Abstract: A process and apparatus for the ultrapurification of cryogenic low boiling liquified gases such as oxygen and nitrogen which contain trace impurities. The impure gas is introduced into a first distillation column provided with a top column condenser and a bottom column reboiler. The impure gas is substantially at its liquid-gas equilibrium temperature at the pressures within the first distillation column. Here the gas is separated by distillation into a first vapor fraction containing low boiling point impurities and a first liquid fraction containing high boiling point impurities. The first vapor fraction is withdrawn and introduced into a second distillation column provided with a top column condenser and a bottom column reboiler. The first vapor fraction is substantially at the liquid-gas equilibrium temperature at the pressures within the second distillation column.

Abstract: A process and apparatus for the ultrapurification of cryogenic low boiling liquified gases such as oxygen and nitrogen which contain trace impurities. The impure gas is introduced into a first distillation column and is substantially at its liquid-gas equilibrium temperature at the pressures within the first distillation column. Here the gas is separated by distillation into a first vapor fraction containing low boiling point impurities and a first liquid fraction containing high boiling point impurities. The first vapor fraction is withdrawn and introduced into a second distillation column. The first vapor fraction is substantially at the liquid-gas equilibrium temperature at the pressures within the second distillation column. Here the vapor fraction is separated by distillation into a second vapor fraction containing high boiling point impurities and a second liquid fraction free of trace impurities which is withdrawn as product.