Abstract: A method of operating a charged particle microscope comprising: Providing a specimen on a specimen holder; Using a source to produce a beam of charged particles, and irradiating the specimen with said beam; Using a detector to detect X-ray radiation emanating from the specimen in response to said irradiation, and to produce a spectrum comprising X-ray characteristic peaks on a Bremsstrahlung background, comprising the following additional steps: Using an elemental decomposition algorithm to analyze the characteristic peaks in said spectrum, thereby determining a reference group of major chemical elements contributing to the spectrum; Calculating an average atomic number for said reference group, and using this in a predictive model to generate a calculated Bremsstrahlung profile for the reference group; Fitting said calculated Bremsstrahlung profile to the Bremsstrahlung background in said spectrum, and attributing a discrepancy between the latter and the former to a residual element absent from, or inc

Abstract: A method of operating a charged particle microscope comprising: Providing a specimen on a specimen holder; Using a source to produce a beam of charged particles, and irradiating the specimen with said beam; Using a detector to detect X-ray radiation emanating from the specimen in response to said irradiation, and to produce a spectrum comprising X-ray characteristic peaks on a Bremsstrahlung background, comprising the following additional steps: Using an elemental decomposition algorithm to analyze the characteristic peaks in said spectrum, thereby determining a reference group of major chemical elements contributing to the spectrum; Calculating an average atomic number for said reference group, and using this in a predictive model to generate a calculated Bremsstrahlung profile for the reference group; Fitting said calculated Bremsstrahlung profile to the Bremsstrahlung background in said spectrum, and attributing a discrepancy between the latter and the former to a residual element absent from, or inco

Abstract: A method and apparatus are provided for identifying a material with a sample-specific reference spectral list or library. A sequential approach to SEM-EDS automated mineralogy classification is carried out by performing two or more material classification analyses. A pre-classification step restricts the processing of spectra deconvolution algorithms to a subset of spectra that pass a dominant mineral criteria resulting in a significantly reduced subset of reference spectra that occur within the measured sample in pure enough form at a given minimum quantity. The following complex classification stages involving deconvolution of multiple constituents within measured spectra is based on this sample relevant subset.

Abstract: Method and apparatus for analysis and display of fine grained mineral samples. A portion of the sample is illuminated with a charged particle beam. Emitted radiation is detected, and a sample emission spectrum is generated and fit with a plurality of standard emission spectra of minerals in a candidate mineral composition. A mineral composition whose emission spectrum best fits the sample emission spectrum is selected from a plurality of candidate mineral compositions. An assigned color is received for each mineral in the selected mineral composition, and the assigned colors are blended according to the proportion of each mineral in the selected mineral composition. An image pixel corresponding to the portion of the sample is rendered for display.

Abstract: A method and apparatus are provided for identifying a material with a sample-specific reference spectral list or library. A sequential approach to SEM-EDS automated mineralogy classification is carried out by performing two or more material classification analyses. A pre-classification step restricts the processing of spectra deconvolution algorithms to a subset of spectra that pass a dominant mineral criteria resulting in a significantly reduced subset of reference spectra that occur within the measured sample in pure enough form at a given minimum quantity. The following complex classification stages involving deconvolution of multiple constituents within measured spectra is based on this sample relevant subset.

Abstract: Method and apparatus for analysis and display of fine grained mineral samples. A portion of the sample is illuminated with a charged particle beam. Emitted radiation is detected, and a sample emission spectrum is generated and fit with a plurality of standard emission spectra of minerals in a candidate mineral composition. A mineral composition whose emission spectrum best fits the sample emission spectrum is selected from a plurality of candidate mineral compositions. An assigned color is received for each mineral in the selected mineral composition, and the assigned colors are blended according to the proportion of each mineral in the selected mineral composition. An image pixel corresponding to the portion of the sample is rendered for display.

