Abstract: The invention relates to a process and apparatus of extraction with the use of vacuum and can be used to extract the bioactive agents from raw materials. The method of extraction of materials, includes the heating the extractant, the preliminary extraction of raw materials with the heated rollers by means of extractant, the impregnation of raw material with extractant and extraction of raw materials in vacuum-impulsive mode by cycles, which include the heating with hot coolant gas not exceeding 39° C. and a creation of vacuum in the chamber in the regime of quick vacuum-impulsive exposure with stepwise multiple pressure drop from the atmospheric pressure to the pressure not more 0.0001 MPa, followed by keeping under vacuum to stabilize the temperature of the mixture and the vacuum relief at the end of the cycle. The distilled water, or organic solvents or mixtures thereof are used as the extractants.

Abstract: The present invention relates to the vacuum drying of capillary porous bulk materials. The method involves preheating of the material, its loading into the vacuum drying chamber having heating elements followed by cycle-by-cycling heating of the material and vacuum creation in the rapid vacuum impulse action mode with stage-by-stage single or multiple reduction of pressure in the range from 0.1 MPa to 0.0001 MPa followed by the exposure to vacuum unless the material temperature is stabilized. Said cycles are repeated unless the required material moisture is achieved. Cooling of the material is performed in the same drying chamber by alternating cooling in spouted bed and vacuum impulse action. The device comprises two vacuum chambers cone-shaped at their bases with heaters mounted inside them, material loading/unloading system, one or several receivers with pumps connected in parallel to them and connected via vacuum pipeline system with quick-acting valves to the drying chamber inlet.

Abstract: The invention relates to a process and apparatus of extraction with the use of vacuum and can be used to extract the bioactive agents from raw materials. The method of extraction of materials, includes the heating the extractant, the preliminary extraction of raw materials with the heated rollers by means of extractant, the impregnation of raw material with extractant and extraction of raw materials in vacuum-impulsive mode by cycles, which include the heating with hot coolant gas not exceeding 39° C. and a creation of vacuum in the chamber in the regime of quick vacuum-impulsive exposure with stepwise multiple pressure drop from the atmospheric pressure to the pressure not more 0.0001 MPa, followed by keeping under vacuum to stabilize the temperature of the mixture and the vacuum relief at the end of the cycle.

Abstract: The present invention relates to the vacuum drying of capillary porous bulk materials. The method involves preheating of the material, its loading into the vacuum drying chamber having heating elements followed by cycle-by-cycling heating of the material and vacuum creation in the rapid vacuum impulse action mode with stage-by-stage single or multiple reduction of pressure in the range from 0.1 MPa to 0.0001 MPa followed by the exposure to vacuum unless the material temperature is stabilized. Said cycles axe repeated unless the required material moisture is achieved. Cooling of the material is performed in the same drying chamber by alternating cooling in spouted bed and vacuum impulse action. The device comprises two vacuum chambers cone-shaped at their bases with heaters mounted inside them, material loading/unloading system, one or several receivers with pumps connected in parallel to them and connected via vacuum pipeline system with quick-acting valves to the drying chamber inlet.