Patents by Inventor Francisco J. Dias

Francisco J. Dias has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 5474587
    Abstract: A process for producing a porous fluid permeable body which is heatable by the passage of electric current therethrough. The process involves coating silicon-containing particles with a cokable organic binder to produce coated particles with a particle size fraction of 0.2 to 10 mm, forming the particles into a molding, coking the binder and heating the molding at 1400.degree. to 2000.degree. C. in the presence of nitrogen to form a doped body containing 30% to 100% .beta.-silicon carbide.
    Type: Grant
    Filed: March 11, 1994
    Date of Patent: December 12, 1995
    Assignee: Forschungszentrum Julich GmbH
    Inventors: Francisco J. Dias, Freimut J. Koch
  • Patent number: 4619805
    Abstract: In order to provide enough permeability (air or liquid throughput) in a pus molded body of carbon made from a mixture of carbon powder and a binder, a first "green" body (a body of the kind that has been fired heretofore, in its green state before firing) is broken up into small pieces with the help of a jaw crusher in a manner providing coarse particles and a fraction of uniform size (largest particle diameter not more than twice the smallest) in the overall range between 0.2 and 10 mm effective diameter is used to make a second green body of molded shape by placing it in a die and applying a pressure which may be light or heavier according to the desired degree of permeability. The second green body is then coked in vacuum or in an inert atmosphere at a temperature in the range between 600.degree. to 1000.degree. C. to produce a strong body through which gas and liquid may pass with a facility far exceeding what has been accomplished before with a body of comparable strength.
    Type: Grant
    Filed: June 3, 1985
    Date of Patent: October 28, 1986
    Assignee: Kernforschungsanlage Julich Gesellschaft mit beschrankter Haftung
    Inventors: Francisco J. Dias, Marian Kampel, Hartmut Luhleich
  • Patent number: 4604249
    Abstract: A molded porous silicon carbide body in the shape of an armor plate, made by coking a mixture of carbon and silicon powder coated with an organic binder to which some silicon carbide powder may be added, and then rapidly raising the temperature to a level at which silicon carbide is formed, is impregnated so that its pores are filled with steel or a steel alloy to produce a plate that has the hardness and stiffness of silicon carbide and the toughness of metal. The plate has superior resistance to hollow or shaped explosive charges. The lower density provided by the silicon carbide favors its use in armored vehicles.
    Type: Grant
    Filed: November 16, 1984
    Date of Patent: August 5, 1986
    Assignee: Kernforschungsanlage Julich GmbH
    Inventors: Hartmut Luhleich, Francisco J. Dias
  • Patent number: 4532091
    Abstract: A porous green-state body of carbon, with or without silicon carbide, made with a cokable binder, is crumbled to produce relatively coarse grains in the range from 0.2 to 10 mm and a fraction of the particles so produced with a much more limited range of grain size is then used to produce a second green-state body, which is then coked, siliconized if the silicon is not already provided in the making of the precursor body that was broken up, and converted into a silicon carbide body. If the siliconizing is done by immersion in a bath of molten silicon, the excess silicon is removed by vaporization or by boiling in sodium hydroxide solution.
    Type: Grant
    Filed: February 13, 1984
    Date of Patent: July 30, 1985
    Assignee: Kernforschungsalage Julich GmbH
    Inventors: Francisco J. Dias, Marian Kampel, Hartmut Luhleich
  • Patent number: 4514346
    Abstract: Refractory parts or articles, even of very large dimensions, are made with starting material of carbon particles mixed with silicon particles in a predetermined ratio which is suspended in a solution of a binder, after which the suspension is squirted into a precipitating liquid to coat the particles with the binder, the solids then being separated and dried, molded under slight pressure, and coked (at 800.degree.-1,000.degree. C.), and then rapidly raised in temperature (to 1,400.degree.-1,600.degree. C.) for formation of silicon carbide throughout the article. It is useful to add powdered silicon carbide and mix it in before the coking step and, also, to hold the heated body at a temperature somewhat below 1,400.degree. C. long enough to remove temperature gradients within it, followed by rapid heating up to a carbide-forming temperature.
