Patents by Inventor Cajetan Ikenna Nlebedim

Cajetan Ikenna Nlebedim has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 11984243
    Abstract: Permanent magnet materials are provided. The permanent magnet materials are cerium based materials including zirconium and iron in combination with cobalt. The permanent magnet materials may have the formula Ce2ZrFe15?xCox wherein 6?x?15. In some embodiments, the permanent magnet materials have the formula Ce2+yZr1?yFe(15?x)(2?z)/2)CoxCu((15?x)z/2) wherein 6?x?15, 0?y?0.4, and z=0 or 1. In other embodiments, the permanent magnet materials have the formula Ce2Zrx(Fe1?yCoy)17?2x, where 0<x?1 and 0.4?y?1. Permanent magnets including the permanent magnet materials are also provided.
    Type: Grant
    Filed: March 3, 2022
    Date of Patent: May 14, 2024
    Assignees: UT-BATTELLE, LLC, Iowa State University Research Foundation, Inc.
    Inventors: David S. Parker, Tribhuwan Pandey, Cajetan Ikenna Nlebedim, Xubo Liu
  • Publication number: 20230212709
    Abstract: A compound or complex containing a rare earth element is impinged with a pulsed laser that is so controlled as to photochemically reduce and obtain a rare earth metal (REM). A mixture of REM salts can be impinged using laser light tuned to selectively reduce a particular rare earth-containing salt of the mixture to separate out as its respective rare earth metal.
    Type: Application
    Filed: December 14, 2022
    Publication date: July 6, 2023
    Inventors: Cajetan Ikenna Nlebedim, Abhishek Sarkar, Pranav Shrotriya, Denis Prodius, Ho-Won Noh, Thomas Lograsso
  • Publication number: 20220320608
    Abstract: Fast charging of a lithium-ion battery at 4C rate or 5C rate or more is improved by applying an external magnetic field relative to the battery to establish magnetic field lines that extend in a direction of primary movement of lithium ions toward the graphite anode during fast charging. Deleterious degradation of the graphite anode from repeated fast charging can be reduced or eliminated by practice of the invention.
    Type: Application
    Filed: March 28, 2022
    Publication date: October 6, 2022
    Inventors: Abhishek Sarkar, Cajetan Ikenna Nlebedim, Pranav Shrotiya
  • Publication number: 20210323070
    Abstract: Embodiments of the present invention provide an electromagnet alignment system for AM or 3D printing technology providing improved in-situ alignment of the magnetic particulate material as it is dispensed during deposition to form a 3D shape. In-situ alignment of the magnetic particulate material can be controlled to be unidirectional or multi-directional.
    Type: Application
    Filed: April 15, 2021
    Publication date: October 21, 2021
    Inventors: Cajetan Ikenna Nlebedim, Abhishek Sarkar, Matthew J. Kramer, Thomas Lograsso, Christopher Haase, Somashekara Adinarayanappa, Mariappan Parans Paranthaman
  • Patent number: 11090579
    Abstract: A method is provided for separating and/or purifying different metal oxalates by mixing the different metal oxalates in an aqueous solution comprising oxalic acid and an organic base so that at least one metal oxalate is soluble and at least another metal oxalate is not soluble. Different rare earth metal oxalates and/or transition metal oxalates can be separated.
    Type: Grant
    Filed: January 22, 2019
    Date of Patent: August 17, 2021
    Assignee: Iowa State University Research Foundation, Inc.
    Inventors: Denis Prodius, Cajetan Ikenna Nlebedim, Anja-Verena Mudring
  • Patent number: 10648063
    Abstract: A chemical dissolution method is provided for use in recycling rare earth metal-containing material such as permanent magnet material including end-of-life magnet shapes, magnet scrap and Terfenol-D alloy material by mixing the rare earth metal-containing material and an aqueous solution of a copper (II) salt to dissolve the material in the solution. The dissolved rare earth metal is then precipitated from the aqueous solution as a rare earth metal compound, such as a rare earth metal oxalate, sulfate or phosphate from which rare earth metal oxide can be obtained.
