Patents by Inventor Ilkka Kilpeläinen

Ilkka Kilpeläinen has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Publication number: 20230383144
    Abstract: According to an example aspect of the present invention, there is provided a method of joining objects of hydrophilic polymeric biomaterials. In the method, an ionic liquid is applied onto the surfaces of the objects; the surfaces are pressed together; and the ionic liquid is removed. The method produces a product that can consist to 100% of biomaterial, with no synthetic polymer or chemicals remaining in the product.
    Type: Application
    Filed: August 4, 2023
    Publication date: November 30, 2023
    Inventors: Lauri Hauru, Alistair King, Ilkka Kilpeläinen, Antti Korpela, Hannes Orelma
  • Patent number: 11753565
    Abstract: According to an example aspect of the present invention, there is provided a method of joining objects of hydrophilic polymeric biomaterials. In the method, an ionic liquid is applied onto the surfaces of the objects; the surfaces are pressed together; and the ionic liquid is removed. The method produces a product that can consist to 100% of biomaterial, with no synthetic polymer or chemicals remaining in the product.
    Type: Grant
    Filed: June 21, 2018
    Date of Patent: September 12, 2023
    Assignee: Teknologian tutkimuskeskus VTT Oy
    Inventors: Lauri Hauru, Alistair King, Ilkka Kilpeläinen, Antti Korpela, Hannes Orelma
  • Publication number: 20230057864
    Abstract: A dispersion of cellulose fibers, a method of preparing the same and uses thereof. The dispersion is produced by providing a cellulose feedstock comprising cellulose fibers; by providing a mixture of an ionic liquid and a protic antisolvent for cellulose as a dispersion medium, the ionic liquid being selected from the group of protic salts of superbases capable of dissolving cellulose; and by mixing said cellulose feedstock into said dispersion medium so as to disperse the cellulose fibers therein to form a dispersion which is stable for at least 24 hours at room temperature. The dispersion can be used as an additive of cellulose pulps for making of fibrous products.
    Type: Application
    Filed: December 18, 2020
    Publication date: February 23, 2023
    Inventors: Lauri Hauru, Ilkka Kilpeläinen, Olli Suontausta, Alexander Deutschle
  • Patent number: 11549200
    Abstract: According to an example aspect of the present invention, there is provided A process for making a cellulose fibre or film comprising the steps of dissolving pulp in an ionic liquid containing a cationic 1,5,7-triazabicyclo[4.4.0]dec-5-enium [TBDH]+ moiety and an anion selected from the group according to Formula a), Formula b) and Formula c), wherein each of R, R2, R3, R4, R5, R7, R8, R9 and R10 is H or an organyl radical and X? is selected from the group consisting of halides, pseudohalides, carboxylates, alkyl sulphite, alkyl sulphate, dialkylphosphite, dialkyl phosphate, dialkyl phosphonites and dialkyl phosphonates, to provide a spinning dope, extruding the spinning dope through a spinneret to form one or more filaments, and a step selected from the group consisting of spinning cellulose fibres from the solution, and extruding a cellulose film from the solution.
    Type: Grant
    Filed: January 30, 2018
    Date of Patent: January 10, 2023
    Assignees: Aalto University Foundation sr, Helsingin Yliopisto
    Inventors: Herbert Sixta, Michael Hummel, Kadvaël Le Boulch, Ilkka Kilpeläinen, Alistair W.T. King, Jussi Helminen, Sanna Hellsten
  • Publication number: 20210403760
    Abstract: According to an example aspect of the present invention, there is provided a method of joining objects of hydrophilic polymeric biomaterials. In the method, an ionic liquid is applied onto the surfaces of the objects; the surfaces are pressed together; and the ionic liquid is removed. The method produces a product that can consist to 100% of biomaterial, with no synthetic polymer or chemicals remaining in the product.