    Type: Grant
    Filed: September 16, 1982
    Date of Patent: April 30, 1985
    Assignee: Kernforschungsanlage Julich Gesellschaft Mit Beschrankter Haftung
    Inventors: Hartmut Luhleich, Francisco J. Dias
  • Patent number: 4512858
    Abstract: An anode for electrolytic oxidation of sulfur dioxide is made by coating an lectrode of a graphite-like carbon material with a layer of cokable organic material such as sugar, phenolic resin, and asphalt pitch, heating the coated electrode body in an inert atmosphere to a temperature of between 400.degree. to 800.degree. C. and thereafter heating the coated electrode to a temperature in the range of 1400.degree. to 2000.degree. C., so that the material is first coked on the graphite to produce a porous flow-through electrode body which, thereafter, is heated to a higher temperature, followed by cooling.
    Type: Grant
    Filed: February 13, 1984
    Date of Patent: April 23, 1985
    Assignee: Kernforschungsanlage Julich Gesellschaft mit beschrankter Haftung
    Inventors: Bernd D. Struck, Francisco J. Dias, Hartmut Luhleich, Ursula Paffen nee Siebert
  • Patent number: 4415632
    Abstract: A molded porous silicon carbide body in the shape of an armor plate, made by coking a mixture of carbon and silicon powder coated with an organic binder to which some silicon carbide powder may be added, and then rapidly raising the temperature to a level at which silicon carbide is formed, is impregnated so that its pores are filled with steel or a steel alloy to produce a plate that has the hardness and stiffness of silicon carbide and the toughness of metal. The plate has superior resistance to hollow or shaped explosive charges. The lower density provided by the silicon carbide favors its use in armored vehicles.
    Type: Grant
    Filed: March 7, 1983
    Date of Patent: November 15, 1983
    Assignee: Kernforschungsanlage Julich GmbH
    Inventors: Hartmut Luhleich, Francisco J. Dias
  • Patent number: 4347671
    Abstract: A method of and an apparatus for the drying of articles, especially foodsfs, biological materials and other substances susceptible to cell damage with overheating, wherein the material is spread in a high-vacuum vessel directly adjacent a cooled condenser and is subjected to a vacuum by a pump capable of developing pressures as low as about 0.1 mbar. The chamber is evacuated until there is a noticeable formation of the condenser whereupon the connection between the pump and the chamber is closed and the product is heated to evaporate liquids but below a predetermined temperature (say a maximum of 50.degree. C.) while the condensate resulting from the evaporation is collected directly below the product and is discharged.
    Type: Grant
    Filed: April 3, 1980
    Date of Patent: September 7, 1982
    Assignee: Kernforschungsanlage Juich, Gesellschaft mit beschrankter Haftung
    Inventors: Francisco J. Dias, Willi Hannen, Hartmut Luhleich, Peter Pflaum
  • Patent number: 4314599
    Abstract: A heat-coalescible graphitic aggregate for making graphite molds, graphite uel elements or moderating elements for nuclear reactors, and so on, is made by first forming a suspension of carbon particles in an alkaline solution of phenolformaldehyde. The suspension is then mixed together with acidulated water, the latter being heated to 40.degree. to 70.degree. C. to accelerate the reaction, with violent mixing, as in a jet device, causing a skin of insoluble phenolformaldehyde to be applied as a coating to each of the particles in suspension, which particles readily settle out and are soon separated by decanting and filtration, after which the composite solid is dried and the aqueous liquid is neutralized before being discarded.