Abstract: Wellbore servicing fluids and methods of using the same to service a wellbore in a subterranean formation are provided. A filter cake in the wellbore is contacted with the gravel packing fluid, which comprises an oil-soluble additive capable of removing the filter cake. The additive undergoes hydrolysis to produce an acid upon contacting water provided from, for example, water in the wellbore servicing fluid, connate water in the subterranean formation, water in the filter cake, water produced by the subterranean formation, water pumped into the wellbore, or combinations thereof. The acid dissolves particulates in the filter cake in situ. In an embodiment in which the wellbore servicing fluid serves as a gravel packing fluid, the fluid also deposits gravel along the face of the subterranean formation, forming a barrier against the migration of sand from the formation and into the wellbore.

Abstract: Methods and compositions for sealing subterranean zones having temperatures in the range of about 80° F. to about 300° F. are provided. In a method of the invention, a sealing composition of the invention of water, a substantially fully hydrated depolymerized polymer and poly lactic acid, with a pH above about 8.5, is introduced into the subterranean zone wherein it becomes substantially rigid and seals the zone when exposed to subterrnean zone temperatures above about 80° F.

Abstract: Wellbore servicing fluids and methods of using the same to service a wellbore in a subterranean formation are provided. A filter cake in the wellbore is contacted with the gravel packing fluid, which comprises an oil-soluble additive capable of removing the filter cake. The additive undergoes hydrolysis to produce an acid upon contacting water provided from, for example, water in the wellbore servicing fluid, connate water in the subterranean formation, water in the filter cake, water produced by the subterranean formation, water pumped into the wellbore, or combinations thereof. The acid dissolves particulates in the filter cake in situ. In an embodiment in which the wellbore servicing fluid serves as a gravel packing fluid, the fluid also deposits gravel along the face of the subterranean formation, forming a barrier against the migration of sand from the formation and into the wellbore.

Abstract: An apparatus and method for completing an interval of a wellbore while drilling comprises a drill string (52) having a drill bit (30) mounted on the lower end thereof. A completion assembly (50) is positioned around a section of the drill string (52) such that when the wellbore (32) is extended by rotating the drill bit (30) and advancing the drill string (52), the completion assembly (50) does not rotate. The advancement of the drill string (52) and rotation of the drill bit (30) is ceased when the completion assembly (50) has reached the desired interval of the wellbore (32). Thereafter, the drill string (52) is disconnected from the drill bit (30) for retrieval to the surface leaving the completion assembly (50) and the drill bit (30) downhole.

Abstract: An expandable sand control screen (100) that is positionable within a wellbore comprises a fluid permeable generally tubular member (102) that is expanded downhole. A filtering assembly is disposed exteriorly of the generally tubular member (102). The filtering assembly includes a filter medium (106) that prevents the flow of particulate material of a predetermined size therethrough but allows the flow of production fluids therethrough. The filtering assembly also includes a compliable member (118) that has a thickness that is radially variable downhole. During or after expansion of the expandable sand control screen (100), the radial variability of the thickness of the compliable member (118) allows the expandable sand control screen (100) to comply with any irregularities in the wellbore profile, thereby preventing any void regions between the expandable sand control screen (100) and the wellbore.

Abstract: Methods and compositions for sealing subterranean zones having temperatures in the range of about 80° F. to about 300° F. are provided. In a method of the invention, a sealing composition of the invention of water, a substantially fully hydrated depolymerized polymer and poly lactic acid, with a pH above about 8.5, is introduced into the subterranean zone wherein it becomes substantially rigid and seals the zone when exposed to subterranean zone temperatures above about 80° F. The methods and compositions are particularly advantageous for use in producing zones because the rigid sealing composition self dissolves over time, freeing the seal and the zone for production of fluids. Moreover, the composition is environmentally compatible.

