Abstract: A system and method of characterizing an at least partially hydrophobic sample. The method includes providing an ethanolic solution of ethanol and sodium hydrogen cyanamide, adding a first portion of the ethanolic solution to a sample to produce a reagent-sample mixture, performing infrared spectroscopic testing of the reagent-sample mixture to generate mixture absorption data representing at least one absorption characteristic of the reagent-sample mixture, and generating acidity data for the sample based on the mixture data.

Abstract: Disclosed herein is a method and apparatus for controlling and extending the performance of lubricating fluids, such as lubricating oils. The method comprises simultaneous detection of multiple additives and contaminant levels in the lubricating fluids and measured input of selected additives to the lubricating fluids. The additive and contaminants levels are simultaneously and quantitatively determined using a Fourier transform infrared (FTIR) spectrometer, and any drop in additive levels below pre-specified limits automatically triggers corrective action whereby a computer-controlled delivery system is employed to replenish the depleted additives. The system can also be employed to detect irreversible degradation of the lubricating fluids and direct the degraded fluids to a holding area where they may undergo treatment or disposal and add new fresh lubricating fluids.