    Type: Grant
    Filed: December 18, 1979
    Date of Patent: February 9, 1982
    Assignee: Kernforschungsanlage Julich, Gesellschaft mit beschrankter Haftung
    Inventors: Hartmut Luhleich, Francisco J. Dias
  • Patent number: 4299881
    Abstract: In order to prevent a protective carbide layer on a graphitic molded arti from splitting off under thermal stress, an external carbide layer is provided on a graphitic molded article having a graded content of silicon or zirconium (in the carbide state) that increases from near zero at the interior boundary of the layer to about 50 atomic percent at the exterior. Such a layer is produced either by dipping the graphitic molded article into melted silicon, dipping it into a succession of suspensions of carbon and either silicon or zirconium, with a greater silicon or zirconium content in each successive dip, the suspensions also including a binder resin, or by applying layers of a paste of carbon and either silicon or zirconium, also with some resin, each successive layer having a higher silicon or zirconium content.
    Type: Grant
    Filed: February 19, 1980
    Date of Patent: November 10, 1981
    Assignee: Kernforschungsanlage Julich Gesellschaft mit beschrankter Haftung
    Inventors: Hartmut Luhleich, Peter Pflaum, Francisco J. Dias, Aristides Nauomidis, Arno Schirbach, Hubertus Nickel
  • Patent number: 4293512
    Abstract: In order to prevent a protective carbide layer on a graphitic molded article from splitting off under thermal stress, an external carbide layer is provided on a graphitic molded article having a graded content of silicon or zirconium (in the carbide state) that increases from near zero at the interior boundary of the layer to about 50 atomic percent at the exterior. Such a layer is produced either by dipping the graphitic molded article into melted silicon, dipping it into a succession of suspensions of carbon and either silicon or zirconium, with a greater silicon or zirconium content in each successive dip, the suspensions also including a binder resin, or by applying layers of a paste of carbon and either silicon or zirconium, also with some resin, each successive layer having a higher silicon or zirconium content.
    Type: Grant
    Filed: November 14, 1979
    Date of Patent: October 6, 1981
    Assignee: Kernforschungsanlage Julich GmbH
    Inventors: Hartmut Luhleich, Peter Pflaum, Francisco J. Dias, Aristides Nauomidis, Arno Schirbach, Hubertus Nickel
  • Patent number: 4265843
    Abstract: In the production of shaped silicon-carbide bodies, especially tubes which onsist predominantly of silicon carbide throughout their thickness for use in nuclear-reactor technology, a carbon-containing preform (body of the desired shape) is contacted with elemental silicon powder at a temperature of 1400.degree. C. to 1500.degree. C. and the silicon-contacted carbon-containing body is thereafter treated at a temperature of 1800.degree. C. to 2000.degree. C. to transform at least the major part of the carbon into silicon carbide.
    Type: Grant
    Filed: December 3, 1979
    Date of Patent: May 5, 1981
    Assignee: Kernforschungsanlage Julich Gesellschaft mit berschrankter Haftung
    Inventors: Francisco J. Dias, Ashok K. Gupta, Erno Gyarmati, Marian Kampel, Hartmut Luhleich, Rudolf Munzer, Aristidis Naoumidis
  • Patent number: 4221689
    Abstract: A suspension of novolac resin is first produced by dissolving phenol in an queous formaldehyde solution and the addition of an acid catalyst, followed by heating and refluxing. The hot novolac suspension is diluted with water and then converted into a solution by the addition of alkali hydroxide solution bringing the pH value to the range from 10 to 13. While the solution is still hot, particles of some form of carbon are suspended therein by mixing, vibration, or other agitation and the suspension is fed at 60.degree. C. into acidulated water of a temperature of about 50.degree. C., with the flow of acidulated water and suspension adjusted for a volume ratio of, respectively, 8:1. The resin is thereby precipitated on the surface of the particles and the particles are filtered, washed, and dried to produce a material made up of fine grains, evenly coated with binder, which are useful for making graphitic molds for casting metal.
    Type: Grant
    Filed: October 12, 1978
    Date of Patent: September 9, 1980
    Assignee: Kernforschungsanlage Julich Gesellschaft mit beschrankter Haftung
    Inventors: Francisco J. Dias, Hartmut Luhleich