    Type: Application
    Filed: June 21, 2018
    Publication date: December 30, 2021
    Inventors: Lauri Hauru, Alistair King, Ilkka Kilpeläinen, Antti Korpela, Hannes Orelma
  • Patent number: 11130763
    Abstract: The present invention relates to a method of producing a bicyclic guanidine and its derivatives. In particular, the present invention relates to a method of producing triazabicyclodecene (TBD) and its derivatives, particularly alkyl derivatives, such as methyl triazabicyclodecene (MTBD), and MTBD-derived ionic liquids. The invention also relates to the use of said compounds in cellulose dissolution and subsequent processing.
    Type: Grant
    Filed: November 8, 2018
    Date of Patent: September 28, 2021
    Assignee: Helsingin Yliopisto
    Inventors: Jussi Helminen, Alistair King, Ilkka Kilpeläinen
  • Publication number: 20200270256
    Abstract: The present invention relates to a method of producing a bicyclic guanidine and its derivatives. In particular, the present invention relates to a method of producing triazabicyclodecene (TBD) and its derivatives, particularly alkyl derivatives, such as methyl triazabicyclodecene (MTBD), and MTBD-derived ionic liquids. The invention also relates to the use of said compounds in cellulose dissolution and subsequent processing.
    Type: Application
    Filed: November 8, 2018
    Publication date: August 27, 2020
    Inventors: Jussi Helminen, Alistair King, Ilkka Kilpeläinen
  • Publication number: 20200002848
    Abstract: According to an example aspect of the present invention, there is provided A process for making a cellulose fibre or film comprising the steps of dissolving pulp in an ionic liquid containing a cationic 1,5,7-triazabicyclo[4.4.0]dec-5-enium [TBDH]+ moiety and an anion selected from the group according to Formula a), Formula b) and Formula c), wherein each of R, R2, R3, R4, R5, R7, R8, R9 and R10 is H or an organyl radical and X? is selected from the group consisting of halides, pseudohalides, carboxylates, alkyl sulphite, alkyl sulphate, dialkylphosphite, dialkyl phosphate, dialkyl phosphonites and dialkyl phosphonates, to provide a spinning dope, extruding the spinning dope through a spinneret to form one or more filaments, and a step selected from the group consisting of spinning cellulose fibres from the solution, and extruding a cellulose film from the solution.
    Type: Application
    Filed: January 30, 2018
    Publication date: January 2, 2020
    Inventors: Herbert Sixta, Michael Hummel, Kadvaël Le Boulch, Ilkka Kilpeläinen, Alistair W.T. King, Jussi Helminen, Sanna Hellsten
  • Publication number: 20190153625
    Abstract: A method of manufacturing a cellulose-based shaped article. The method comprises subjecting a solution of lignocellulosic material, dissolved in a distillable ionic liquid, to a spinning method, wherein the ionic liquid is a diazabicyclononene (DBN)-based ionic liquid. DBN-based ionic liquids have good dissolution power, high thermal and chemical stability, lack runaway reactions and exhibit low energy consumption, due to low spinning temperatures. The shaped cellulose articles can be used as textile fibres, high-end non-woven fibres, technical fibres, films for packaging, and barriers films in batteries, as membranes and as carbon-fibre precursors.
    Type: Application
    Filed: January 30, 2019
    Publication date: May 23, 2019
    Inventors: Anne Michud, Alistair W.T. King, Arno Parviainen, Herbert Sixta, Lauri Hauru, Michael Hummel, Ilkka Kilpeläinen
  • Patent number: 10208132
    Abstract: A method of modifying a polymer having hydroxyl groups, selected from the group of polysaccharides and lignin, to give a modified polymer comprising the step of contacting said polymer with at least one organic phosphonate salt in order to chemically modify the polymer, said organic phosphonate salt being in a liquid phase. The method of polymer modification provides novel polymers. Modified polymers obtained from a polymer having been treated with at least one organic phosphonate salt are also disclosed. The modified polymers can be used as such or separated and optionally recovered from the solution, optionally being formed into particular materials or shapes.
