.2 pigment. A sufficient amount of aluminum chloride is added to provide at least 2 wt. % alumina in the TiO.sub.2 pigment. The TiO.sub.2 pigment is separated from the reaction gases; and mixed with sufficient water to produce a TiO.sub.2 slurry comprising at least 78 wt. % TiO.sub.2 solids. The slurry may be used in coating formulations such as paints.Type: GrantFiled: July 3, 1997Date of Patent: October 20, 1998Assignee: E. I. du Pont de Nemours and CompanyInventor: Michael Warren Ott
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Patent number: 5824145Abstract: This invention relates to a new method for making a photodurable, aqueous titanium dioxide (TiO.sub.2) pigment slurry. The method involves mixing amorphous alumina, TiO.sub.2 pigment particles, water, and at least one dispersant to form the slurry. The initial slurry comprises at least about 78 wt. % TiO.sub.2 solids and at least about 3 wt. % alumina. The resulting slurry may be diluted to a lower TiO.sub.2 solids content and subsequently screened and media-milled. The titanium dioxide pigment slurry is suitable for use in coatings formulations such as paints.Type: GrantFiled: May 14, 1997Date of Patent: October 20, 1998Assignee: E. I. du Pont de Nemours and CompanyInventors: Robert Elroy Marganski, Michael Warren Ott
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Patent number: 5820667Abstract: The specification discloses a method for treating a pigment presscake containing pigment and water to remove the water therefrom. The method is carried out by contacting the presscake with a flushing agent containing an uncatalyzed or acid catalyzed rosin ester and an ink oil to provide a mixture containing the pigment, the flushing agent and water which is then separated from the mixture by well known separation techniques such as decanting to provide a flushed pigment. The specification also discloses a flushing agent and an ink composition containing the uncatalyzed or acid catalyzed rosin ester.Type: GrantFiled: March 27, 1997Date of Patent: October 13, 1998Assignee: Arizona Chemical CompanyInventors: Zheng Lu, Thomas C. Jordan
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Patent number: 5814144Abstract: For paints and the like, an aqueous tinter which does not block dispensing nozzles and which has a viscosity of from 0.05 to 1.5 Ns/m.sup.2 (20.degree. C.) and which contains pigment particles, water, micellising dispersant and a non-micellising auxiliary material. The weight ratio of dispersant to pigment must exceed the ratio which would be present at the Daniel Flow Point for a notional tinter consisting only of the pigment, water and the dispersant. The amount of auxiliary material must be sufficient to enable the tinter to be expelled through a bore 2 mm in diameter and 15 mm long by a pressure of not more than 320 MN/m.sup.2 after storage in the bore at 25.degree. C. for 18 hours under a relative humidity of 50%. Preferred dispersants comprise long chain hydrophilic and long chain hydrophobic moieties which may be poly(alkylene glycol) esters of long chain fatty acids or hydrophobic backbone copolymers with pendant poly(alkylene glycol) moieties as hydrophilic side chains.Type: GrantFiled: August 3, 1995Date of Patent: September 29, 1998Assignee: Imperial Chemical Industries PLCInventors: Jennifer Ruth Coutts, Jonathan Albert Graystone, Trevor Stephen Beverley Sayer
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Patent number: 5814141Abstract: The invention relates to a liquid crystalline, photo cross-linkable main-chain polymer used as interferentially effective, chromophoric substance for colored paints, in which the main mesogenic groups are disposed at least approximately in a chiral-nematic manner. An etherified cellulose ether or a mixture of several etherified cellulose ethers is used pursuant to the invention as liquid crystalline main-chain polymer or polymers wherein:the cellulose ethers have a molecular weight of 500 to 1,000,000,the anhydroglucose units of the cellulose ethers are etherified with an average degree of molar substitution of 2 to 7 with propylene oxide or ethylene oxide units (C.sub.3 H.sub.6 O- or C.sub.2 H.sub.4 O-units), andthe cellulose ethers are etherified with an average degree of molar substitution of 1.5 to 3 with unsaturated hydrocarbon groups (C.sub.r H.sub.2r-1).Type: GrantFiled: November 27, 1996Date of Patent: September 29, 1998Assignee: Daimler-Benz AGInventors: Martin Kirschbaum, Maria-Theresia Sailer, Fritz Dannenhauer, Hartmut Seliger
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Patent number: 5814143Abstract: A synthetic alkali metal silicate pigment is modified with a source of a water soluble zirconium ion to form an oxy-hydroxy zirconium species precipitate on the pigment surface. The surface modified pigment is made by slurrying the pigment and reacting it with the source of a water soluble zirconium ion. The surface modified pigment provides improvements over conventional synthetic alkali metal silicate pigments in terms of optical properties, particularly in paper applications, and physical properties, particularly in rubber applications. The surface modified pigment is also useful as an extender or replacement for TiO.sub.2, a conventional synthetic alkali metal silicate such as a sodium-aluminosilicate pigment, a clay, a calcined clay or the like.Type: GrantFiled: November 21, 1997Date of Patent: September 29, 1998Assignee: J.M. Huber CorporationInventors: Gary M. Freeman, Richard C. Zielke