Abstract: A freeze-dried soluble coffee product in the form of particles or granules and having a microporous structure is prepared by prechilling a metal plate in a liquid refrigerant, immersing the plate in aqueous extract of coffee solids, reimmersing the plate in a liquid refrigerant, removing the frozen particles in the form of flakes from the plate, grinding and freeze-drying the flakes to produce frozen extract particles with reduced entrainment losses. The product so prepared has a unique porosity and is capable of sorbing, retaining and releasing volatile aromatic compounds.

Abstract: This invention involves applying a warm coffee extract onto a freezing surface in a plurality of layers until a desired thickness is obtained. Thus applied, there is continual melting and refreezing of the extract. This permits the formation of large ice crystals whereby the finished product is darker and more coffee-like in color. Overall efficiency of the freezing process is also increased allowing higher productivity rates.