    Type: Grant
    Filed: May 26, 2014
    Date of Patent: February 19, 2019
    Assignees: Metsa Fibre Oy, Stora Enso Oyj
    Inventors: Alistair W. T. King, Christoph Selg, Pirkko Karhunen, Jorma Matikainen, Ilkka Kilpeläinen
  • Publication number: 20190023862
    Abstract: Method of dewatering nanocellulose and other water soluble of hydrophilic polymers. The method comprises providing an aqueous suspension formed by nanocellulose in water, said nanocellulose having free hydroxyl groups; mixing the aqueous suspension with an ionic liquid or eutectic solvent which is capable of hydrogen bonding to at least a part of the free hydroxyl groups to form a modified suspension; and evaporating off water from the modified suspension in order to dewater the nanocellulose. With the ionic liquid procedure, solvent exchange with repeated centrifugation steps can be avoided, and solvent consumption and costs reduced, and processing sped up. The nanocellulose stabilized in the water-free environment then allows for access to efficient and thorough water-free chemical modification procedures resulting in highly fibrillated products.
    Type: Application
    Filed: September 5, 2016
    Publication date: January 24, 2019
    Inventors: Alistair W.T. King, Ilari Filpponen, Jussi Helminen, Ilkka Kilpeläinen
  • Patent number: 10086530
    Abstract: A method of treating wood with an organic phosphonate salt in a liquid phase to chemically modify its surface and thus provide protection from microorganisms. The organic phosphonate salts are of Formula III wherein R1 is a hydrogen radical or an alkyl or aryl radical having 1 to 20 carbon atoms and R2 is a cation selected from the group of NH4+, H+, Li+, Na+, K+, Rb+, Cs+, Fr+, Cu+, Ag+, substituted or unsubstituted ammonium, phosphonium, and sulfonium, methylpyrrolidinium, isothiazolium, isoxazolium, oxazolium, pyrrolium, thiophenium, pyridinium, pyridazinium, pyrimidinium, pyrazinium, imidazolium, pyrazolium, thiazolium, oxazolium, 1-ethyl-3-methylimidazolium , and triazolium, or a mixture thereof, said method preferably comprising using one or more salt compounds having formula III. Products comprising a raw material having been treated according to the method with one or more organic salts of formula III are also disclosed.
    Type: Grant
    Filed: May 26, 2014
    Date of Patent: October 2, 2018
    Assignees: Stora Enso Oyj, Tikkurila Oyj, Metsäliitto Osuuskunta
    Inventors: Pirkko Karhunen, Jorma Matikainen, Lasse Kyllönen, Pirjo Ahola, Ilkka Kilpeläinen, Alistair W. T. King
  • Publication number: 20160145356
    Abstract: A method of modifying a polymer having hydroxyl groups, selected from the group of polysaccharides and lignin, to give a modified polymer comprising the step of contacting said polymer with at least one organic phosphonate salt in order to chemically modify the polymer, said organic phosphonate salt being in a liquid phase. The method of polymer modification provides novel polymers. Modified polymers obtained from a polymer having been treated with at least one organic phosphonate salt are also disclosed. The modified polymers can be used as such or separated and optionally recovered from the solution, optionally being formed into particular materials or shapes.
    Type: Application
    Filed: May 26, 2014
    Publication date: May 26, 2016
    Inventors: Alistair W.T. King, Christoph Selg, Pirkko Karhunen, Jorma Matikainen, Ilkka Kilpeläinen
  • Patent number: 7850841
    Abstract: The invention relates to a process for producing high-quality hydrocarbon base oil particularly of biological origin. The process of the invention comprises aldol condensation, hydrodeoxygenation, and isomerization steps. Aldehydes and/or ketones, preferably of biological origin are used as the feedstock.
    Type: Grant
    Filed: December 12, 2006
    Date of Patent: December 14, 2010
    Assignee: Neste Oil Oyj
    Inventors: Eija Koivusalmi, Ilkka Kilpeläinen, Pirkko Karhunen, Jorma Matikainen