    Type: Grant
    Filed: June 25, 2018
    Date of Patent: May 12, 2020
    Assignee: Iowa State University Research Foundation, Inc.
    Inventors: Anja-Verena Mudring, Denis Prodius, Cajetan Ikenna Nlebedim
  • Publication number: 20190160394
    Abstract: A method is provided for separating and/or purifying different metal oxalates by mixing the different metal oxalates in an aqueous solution comprising oxalic acid and an organic base so that at least one metal oxalate is soluble and at least another metal oxalate is not soluble. Different rare earth metal oxalates and/or transition metal oxalates can be separated.
    Type: Application
    Filed: January 22, 2019
    Publication date: May 30, 2019
    Inventors: Denis Prodius, Cajetan Ikenna Nlebedim, Anja-Verena Mudring
  • Publication number: 20180312941
    Abstract: A chemical dissolution method is provided for use in recycling rare earth metal-containing material such as permanent magnet material including end-of-life magnet shapes, magnet scrap and Terfenol-D alloy material by mixing the rare earth metal-containing material and an aqueous solution of a copper (II) salt to dissolve the material in the solution. The dissolved rare earth metal is then precipitated from the aqueous solution as a rare earth metal compound, such as a rare earth metal oxalate, sulfate or phosphate from which rare earth metal oxide can be obtained.
    Type: Application
    Filed: June 25, 2018
    Publication date: November 1, 2018
    Inventors: Anja-Verena Mudring, Denis Prodius, Cajetan Ikenna Nlebedim
  • Publication number: 20180215854
    Abstract: A method for producing a bonded permanent magnet by additive manufacturing, the method comprising: (i) incorporating components of a reactive precursor material into an additive manufacturing device, the reactive precursor material comprising an amine component, an isocyanate component, and particles having a permanent magnetic composition; and (ii) mixing and extruding the crosslinkable reactive precursor material through a nozzle of the additive manufacturing device and depositing the extrudate onto a substrate under conditions where the extrudate is permitted to cure, to produce a bonded permanent magnet of desired shape. The resulting bonded permanent magnet and articles made thereof are also described.
    Type: Application
    Filed: February 2, 2018
    Publication date: August 2, 2018
    Inventors: M. Parans PARANTHAMAN, Orlando RIOS, William G. CARTER, David FENN, Cajetan Ikenna NLEBEDIM
  • Publication number: 20180122570
    Abstract: A method for producing a bonded permanent magnet by additive manufacturing, comprising: (i) incorporating components of a solid precursor material into at least one deposition head of at least one multi-axis robotic arm of a big area additive manufacturing (BAAM) system, the components of the solid precursor material comprising a thermoplastic polymer and hard magnetic powder; said deposition head performs melting, compounding, and extruding functions; and said BAAM system has an unbounded open-air build space; and (ii) depositing an extrudate of said solid precursor material layer-by-layer from said deposition head until an object constructed of said extrudate is formed, and allowing the extrudate to cool and harden after each deposition, to produce the bonded permanent magnet. The resulting bonded permanent magnet and articles made thereof are also described.
    Type: Application
    Filed: October 27, 2017
    Publication date: May 3, 2018
    Inventors: Ling LI, Mariappan Parans PARANTHAMAN, Vlastimil KUNC, Brian K. POST, Orlando RIOS, Robert H. FREDETTE, John ORMEROD, Cajetan Ikenna NLEBEDIM, Thomas LOGRASSO
  • Publication number: 20180058953
    Abstract: An example apparatus can comprise an emitter to emit radio frequency radiation, an absorber that changes temperature based on emissions from the emitter, and one or more sensors to measure a temperature difference between a sample and a reference coupled to the absorber.
    Type: Application
    Filed: September 1, 2017
    Publication date: March 1, 2018
    Inventors: Tom Byvank, Benjamin S. Conner, Roger A. Kisner, Michael A. McGuire, Orlando Rios, Boyd Evans, Cajetan Ikenna Nlebedim, Ralph William McCallum