Abstract: An expandable sand control screen (100) that is positionable within a wellbore comprises a fluid permeable generally tubular member (102) that is expanded downhole. A filtering assembly is disposed exteriorly of the generally tubular member (102). The filtering assembly includes a filter medium (106) that prevents the flow of particulate material of a predetermined size therethrough but allows the flow of production fluids therethrough. The filtering assembly also includes a compliable member (118) that has a thickness that is radially variable downhole. During or after expansion of the expandable sand control screen (100), the radial variability of the thickness of the compliable member (118) allows the expandable sand control screen (100) to comply with any irregularities in the wellbore profile, thereby preventing any void regions between the expandable sand control screen (100) and the wellbore.

Abstract: An apparatus and method for completing an interval of a wellbore while drilling comprises a drill string (52) having a drill bit (30) mounted on the lower end thereof. A completion assembly (50) is positioned around a section of the drill string (52) such that when the wellbore (32) is extended by rotating the drill bit (30) and advancing the drill string (52), the completion assembly (50) does not rotate. The advancement of the drill string (52) and rotation of the drill bit (30) is ceased when the completion assembly (50) has reached the desired interval of the wellbore (32). Thereafter, the drill string (52) is disconnected from the drill bit (30) for retrieval to the surface leaving the completion assembly (50) and the drill bit (30) downhole.

Abstract: In general, a method is provided for completing a subterranean wellbore, and an apparatus for using the method. The method comprises positioning an expandable sand-control device in the wellbore thereby forming an annulus between the sand-control device and the wellbore; depositing a filter media in the annulus; and after the depositing step, radially expanding the sand-control device to decrease the volume of the annulus. The sand-control device can be a sand screen or slotted or perforated liner having radially extending passageways in the walls thereof, the passageways designed to substantially prevent movement of the particulate material through the passageways and into the sand-control device. Where a slotted liner is desired, the passageways can be plugged during positioning and later unplugged for production.

Abstract: In general, a method is provided for completing a subterranean wellbore, and an apparatus for using the method. The method comprises positioning an expandable sand-control device in the wellbore thereby forming an annulus between the sand-control device and the wellbore; depositing a filter media in the annulus; and after the depositing step, radially expanding the sand-control device to decrease the volume of the annulus. The sand-control device can be a sand screen or slotted or perforated liner having radially extending passageways in the walls thereof, the passageways designed to substantially prevent movement of the particulate material through the passageways and into the sand-control device. Where a slotted liner is desired, the passageways can be plugged during positioning and later unplugged for production.

Abstract: A well service fluid and method using same for brine-sensitive formations is disclosed. The fluid is an invert oil emulsion comprising heavy, solids-free brine, an oil or synthetic, and sufficient emulsifier to create the emulsion. The fluid has particular applicability in gravel packing a horizontal well.

Abstract: In general, a method is provided for completing a subterranean wellbore, and an apparatus for using the method. The method comprises positioning an expandable sand-control device in the wellbore thereby forming an annulus between the sand-control device and the wellbore; depositing a filter media in the annulus; and after the depositing step, radially expanding the sand-control device to decrease the volume of the annulus. The sand control device can be a sand screen or slotted or perforated liner having radially extending passageways in the walls thereof, the passageways designed to substantially prevent movement of the particulate material through the passageways and into the sand-control device. Where a slotted liner is desired, the passageways can be plugged during positioning and later unplugged for production. The filter media is typically a particulate material and can be deposited as a slurry comprising liquid material and particulate material, or as a cement slurry.

Abstract: Permeable subterranean underground formations and fractures can be sealed using lost circulating material fluids having borate and metallic crosslinked polysaccharide gels that are crosslink in the well bore. Compositions and methods are illustrated whereby lost circulation material solids can be mixed in a mixing tank on the surface with a crosslinkable polysaccharide and a crosslinking agent under conditions whereby the lost circulating material fluid can be pumped into the well bore before undergoing gelation. Once the lost circulation material fluid equilibrates to the reservoir temperature the polysaccharide component of the lost circulation material fluid will crosslink.